Composite protection glass with excellent impact resistance
An impact resistance, protective glass technology, applied in glass/slag layered products, synthetic resin layered products, lamination and other directions, can solve the problems of limiting the application of protective slope glass, complex process, high cost, and achieve light weight, High optical clarity, outstanding weathering and aging resistance effects
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Embodiment 1
[0017] A composite protective glass with excellent impact resistance, in which modified polyurethane is added as an adhesive layer material in the middle of the composite protective glass, the preparation method comprising the following steps:
[0018] (1) Put the thermoplastic polyurethane film into absolute ethanol and deionized water for 15 minutes, and then dry it for later use. Mix the silane coupling agent KH550, absolute ethanol, and deionized water in a mass ratio of 1.2:85 : Mixed in a ratio of 3.0, stirred at room temperature for 30 minutes, heated to 45° C., and continued magnetic stirring for 1 hour to obtain a silane coupling agent hydrolyzate;
[0019] (2) Put the thermoplastic polyurethane film washed and dried in step (1) into the hydrolyzate of silane coupling agent, the mass ratio of the film to the hydrolyzate is 1:4.5. Ultrasonic treatment for 15 minutes and 10 minutes, the treated film was ultrasonically cleaned with deionized water for 20 minutes, and dri...
Embodiment 2
[0026] A composite protective glass with excellent impact resistance, in which modified polyurethane is added as an adhesive layer material in the middle of the composite protective glass, the preparation method comprising the following steps:
[0027] (1) Put the thermoplastic polyurethane film into absolute ethanol and deionized water for 18 minutes, and then dry it for later use. Mix the silane coupling agent KH550, absolute ethanol, and deionized water in a mass ratio of 1.25:88 : Mixed in a ratio of 3.3, stirred at room temperature for 35 minutes, heated to 48° C., and continued magnetic stirring for 1.5 hours to obtain a silane coupling agent hydrolyzate;
[0028] (2) Put the thermoplastic polyurethane film washed and dried in step (1) into the silane coupling agent hydrolyzate, the mass ratio of the film to the hydrolyzate is 1:4.8, at 23°C and 38°C, respectively Ultrasonic treatment for 18 minutes and 12 minutes, the treated film was ultrasonically cleaned with deioniz...
Embodiment 3
[0035] A composite protective glass with excellent impact resistance, in which modified polyurethane is added as an adhesive layer material in the middle of the composite protective glass, the preparation method comprising the following steps:
[0036] (1) Put the thermoplastic polyurethane film into absolute ethanol and deionized water for 20 minutes, and then dry it for later use. Mix the silane coupling agent KH550, absolute ethanol, and deionized water in a mass ratio of 1.3:90 : Mixed in a ratio of 3.5, stirred at room temperature for 40 minutes, heated to 50°C, and continued magnetic stirring for 2 hours to obtain a silane coupling agent hydrolyzate;
[0037] (2) Put the thermoplastic polyurethane film washed and dried in step (1) into the hydrolyzed solution of silane coupling agent, the mass ratio of the film to the hydrolyzed solution is 1:5.0, at 25°C and 40°C, respectively Ultrasonic treatment for 20 minutes and 15 minutes, the treated film was ultrasonically cleane...
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