Pulling device and pulling method for growing monocrystalline silicon

A technology for growing single crystal silicon and single crystal silicon, applied in chemical instruments and methods, crystal growth, single crystal growth and other directions, can solve problems such as uneconomical and complex production process of solid silicon material, save investment and reduce energy consumption , to ensure the effect of purity

Inactive Publication Date: 2018-07-20
新疆知信科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Chemical vapor deposition or thermal decomposition of gaseous silicon sources is generally carried out at high temperatures, while the production of crystalline silicon from solid silicon materials is generally heated from room temperature to above the melting temperature of silicon. Therefore, from an energy perspective, from high-temperature gaseous silicon sources to It is uneconomical to produce crystalline silicon from solid silicon material at room temperature and then to molten high-temperature silicon liquid
In addition, the production process of solid silicon material itself is relatively complicated and requires special equipment, such as the free space method disclosed in patents CN200580017512 and EP2019084A2. Solid silicon grown from polycrystalline ingots or single crystals

Method used

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  • Pulling device and pulling method for growing monocrystalline silicon
  • Pulling device and pulling method for growing monocrystalline silicon

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Such as figure 1 As shown, this embodiment provides a pulling device for growing single crystal silicon, including:

[0039] The first chamber 1 is provided with a tubular reactor 2 for heating and a first crucible 3 inside the first chamber 1. The first crucible 3 is used to hold molten silicon, and the gaseous silicon source is thermally decomposed in the tubular reactor 2 The reaction generates silicon powder, and silicon powder or silicon powder is melted into molten silicon and enters into the first crucible 3; specifically, the tubular reactor 2 in this embodiment includes a tube body 21 and a heating element for heating the tube body 21 The tube body 21 includes a tube body inlet 211 and a tube body outlet 212. The gas silicon source passes into the tube body 21 through the tube body inlet 211 to be heated and reacts in the tube body 21, and is discharged from the tube body outlet 212.

[0040] Single crystal silicon pulling furnace 4, used to pull and grow sing...

Embodiment 2

[0071] Such as figure 2 As shown, the difference between the pulling device for growing single crystal silicon in this embodiment and that in Embodiment 1 is that: the conveying mechanism in this embodiment includes a siphon 9, when the liquid level of molten silicon in the first crucible 3 is higher than The liquid level of the molten silicon in the second crucible 6, one end of the siphon tube 9 is positioned under the liquid level of the molten silicon in the first crucible 3, and the siphon tube 9 is used to siphon the molten silicon in the first crucible 3 into the second crucible 6 , The delivery mechanism also includes a valve 10 that is arranged on the siphon 9 and can be opened and closed.

[0072] It should be noted that the tubular reactor 2 in this embodiment is made of silicon carbide;

[0073] The inner wall of the tubular reactor 2 is coated with high-purity Si 3 N 4 .

[0074] This embodiment also provides a method for growing single crystal silicon using ...

Embodiment 3

[0084] This embodiment also provides a pulling method for growing single crystal silicon using the pulling device for growing single crystal silicon in embodiment 1. The difference between the method in this embodiment and the method in embodiment 1 is that:

[0085] The gaseous silicon source in this embodiment is dichlorodihydrosilane.

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Abstract

The invention discloses a pulling device and a pulling method for growing monocrystalline silicon. The device comprises: a first chamber, wherein a tubular reactor for heating and a first crucible arearranged in the first chamber, a gaseous silicon source undergoes a thermal decomposition reaction in the tubular reactor to generate silicon powder, and the silicon powder or molten silicon formed after melting the silicon powder enters the first crucible; a monocrystalline silicon pulling furnace used for pulling the molten silicon used as a raw material to grow the monocrystalline silicon; anda conveying mechanism respectively connected with the first chamber and the monocrystalline silicon pulling furnace, wherein the conveying mechanism is used for introducing the molten silicon in thefirst crucible of the first chamber into the monocrystalline silicon pulling furnace in order to make the molten silicon used as the raw material for the pulling growth of the monocrystalline siliconin the monocrystalline silicon pulling furnace. The device and the method for growing the monocrystalline silicon by using the gaseous silicon source as the raw material omit a step for producing a solid silicon material, so the energy consumption is reduced, and huge investment for producing and processing the solid silicon material is saved.

Description

technical field [0001] The invention belongs to the technical field of crystal silicon growth, and in particular relates to a pulling device and a pulling method for growing single crystal silicon. Background technique [0002] Crystalline silicon is an important raw material for silicon-based semiconductors and solar photovoltaic cells. At present, there are two main methods of growing crystalline silicon: one method is to place solid silicon material in an ingot furnace for ingot casting, and the product produced is polycrystalline silicon, which is mainly used for the manufacture of solar photovoltaic cells after slicing; The first method is to put solid silicon material in a single crystal furnace, and after melting, use the pulling method to grow single crystal silicon rods. Single crystal silicon wafers used in semiconductors and solar photovoltaic cells can be manufactured from single crystal silicon rods. In addition to the above two methods, there is also the zone ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C30B15/02C30B29/06
CPCC30B15/002C30B15/02C30B29/06
Inventor 银波范协诚夏高强王文胡颖宋高杰
Owner 新疆知信科技有限公司
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