Negative electrode of high-specific energy lithium-ion battery and preparation method of negative electrode
A lithium-ion battery, negative electrode technology, applied in battery electrodes, batteries, secondary batteries, etc., can solve problems such as electrode collapse and fall off, and achieve the effect of offsetting volume expansion, reducing unsafe risks, and improving bonding strength
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[0024] The present invention also proposes a method for preparing a negative electrode of a high specific energy lithium ion battery, comprising the following steps:
[0025] S1 Add the negative electrode active material, conductive agent 1, conductive agent 2 and binder into deionized water, and fully stir to obtain negative electrode slurry;
[0026] S2 Coat the above-mentioned negative electrode slurry with a coating machine on a copper foil current collector with a thickness of 4-12um, a porosity of 0%-50%, and a pore size of 0-200um, and dry it;
[0027] S3 rolling the copper foil current collector dried in step S2 to make a negative electrode sheet.
[0028] In a specific embodiment of the present invention, the copper foil current collector is one or more of rolled copper foil, electrolytic copper foil, smooth surface foil, and rough surface foil.
[0029] In a specific embodiment of the present invention, the thickness of the copper foil current collector coated with ...
Embodiment 1
[0033] The negative electrode active material is silicon oxygen carbon, the conductive agent 1 and the conductive agent 2 are SP and VGCF, and the binder is CMC and SBR.
[0034] Add appropriate amount of deionized water to silicon oxygen carbon, SP, VGCF, CMC, and SBR according to the mass ratio of 88:3:3:3.5:2.5, and fully stir to prepare slurry. The solid content of the slurry is 35-50%. The viscosity is 4000-6000mPas. Use the coating machine to coat the prepared slurry on the smooth copper foil with a thickness of 8um and a porosity of 0% with a gap of 150um, and dry it. The coated copper foil Roll to a thickness of 60um to make a negative electrode sheet, measure its peeling force, use this electrode sheet to make a 2Ah full battery, the positive electrode matches the ternary positive electrode, and the formula is NCM523:sp:KS-6:PVDF=88:2:2 : 8, the electrolyte is 1MLiPF6inEC / EMC / DEC (1:1:1v / v)+2%VC, and the diaphragm is 25umPP diaphragm. Electrochemical characterization...
Embodiment 2
[0036] The negative electrode active material is silicon oxygen carbon, the conductive agent 1 and the conductive agent 2 are SP and SFG, and the binder is CMC and SBR.
[0037] Add an appropriate amount of deionized water to silocarb, SP, SFG, CMC, and SBR according to the mass ratio of 88:3:3:3.5:2.5, and fully stir to prepare a slurry. The solid content of the slurry is 35-50%. The viscosity is 4000-6000mPas. Use a coating machine to coat the prepared slurry on a smooth copper foil with a thickness of 8um, a porosity of 20%, and a pore diameter of 30um with a gap of 150um, and dry it. The copper foil is rolled to a thickness of 60um to make a negative pole piece, and its peeling force is measured. This pole piece is used to make a 2Ah full battery. The positive electrode matches the ternary positive electrode. The formula is NCM523:sp:KS-6:PVDF=88: 2:2:8, the electrolyte is 1MLiPF6inEC / EMC / DEC (1:1:1v / v)+2%VC, and the diaphragm is 25umPP diaphragm. Electrochemical characte...
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