Iridium-nickel alloy and preparation method and application thereof
A technology of nickel alloy and alloy liquid, applied in the field of spark plug iridium electrode preparation, can solve the problems of easy falling off of alloy, large thermal expansion coefficient of nickel-based alloy, limited application, etc., and achieve the effect of saving precious metal and good resistance to cold and heat fatigue.
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Embodiment 1
[0037] An iridium-nickel alloy is composed of the following components in mass percentage: 40% iridium and 60% nickel. Its preparation method comprises the following steps:
[0038] (1) Mold installation: Assemble a smelting mold with a cavity diameter of 20 mm and a length of 60 mm in a vacuum electric arc furnace;
[0039] (2) Loading samples: start the vacuum electric arc furnace, put 40g of high-purity iridium (>99.9 wt.%) and 60g of high-purity nickel (>99.9 wt.%) into the crucible of the vacuum electric arc furnace;
[0040] (3) Vacuuming: Open the vacuum valve and evacuate the vacuum electric arc furnace to a vacuum degree of 2.0×10 -3 MPa, then tighten the vacuum valve;
[0041] (4) Gas filling: fill the sample chamber of the vacuum electric arc furnace with argon until the vacuum degree is 0.50MPa;
[0042] (5) Repeat step (2) to step (3);
[0043] (6) The vacuum electric arc furnace is energized, the arc is melted to melt the mixture of Ni and Ir, and the heating...
Embodiment 2
[0053] An iridium-nickel alloy is composed of the following components in mass percentage: 70% iridium and 30% nickel. Its preparation method comprises the following steps:
[0054] (1) Mold installation: Assemble a smelting mold with a cavity diameter of 30 mm and a length of 50 mm in a vacuum electric arc furnace;
[0055] (2) Loading samples: start the vacuum electric arc furnace, put 70g of high-purity iridium (>99.9 wt.%) and 30g of high-purity nickel (>99.9 wt.%) into the crucible of the vacuum electric arc furnace;
[0056] (3) Vacuuming: Open the vacuum valve and evacuate the vacuum electric arc furnace to a vacuum degree of 5.0×10 -3 MPa, then tighten the vacuum valve;
[0057] (4) Gas filling: fill the sample chamber of the vacuum electric arc furnace with argon until the vacuum degree is 0.80MPa;
[0058] (5) Repeat steps (2) to (3) twice;
[0059] (6) The vacuum electric arc furnace is energized, the arc is melted to melt the mixture of Ni and Ir, and the heati...
Embodiment 3
[0069] An iridium-nickel alloy is composed of the following components in mass percentage: 50% iridium and 50% nickel. Its preparation method comprises the following steps:
[0070] (1) Mold installation: Assemble a smelting mold with a cavity diameter of 45 mm and a length of 20 mm in a vacuum electric arc furnace;
[0071] (2) Loading samples: start the vacuum electric arc furnace, put 50g of high-purity iridium (>99.9 wt.%) and 50g of high-purity nickel (>99.9 wt.%) into the crucible of the vacuum electric arc furnace;
[0072] (3) Vacuuming: Open the vacuum valve and evacuate the vacuum electric arc furnace to a vacuum degree of 3.5×10 -3 MPa, then tighten the vacuum valve;
[0073] (4) Gas filling: fill the sample chamber of the vacuum electric arc furnace with argon until the vacuum degree is 0.65MPa;
[0074] (5) Repeat steps (2) to (3) three times;
[0075] (6) The vacuum electric arc furnace is energized, the arc is melted to melt the mixture of Ni and Ir, and the...
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