Refining agent for smelting aluminum alloy and preparation method of refining agent
A refining agent, aluminum alloy technology, applied in the field of aluminum alloy processing, can solve the problems of high hydrogen content and non-metallic inclusion content, achieve good impurity removal effect, improve performance, and reduce metal burning loss.
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[0025] A method for preparing a refining agent for aluminum alloy smelting comprising the above raw materials, comprising the following steps:
[0026] S1: La 2 o 3 Dissolve in hydrochloric acid and dilute to 120-130g / L, heat the solution to 72-75°C, add 48% hydrofluoric acid, stir to obtain a precipitate, then wash, filter, and dry the precipitate until the water content is ≤2% , crushed to a particle size of ≤2mm, and dehydrated under the condition of a vacuum of 0.5-0.8MPa to obtain F 3 La powder;
[0027] S2: put Nd 2 o 3 Dissolve in hydrochloric acid and dilute to 120-130g / L, heat the solution to 72-75°C, add 48% hydrofluoric acid, stir to obtain a precipitate, then wash, filter, and dry the precipitate until the water content is ≤2% , Grinding to particle size ≤ 2mm, and dehydrating under the condition of vacuum degree of 0.5-0.8MPa to obtain FNd powder;
[0028] S3: KCl, NaCl, KNO 3 , MgS, CaS, A1F 3 , NaF, MgF 2 、Na 3 A1F 6 、Na 2 SiF 6 Put the powder into ...
Embodiment 1
[0031] A refining agent for aluminum alloy smelting, in parts by weight, comprising the following raw materials: 40 parts of KCl, 30 parts of NaCl, KNO 3 33 parts, 10 parts of MgS, 10 parts of CaS, A1F 3 7 parts, NaF8 parts, MgF 2 3 parts, Na 3 A1F 6 8 parts, Na 2 SiF 6 2 parts, FNd 0.5 parts, F 3 La 0.5 parts;
[0032] A method for preparing a refining agent for aluminum alloy smelting comprising the above raw materials, comprising the following steps:
[0033] S1: La 2 o 3 Dissolve in hydrochloric acid and dilute to 125g / L, heat the solution to 72°C, add 48% hydrofluoric acid, stir to obtain a precipitate, then wash, filter, dry the precipitate to a water content of ≤2%, and crush to particle size ≤2mm, dehydration under the condition of vacuum degree of 0.8MPa to get F 3 La powder;
[0034] S2: put Nd 2 o 3 Dissolve in hydrochloric acid and dilute to 125g / L, heat the solution to 72°C, add 48% hydrofluoric acid, stir to obtain a precipitate, then wash, filter...
Embodiment 2
[0038] A refining agent for aluminum alloy smelting, in parts by weight, comprising the following raw materials: 36 parts of KCl, 24 parts of NaCl, KNO 3 30 parts, MgS 15 parts, CaS 6 parts, A1F 3 6 parts, NaF 4 parts, MgF 2 8 parts, Na 3 A1F 6 4 parts, Na 2 SiF 6 7 parts, FNd 0.2 parts, F 3 La1.1 part;
[0039] A method for preparing a refining agent for aluminum alloy smelting comprising the above raw materials, comprising the following steps:
[0040] S1: La 2 o 3 Dissolve in hydrochloric acid and dilute to 120g / L, heat the solution to 75°C, add 48% hydrofluoric acid, stir to obtain a precipitate, then wash, filter, dry the precipitate to a water content of ≤2%, and crush to particle size ≤2mm, dehydration under the condition of vacuum degree of 0.6MPa to get F 3 La powder;
[0041] S2: put Nd 2 o 3 Dissolve in hydrochloric acid and dilute to 120g / L, heat the solution to 75°C, add 48% hydrofluoric acid, stir to obtain a precipitate, then wash, filter, dry ...
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