Bamboo fiber/polypropylene composite material as well as preparation method and application thereof
A composite material and bamboo fiber technology, applied in the field of bamboo fiber/polypropylene composite material and its preparation, can solve the problems of bamboo fiber being difficult to disperse, poor compatibility, etc. The effect of increasing the interfacial adhesion
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Embodiment 1
[0029] Step 1: Prepare modified bamboo fiber
[0030] First weigh bamboo fiber, wash it alternately with hydrochloric acid and water, put it into an oven to dry after washing; place the dried bamboo fiber and oleic acid for 6 hours, add methanol after standing, and the mass ratio of bamboo fiber: oleic acid: methanol is 1:2:4, after heating to 70°C, add 10% sodium dihydrogen phosphate of bamboo fiber mass and 10% N,N-dimethylacetamide of bamboo fiber mass, stir and react for 2 hours to obtain the reactant, wash with deionized water After freeze-drying, the modified bamboo fiber can be obtained.
[0031] Step 2: Prepare raw materials
[0032] In parts by weight, respectively select 25 parts of homopolypropylene, 25 parts of copolymerized polypropylene, 10 parts of calcium carbonate with a particle size of 2 microns, 3 parts of modified bamboo fiber, 0.1 part of coupling agent, 0.1 part of antioxidant, auxiliary 0.2 parts of antioxidant, 0.2 parts of lubricant;
[0033] Where...
Embodiment 2
[0043] Step 1: Prepare modified bamboo fiber
[0044] First weigh bamboo fiber, wash it alternately with hydrochloric acid and water, put it into an oven to dry after washing; place the dried bamboo fiber and oleic acid for 7 hours, add methanol after standing, and the mass ratio of bamboo fiber: oleic acid: methanol is 1:2:4, after heating to 75°C, add 13% sodium dihydrogen phosphate of bamboo fiber mass and 15% N,N-dimethylacetamide of bamboo fiber mass, stir and react for 2.5h to obtain the reactant, use deionized After washing with water, freeze-drying, the modified bamboo fiber can be obtained.
[0045] Step 2: Prepare raw materials
[0046] In terms of parts by weight, respectively select 30 parts of homopolypropylene, 45 parts of copolymerized polypropylene, 20 parts of calcium carbonate with a particle size of 3 microns, 10 parts of modified bamboo fiber, 0.3 parts of coupling agent, and 2 parts of compatibilizer. 0.2 parts of oxygen agent, 0.4 parts of auxiliary ant...
Embodiment 3
[0057] Step 1: Prepare modified bamboo fiber
[0058] First weigh bamboo fiber, wash it alternately with hydrochloric acid and water, and put it into an oven to dry after washing; place the dried bamboo fiber and oleic acid for 8 hours, add methanol after standing, and the mass ratio of bamboo fiber: oleic acid: methanol is 1:2:4, after heating to 78°C, add 15% sodium dihydrogen phosphate of bamboo fiber mass and 20% N,N-dimethylacetamide of bamboo fiber mass, stir for 3 hours, and use deionized water to obtain the reactant Washing, freeze-drying after washing, the modified bamboo fiber can be obtained.
[0059] Step 2: Prepare raw materials
[0060] According to parts by weight, select respectively 40 parts of homopolypropylene, 60 parts of copolymerized polypropylene, 30 parts of calcium carbonate with a particle size of 4 microns, 15 parts of modified bamboo fiber, 0.5 part of coupling agent, and 5 parts of compatibilizer. 0.3 parts of oxygen agent, 0.6 parts of auxiliary...
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