Preparation method of binuclear rhodamine bispyrazole acetate organic laser material
A technology of bispyrazole acetate and bispyrazole acetic acid, which is applied in the field of dual-core rhodamine bispyrazole acetate organic laser materials, can solve the problems that organic lasers are difficult to realize and plague the development of organic lasers, and achieve the cost of preparation Effects of low, excellent thermal stability, high luminous efficiency and mobility
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Embodiment 1
[0026] The preparation method of rhodamine bispyrazole acetate organic laser material comprises the following steps: in the presence of triethylamine, rhodamine 110 and bis(1-pyrazole)acetic acid are reacted at room temperature for 3-5 hours to obtain bispyrazole Acetic acid coumarin derivative; wherein, the molar ratio of bis(1-pyrazole), rhodamine 110, and triethylamine is 1.1:1:3; the yield is 85.6%;
[0027] The reaction formula is:
[0028]
Embodiment 2
[0030] The preparation method of rhodamine bispyrazole acetate organic laser material comprises the following steps: in the presence of triethylamine, rhodamine 110 and bis(1-pyrazole) acetic acid are reacted at room temperature for 5 hours to obtain bispyrazole acetic acid aroma Soybein derivatives; wherein, the molar ratio of bis(1-pyrazole), rhodamine 110, and triethylamine is 1:1:2; the yield is 84.2%.
Embodiment 3
[0032] The preparation method of rhodamine bispyrazole acetate organic laser material comprises the following steps: in the presence of triethylamine, rhodamine 110 and bis(1-pyrazole) acetic acid are reacted at room temperature for 3 hours to obtain bispyrazole acetic acid aroma Soybein derivatives; wherein, the molar ratio of bis(1-pyrazole), rhodamine 110, and triethylamine is 1.2:1:4; the yield is 83.6%.
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