Sound-absorption and anti-corrosion rubber specially used for ultrasonic device
A technology of anti-corrosion rubber and ultrasonic device, which is applied in the field of polymer materials to achieve excellent ultrasonic absorption performance and good anti-corrosion effect.
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Embodiment 1
[0020] Graphene oxide was prepared by the Hummers method. Cool 4L of 98% concentrated sulfuric acid to 0°C, add 20g of graphene, 10g of sodium nitrate and 6g of potassium permanganate, stir magnetically in a water bath at 0°C for 5 hours, heat up to 35°C, and react 30min, add 1L of deionized water, rapidly raise the temperature to 98°C, keep for 15min, stop heating, use 40°C deionized water to make up to 10L, add 1L of 30% hydrogen peroxide and 7L of 5% hydrochloric acid for pickling, magnetically stir for 5min, centrifuge and wash (7000r Remove the supernatant after centrifuging at 10 min at 10 min, stir for 1 min, add deionized water and centrifuge at 7000 r / min for 10 min, repeat this 3 times or more) until the pH is close to neutral to obtain graphite oxide, ultrasonic 2 h, make it fully peeled off, A graphene oxide suspension was prepared.
[0021] The glass fibers were leached in a 1.0 mg / ml graphene oxide suspension for 5 minutes, and then dried at 120° C. to obtain gra...
Embodiment 2
[0036] Graphene oxide was prepared by the Hummers method. Cool 4L of 98% concentrated sulfuric acid to 0°C, add 20g of graphene, 10g of sodium nitrate and 6g of potassium permanganate, stir magnetically in a water bath at 0°C for 5 hours, heat up to 35°C, and react 30min, add 1L of deionized water, rapidly raise the temperature to 98°C, keep for 15min, stop heating, use 40°C deionized water to make up to 10L, add 1L of 30% hydrogen peroxide and 7L of 5% hydrochloric acid for pickling, magnetically stir for 5min, centrifuge and wash (7000r Remove the supernatant after centrifuging at 10 min at 10 min, stir for 1 min, add deionized water and centrifuge at 7000 r / min for 10 min, repeat this 3 times or more) until the pH is close to neutral to obtain graphite oxide, ultrasonic 2 h, make it fully peeled off, A graphene oxide suspension was prepared.
[0037] The glass fiber was leached in a 1.2 mg / ml graphene oxide suspension for 5 minutes, and then dried at 120°C to obtain a graph...
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