Polymer with water plugging profile control performance, preparation method and application thereof
A technology for water plugging and profile control and polymer, which is applied to drilling compositions, chemical instruments and methods, etc., and can solve the problem of short action distance of water plugging and profile control agents, chromatographic separation, and gelation reactivity of water plugging and profile control agents. Uncontrollable and other problems, to achieve the effect of aging retention and high viscosity
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[0032] In a second aspect, the present invention provides a method for preparing a polymer with water shutoff and profile control properties, wherein the method includes: in the presence of an initiator and water as a solvent, and under an inert gas atmosphere, make a single Body D, monomer E and monomer F carry out solution polymerization; Wherein, the monomer D is an acrylamide monomer, and the monomer E is 2-acrylamido-2-methylpropanesulfonic acid (AMPS) monomer, the monomer F is a monomer having a structure shown in formula (1); wherein, the amount of the monomer D, the monomer E and the monomer F is such that in the prepared polymer, the amount of the structural unit A The content is 60-98% by weight, the content of structural unit B is 1-39% by weight, and the content of structural unit C is 1-39% by weight;
[0033]
[0034] Among them, in formula (1), R 1 , R 2 , R 3 Each is independently H, C1-C12 alkyl, C6-C12 substituted or unsubstituted aryl; R 4 C1-C12 alky...
specific Embodiment approach
[0049] According to a preferred embodiment of the present invention, the preparation method of the polymer with water shutoff and profile control properties comprises the following steps:
[0050] Step 1: Add monomer D, monomer E and monomer F to the polymerization reactor to prepare an aqueous solution, adjust the pH value of the aqueous solution to 8-10 with alkali, and pass nitrogen gas for 5-60 minutes to remove it of oxygen;
[0051] Step 2: Add an initiator to the aqueous solution in Step 1 and mix evenly, stop feeding nitrogen gas and seal it, and polymerize for 5-10 hours to obtain a colloidal polymer aqueous solution; wherein, when the initiator is azo When the initiator is a redox type initiator, the temperature of the polymerization reaction is 40-70°C; when the initiator is a redox type initiator, the temperature of the polymerization reaction is 15-30°C;
[0052] Step 3: Take out the colloid and then granulate, dry, pulverize and sieve to obtain the polymer produ...
Embodiment 1
[0062] This example is used to illustrate the polymer with water shutoff and profile control properties provided by the present invention and its preparation method
[0063] (1) 225 parts by mass of acrylamide (AM), 50 parts of 2-acrylamido-2-methylpropanesulfonic acid (AMPS) and 12.5 parts of acrylamide shown in formula (2) The methyl ester compound was dissolved in 1000 parts of water under stirring, the pH value of the solution was adjusted to 9.2 with sodium hydroxide, and at room temperature, the aqueous solution was purged with nitrogen for 30 minutes.
[0064]
[0065] (2) Add 0.02 parts of initiator 2,2-azobis(2-methylpropionamidine) hydrochloride (AIBA), stop feeding nitrogen at the same time, and react at a constant temperature of 50°C under airtight conditions for 6 hours, A gummy polymer solution product was obtained.
[0066] (3) The product is dried, granulated, pulverized, and sieved to obtain the polymer A1 with water shutoff and profile control properties of...
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