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Corrosion-resistant microporous andalusite lightweight refractory brick and preparation method thereof

A technology of refractory bricks and andalusite, applied in the field of refractory materials, can solve the problems of increased damage of refractory materials, increased thermal conductivity of refractory materials, and increased loss of heat energy, so as to improve high temperature resistance and surface corrosion resistance, and strengthen the skeleton structure, the effect of increasing the critical particle size

Inactive Publication Date: 2018-04-24
HENAN HAINADE NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The commonly used refractory castables are mainly Al 2 o 3 -SiO 2 However, when this type of refractory material is used in petrochemical and other industries, due to the influence of the reducing atmosphere environment, the damage of the refractory material will be aggravated, thereby reducing the service life of the material
In addition, due to the large size of pores in traditional refractory aggregates, the pore diameters are mostly at the millimeter level, so when the material is used in a high temperature environment, due to the intensification of radiation heat transfer and convective heat transfer through the gas in the pores, the refractory material will The thermal conductivity of the refractory increases, which in turn reduces the heat insulation effect of the refractory material, increases the loss of heat energy, and leads to an increase in energy costs

Method used

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  • Corrosion-resistant microporous andalusite lightweight refractory brick and preparation method thereof

Examples

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Effect test

Embodiment 1

[0027] This embodiment provides a kind of corrosion-resistant microporous andalusite lightweight refractory brick, which includes a refractory brick substrate and a high-temperature-resistant coating coated on the surface of the refractory brick substrate; wherein, the preparation raw materials for the refractory brick substrate include: 20% andalusite particles, 30% calcium aluminate fine powder, 20% metakaolin superfine powder, 3% alumina, 17% bonded clay, 10% pulp water; the raw materials for the preparation of the high temperature resistant coating include: silicon carbide Whiskers 3%, Silica Airgel 20%, Yttrium Oxide Gel 50%, Water 27%.

[0028] Wherein, the particle size of the andalusite particles is 1 mm to 3 mm, the particle size of the calcium aluminate fine powder is less than 0.074 mm, the particle size of the metakaolin superfine powder is less than 0.074 mm, and the particle size of the alumina is less than 0.043 mm . The chemical composition of each raw materia...

Embodiment 2

[0035]This embodiment provides a kind of corrosion-resistant microporous andalusite lightweight refractory brick, its structure includes refractory brick substrate and the high temperature resistant coating that is coated on the surface of described refractory brick substrate; Wherein, the raw material that makes refractory brick substrate includes : 20% of andalusite particles, 25% of calcium aluminate fine powder, 25% of metakaolin superfine powder, 5% of aluminum oxide, 10% of combined clay and 15% of pulp water; the raw materials for preparing the high temperature resistant coating include: Silicon carbide whiskers 3%, silica airgel 25%, yttrium oxide gel 50%, water 22%.

[0036] The preparation method of the corrosion-resistant microporous andalusite lightweight refractory brick described in this example is the same as that in Example 1. After testing, the density of the corrosion-resistant microporous andalusite lightweight refractory bricks prepared in this example is 1...

Embodiment 3

[0038] This embodiment provides a kind of corrosion-resistant microporous andalusite lightweight refractory brick, which includes a refractory brick substrate and a high-temperature-resistant coating coated on the surface of the refractory brick substrate; wherein, the preparation raw materials for the refractory brick substrate include: 20% andalusite particles, 23% calcium aluminate fine powder, 19% metakaolin superfine powder, 3% alumina, 10% bonded clay, 25% pulp water; the raw materials for the preparation of the high temperature resistant coating include: silicon carbide Whiskers 3%, Silica Airgel 20%, Yttrium Oxide Gel 60%, Water 17%.

[0039] The preparation method of the corrosion-resistant microporous andalusite lightweight refractory brick described in this example is the same as that in Example 1. After testing, the density of the corrosion-resistant microporous andalusite lightweight refractory bricks prepared in this example is 1.6 g / cm 3 .

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Abstract

The invention provides a corrosion-resistant microporous andalusite lightweight refractory brick. The refractory brick comprises a refractory brick matrix and a high-temperature resistant coating which coats the surface of the refractory brick matrix; the refractory brick matrix comprises the following preparation raw materials: 20%-30% of andalusite particles, 23%-30% of calcium aluminate fine powder, 19%-27% of metakaolin ultrafine powder, 3%-5% of aluminium oxide, 10%-18% of bonding clay, and the balance of paper pulp water; and the high-temperature resistant coating comprises the followingpreparation raw materials: 3%-6% of silicon carbide crystal whiskers, 20%-25% of silicon dioxide aerogel, 50%-60% of yttrium oxide gel, and the balance of water. According to the corrosion-resistantmicroporous andalusite lightweight refractory brick provided by the invention, uniformly-distributed micron-sized air pores are formed in the brick, and the brick has better thermal stability and higher refractoriness under load. The invention also provides a preparation method of the above corrosion-resistant microporous andalusite lightweight refractory brick. The method provided by the invention has simple steps and is convenient for automatic production.

Description

technical field [0001] The invention belongs to the technical field of refractory materials, and in particular relates to a corrosion-resistant microporous andalusite lightweight refractory brick and a preparation method thereof. Background technique [0002] Refractory materials are widely used in metallurgy, petrochemical, glass and other high-temperature industries due to their good corrosion resistance to high-temperature media and their thermal insulation properties. As my country's emphasis on energy saving and consumption reduction continues to increase, more research and development has been done on lightweight refractory materials with good thermal insulation effects. Unshaped refractory materials have received special attention due to their advantages of convenient construction, low production cost, and good overall structure of the lining, among which refractory castables are the most widely used. [0003] The commonly used refractory castables are mainly Al 2 o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/66C04B38/00C04B41/87
CPCC04B35/66C04B38/00C04B41/5045C04B41/87C04B2235/3208C04B2235/3217C04B2235/3222C04B2235/3463C04B2235/349C04B2235/77C04B2235/96C04B41/5035C04B41/4596C04B41/4539C04B41/0072C04B38/0054C04B38/0067
Inventor 张微微计富宝吉飞虎
Owner HENAN HAINADE NEW MATERIAL CO LTD
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