High-strength and high-conductivity graphene reinforced copper matrix composite material, preparation method and application thereof
A technology of copper-based composite materials and graphene, applied in metal processing equipment, transportation and packaging, etc., can solve the problems of not meeting the requirements of high-strength and high-conductivity copper-based composite materials, and avoid oxidation and graphene structure damage, The effect of preventing agglomeration and improving the uniformity of dispersion
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Embodiment 1
[0054] Prepare 0.5wt% graphene-reinforced copper-based composite material, graphene and quasi-spherical copper powder are commercially available, and the specific steps are as follows:
[0055] (1) Mix 5g of graphene with 2000ml of absolute ethanol, first carry out shear dispersion treatment in a high-speed shear disperser, wherein the rotating speed is 7000rpm, and the time is 0.5h; then perform ultrasonic oscillation treatment in an ultrasonic cell pulverizer To disperse the graphene, the ultrasonic frequency is 50KHz, and the running time is 5h to obtain a graphene monodisperse liquid; 1kg of copper powder (15-25 μm in particle size, spherical shape) is added to the graphene monodisperse liquid, and then Put the mixture of graphene monodispersion and copper powder into a ball mill jar for mechanical ball milling for 18 hours, the ball-to-material ratio in the ball mill jar is 20:1, the ball mill speed is 100rpm, and the total amount of the mixture does not exceed 2 / 3 of the ...
Embodiment 2
[0065] Prepare 0.1wt% graphene-reinforced copper-based composite material, graphene and quasi-spherical copper powder are commercially available, and the specific steps are as follows:
[0066] (1) Mix 0.1g of graphene with 500ml of absolute ethanol, first carry out shear dispersion treatment in a high-speed shear disperser, wherein the rotation speed is 2000rpm, and the time is 4h; then perform ultrasonic oscillation treatment in an ultrasonic cell pulverizer To disperse the graphene, the ultrasonic frequency is 50KHz, and the operation time is 0.5h to obtain a graphene monodisperse liquid; 0.1kg copper powder (15-20 μm in particle size, spherical shape) is added to the graphene monodisperse liquid , then the graphene monodispersion and the copper powder mixture are placed in a ball milling tank for mechanical ball milling for 2h, the ball-to-material ratio in the ball milling tank is 50:1, the ball milling speed is 500rpm, and the total amount of the mixture is no more than 2...
Embodiment 3
[0076] Prepare 1wt% graphene-reinforced copper-based composite material, graphene and quasi-spherical copper powder are commercially available, and the specific steps are as follows:
[0077] (1) 1g graphene is mixed with 1000ml absolute ethanol, first carry out shear dispersion process in high-speed shear disperser, wherein, rotating speed is 4000rpm, time is 2h; Graphene is dispersed, the ultrasonic frequency is 50KHz, and the running time is 2h to obtain a graphene monodisperse liquid; 0.1kg of copper powder (20-40 μm in particle size, spherical shape) is added to the graphene monodisperse liquid, and then Put the mixture of graphene monodispersion and copper powder into a ball mill jar for mechanical ball milling for 4 hours, the ball-to-material ratio in the ball mill jar is 10:1, the ball mill speed is 400rpm, and the total amount of the mixture does not exceed 2 / 3 of the volume of the ball mill jar; graphite is obtained Mixture of ethylene / copper composite powder and et...
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