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Anti-corrosion microporous flint clay lightweight refractory brick and preparation method thereof

A technology of refractory bricks and microporous coke, which is applied in the field of refractory materials, can solve the problems of increased damage to refractory materials, increased loss of heat energy, and increased thermal conductivity of refractory materials, so as to improve high temperature resistance and surface corrosion resistance. The effect of critical particle size and strong skeleton structure

Inactive Publication Date: 2018-04-24
HENAN HAINADE NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The commonly used refractory castables are mainly Al 2 o 3 -SiO 2 However, when this type of refractory material is used in petrochemical and other industries, due to the influence of the reducing atmosphere environment, the damage of the refractory material will be aggravated, thereby reducing the service life of the material
In addition, due to the large size of pores in traditional refractory aggregates, the pore diameters are mostly at the millimeter level, so when the material is used in a high temperature environment, due to the intensification of radiation heat transfer and convective heat transfer through the gas in the pores, the refractory material will The thermal conductivity of the refractory material increases, which in turn reduces the heat insulation effect of the refractory material, increases the loss of heat energy, and leads to an increase in energy costs.

Method used

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  • Anti-corrosion microporous flint clay lightweight refractory brick and preparation method thereof

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Experimental program
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Effect test

Embodiment 1

[0027] This embodiment provides a kind of corrosion-resistant microporous coke stone lightweight refractory brick, its structure includes a refractory brick substrate and a high temperature resistant coating coated on the surface of the refractory brick substrate; wherein, the preparation raw material of the refractory brick substrate Including the following materials by mass percentage: 30% of burnt gemstone aggregate, 20% of metakaolin superfine powder, 29% of ceramic refractory fiber, 0.1% of expanded graphite, 10.9% of bonded clay, and 10% of pulp water. The raw materials for the preparation of the high-temperature-resistant coating include the following materials in mass percentages: 5% silicon nitride whiskers, 45% yttrium oxide gel, 30% silica airgel, and 20% ethanol.

[0028] Wherein, the particle size of the burnt gemstone aggregate is 1 mm to 3 mm, the particle size of the metakaolin superfine powder is less than 0.074 mm, and the length of the ceramic refractory fibe...

Embodiment 2

[0036] This embodiment provides a kind of corrosion-resistant microporous coke stone lightweight refractory brick, its structure includes refractory brick substrate and the high temperature resistant coating that is coated on the surface of described refractory brick substrate; Wherein, making described refractory brick substrate includes The following mass percentages of materials: 20% of burnt gemstone aggregate, 25% of metakaolin superfine powder, 30% of ceramic refractory fiber, 0.1% of expanded graphite, 14.9% of bonded clay, and 10% of pulp water; The layer includes the following materials in mass percentage: silicon nitride whisker 7%, yttrium oxide gel 25%, silica airgel 33%, ethanol 35%.

[0037] The preparation method of the corrosion-resistant microporous coke gem lightweight refractory brick described in this embodiment is the same as that in Example 1. After testing, the density of the corrosion-resistant microporous coke gem lightweight refractory bricks prepared...

Embodiment 3

[0039] This embodiment provides a kind of corrosion-resistant microporous coke stone lightweight refractory brick, its structure includes refractory brick substrate and the high temperature resistant coating that is coated on the surface of described refractory brick substrate; Wherein, making described refractory brick substrate includes The following mass percentages of materials: 27% of burnt gemstone aggregate, 23% of metakaolin superfine powder, 29% of ceramic refractory fiber, 0.15% of expanded graphite, 5.85% of bonded clay, and 15% of pulp water; The layer includes the following materials in mass percentage: silicon nitride whisker 5%, yttrium oxide gel 45%, silica airgel 35%, ethanol 15%.

[0040] The preparation method of the corrosion-resistant microporous coke gem lightweight refractory brick described in this embodiment is the same as that in Example 1. After testing, the density of the corrosion-resistant microporous coke gem lightweight refractory bricks prepare...

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Abstract

The invention provides a kind of corrosion-resistant microporous burnt stone lightweight refractory brick, comprising a refractory brick substrate and a high temperature resistant coating coated on the surface of the refractory brick substrate; wherein, the preparation raw materials for the refractory brick substrate include: burnt gemstone Aggregate 20%~30%, metakaolin superfine powder 17%~25%, ceramic refractory fiber 25%~30%, expanded graphite 0.1%~0.15%, bonded clay 5%~15%, and the balance is pulp water; The raw materials for the preparation of the high temperature resistant coating include: 5%-7% of silicon nitride whiskers, 25%-45% of yttrium oxide gel, 30%-35% of silicon dioxide airgel, and ethanol as the balance. The corrosion-resistant microporous coke gem lightweight refractory brick has evenly distributed micron-sized pores inside, and has good thermal stability and high load softening temperature. The invention also provides a method for preparing the corrosion-resistant microporous coke gemstone lightweight refractory brick. The method has simple steps and is easy for automatic production.

Description

technical field [0001] The invention belongs to the technical field of refractory materials, and in particular relates to a corrosion-resistant microporous coke jewel lightweight refractory brick and a preparation method thereof. Background technique [0002] Refractory materials are widely used in metallurgy, petrochemical, glass and other high-temperature industries due to their good corrosion resistance to high-temperature media and their thermal insulation properties. As my country's emphasis on energy saving and consumption reduction continues to increase, more research and development has been done on lightweight refractory materials with good thermal insulation effects. Unshaped refractory materials have received special attention due to their advantages of convenient construction, low production cost, and good overall structure of the lining, among which refractory castables are the most widely used. [0003] The commonly used refractory castables are mainly Al 2 o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B33/13C04B38/08C04B41/85
CPCC04B33/13C04B38/08C04B41/009C04B41/5089C04B41/85C04B2235/5216C04B41/5066C04B41/5027
Inventor 张微微计富宝吉飞虎
Owner HENAN HAINADE NEW MATERIAL CO LTD
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