Compounded preparation for preventing and treating amyloodiniosis of large yellow croakers, and preparation method thereof
A technology of dinoflagellate and large yellow croaker, which is applied in the field of breeding, can solve the problems of unstable effect, chronic poisoning of large yellow croaker that pollutes water, etc., and achieve the effects of no secondary pollution, control of pathogenic reproduction, and high activity
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Embodiment 1
[0022] Get 4g of DL-malic acid, 6g of maleic acid and 10g of xylitol and 79.6g of distilled water in a 500ml beaker, add a magnetic bar, after mixing uniformly on a magnetic stirrer, add 0.4g of solid acid catalyst (SO 4 2- / SiO 2 -TiO 2 ), using an ultrasonic cell disruptor with the assistance of ultrasound (frequency 20kHz), place the beaker in a water bath at 80°C for 8 hours to prepare raw material 1; take another 250 beaker, add 1g glyceraldehyde, 10g β-1,4-N- Acetyl-D-amino-glucose 8-mer and 89g distilled water at an intensity of 20W / m 2 The reaction was stirred for 10 h under the irradiation of ultraviolet light to prepare raw material 2. After mixing the raw materials 1 and 2 according to the volume ratio of 1:1, stirring continuously for 2 hours, the finished compound preparation is obtained.
[0023] Place 6 4M aquaculture ponds in a mariculture pond with a depth of 3 meters, a maximum water level of 2.5 meters, clean water, no pollution, and an average salinity ...
Embodiment 2
[0030] Get 2 g of DL-malic acid, 7 g of maleic acid, 4 g of xylitol and 86.7 g of distilled water in a 500 ml beaker, add a magnetic rod, mix well on a magnetic stirrer, and then add 0.3 g of a solid acid catalyst (SO 4 2- / SiO 2 -TiO 2 ), using an ultrasonic cell disruptor with the assistance of ultrasound (frequency 50kHz), put the beaker in a water bath at 60°C for 10h to prepare raw material 1; take another 250 beaker, add 0.4g glyceraldehyde, 5g β-1,4-N - Acetyl-D-amino-glucose 8-mer and 94.6g distilled water at an intensity of 10W / m 2 The reaction was stirred for 20 h under the irradiation of ultraviolet light to prepare raw material 2. After mixing the raw materials 1 and 2 according to the volume ratio of 1:1, stirring continuously for 2 hours, the finished compound preparation is obtained.
[0031] Place 6 4M aquaculture ponds in a mariculture pond with a depth of 3 meters, a maximum water level of 2.5 meters, clean water, no pollution, and an average salinity of ...
Embodiment 3
[0038] Get DL-malic acid 2g, maleic acid 3g and xylitol 4g and 90.7 g of water in a 500ml beaker respectively, add a magnetic bar, after mixing uniformly on a magnetic stirrer, in 0.3g solid acid catalyst (SO 4 2- / SiO 2 -TiO 2 ) under the action of an ultrasonic cell disruptor with the assistance of ultrasound (frequency 80kHz), place the beaker in a water bath at 80°C for 8 hours to prepare raw material 1; take another 250 beaker, add 1g glyceraldehyde, 5g β-1,4- N-acetyl-D-amino-glucose 8-mer and 94ml of distilled water at an intensity of 30W / m 2 The reaction was stirred for 15 h under the irradiation of ultraviolet light to prepare raw material 2. After mixing the raw materials 1 and 2 according to the volume ratio of 1:1, stirring continuously for 2 hours, the finished compound preparation is obtained.
[0039] Place 6 4M aquaculture ponds in a mariculture pond with a depth of 3 meters, a maximum water level of 2.5 meters, clean water, no pollution, and an average sal...
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