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328results about How to "Good optical clarity" patented technology

Thermoplastic polyurethane block copolymer compositions

A novel block copolymer composition including a hydrogenated block copolymer that has at least one block A and at least one block B, and wherein (a) prior to hydrogenation each A block is a mono alkenyl arene homopolymer block and each B block is a controlled distribution copolymer block of at least one conjugated diene and at least one mono alkenyl arene, (b) subsequent to hydrogenation about 0-10% of the arene double bonds have been reduced, and at least about 90% of the conjugated diene double bonds have been reduced, (c) each A block having a number average molecular weight between about 3,000 and about 60,000 and each B block having a number average molecular weight between about 30,000 and about 300,000, (d) each B block comprises terminal regions adjacent to the A blocks that are rich in conjugated diene units and one or more regions not adjacent to the A blocks that are rich in mono alkenyl arene units, (e) the total amount of mono alkenyl arene in the hydrogenated block copolymer is about 5 percent weight to about 50 percent weight, and (f) the weight percent of mono alkenyl arene in each B block is between about 10 percent and about 75 percent. The thermoplastic polyurethane elastomer is present in the block copolymer in an amount from about 50 to about 95 percent by weight of a thermoplastic polyurethane elastomer.
Owner:KRATON POLYMERS US LLC

Composite flexible surface enhanced Raman substrate based on silver nanoparticles and preparation method of substrate

The invention provides a composite flexible surface enhanced Raman substrate based on silver nanoparticles and a preparation method of the substrate. According to the method, first, a chemical reduction method is utilized to prepare a silver colloid containing a large quantity of silver nanoparticles (AgNPs); second, the silver colloid is mixed with polydimethylsiloxane (PDMS) diluted with methylbenzene to form a suspension, the suspension is dropwise added onto the surface of a hard baseboard, and a PDMS thin film containing a large quantity of silver nanoparticles is formed through heat curing and is peeled off; and last, an impregnation method is used to transfer a layer of silver nanoparticles on the prepared thin film, and the composite flexible surface enhanced Raman substrate basedon silver nanoparticles is prepared. An experiment indicates that by use of the surface enhanced Raman scattering substrate prepared through the method, high-sensitivity SERS detection can be realized, and Raman signals are uniform; and meanwhile, the substrate has good mechanical stability and flexibility, and SERS signals are not attenuated but even substantially enhanced under large-range tensile strain. The method is convenient and fast to use and low in cost, and large-area repetitive preparation can be realized.
Owner:SHANDONG NORMAL UNIV

Unsymmetrical fragrant diamine containing fluorine, preparation and application in synthesizing polyimide thereof

The present invention relates to fluorine-containing asymmetric aromatic diamine, a preparation method and an application thereof in the synthesis of polyimide. The compound has a constitutional formula as shown in the right. The preparation method comprises the following steps: (1) 2, 6-dimethyl phenol, paranitrobensoyl chloride and alchlor have catalytic reaction in an organic solvent to prepare (4'-hydroxy-3', 5'-dimethyl benzene)-(4-nitrophenyl) ketone; (2) the (4'-hydroxy-3', 5'-dimethyl benzene)-(4-nitrophenyl) ketone reacts with 2-chlorine-5-nitro trifluorotoluene with alkaline, to prepare (3', 5'-dimethyl-4'-(4''-nitro-2''-trifluoromethyl phenoxy) benzene)-(4-nitrophenyl) ketone; (3) the prepared product in the second step is reduced by reducing agent with organic solvents and catalysts; thus the fluorine-containing asymmetric aromatic diamine can be prepared. The fluorine-containing asymmetric aromatic diamine can be used for preparing fluorine-containing polyimide. The fluorine-containing asymmetric aromatic diamine prepared in the method has high purity and can keep stable at the room temperature; the polyimide made of the fluorine-containing asymmetric aromatic diamine has excellent solubility, film forming capability, optical transparency, mechanical properties and heat resistance.
Owner:DONGHUA UNIV

Intelligent window and manufacturing method thereof

The invention relates to the technical field of windows, and provides a manufacturing method for manufacturing an intelligent window. The method includes the steps that dyeing, stretching and color complementing are conducted on a first polyvinyl alcohol film, and the upper surface and the lower surface of the first polyvinyl alcohol film are covered by first triacetyl cellulose membranes to be dried; dyeing, stretching and color complementing are conducted on a second polyvinyl alcohol film, the upper surface and the lower surface of the polyvinyl alcohol film are covered by a third triacetyl cellulose membrane and a second triacetyl cellulose membrane to be dried, the second triacetyl cellulose membrane is coated with a pressure-sensitive adhesive layer, and then thermocuring and spontaneous curing are conducted; first glass, a first polaroid, a liquid crystal coating, a second polaroid and second glass are sequentially stacked. The invention further provides the intelligent window. The intelligent window comprises the first glass, the first polaroid, the liquid crystal coating, the second polaroid and the second glass. The first polaroid comprises the first polyvinyl alcohol film and the first triacetyl cellulose membrane. The second polaroid comprises the pressure-sensitive adhesive layer, the second triacetyl cellulose membrane, the second polyvinyl alcohol film and the third triacetyl cellulose membrane.
Owner:SHENZHEN SUNNYPOL OPTOELECTRONICS

Transparent biodegradable polylactic acid nano composite material and preparation thereof

The invention relates to transparent biodegradable polylactic acid nano composite material and a preparation method thereof. The nano composite material comprises the following components: polylactic acid, nano silicon dioxide, a plasticizer, an antioxidant and a lubricant. The preparation method comprises the following steps: premixing; milling or extruding granulation; and hot-press forming. The nano composite material is fully biodegradable; compared with pure polylactic acid, the nano composite material has obviously improved thermal stability; and the initial thermal decomposition temperature is maximally improved by 34.79 DEG C, and the highest thermal decomposition temperature is maximally improved by 31.35 DEG C. The nano composite material has good penetrability; and the visible light transmission rate of the material is between 85 and 89, and the haze value of the material is from 3.8 to 4.7. The nano composite material also has an excellent processability; the material has the following adjustable mechanical properties: a tensile strength between 32.6 and 70.4MPa, the stretch modulus between 0.80 and 2.36GPa, and breaking elongation rate between 6.2 and 280. The nano composite material is widely applied in the fields of agricultural use products, food package, daily articles, and the like.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Microfluidic-control preparation method for microsphere of polymethylmethacrylate-coated cadmium telluride (CdTe) quantum dot

InactiveCN102504822AUniform shapeConsistent and uniform sizeLuminescent compositionsInjectorQuantum dot
The invention relates to a microfluidic-control preparation method for a microsphere of a polymethylmethacrylate-coated cadmium telluride (CdTe) quantum dot, and relates to a preparation method for the microsphere of a polymethylmethacrylate-coated CdTe quantum dot. The microfluidic-control preparation method for the microsphere of the polymethylmethacrylate-coated (CdTe) quantum dot aims to solve the problems that the surface of the quantum dot needs to be modified and the quantum dot is easy to dissolve by the microsphere of the polymethylmethacrylate-coated CdTe quantum dot by adopting a traditional preparation method for the microsphere of the polymethylmethacrylate-coated CdTe quantum dot. The method comprises the following steps: preparing a sodium hydrogen telluride solution; preparing a CdTe quantum dot; preparing a polymer solution; connecting a microfluidic-control system; respectively putting the polymer solution and silicone oil into injectors A and B of the microfluidic-control system; setting the propulsion speed of the injectors A and B; after starting, formed liquid beads flow into a rotary evaporator; and curing and evaporating the silicone oil to obtain the microsphere of the polymethylmethacrylate-coated CdTe quantum dot. In the microfluidic-control preparation method for the polymethylmethacrylate-coated CdTe quantum dot, the polymethylmethacrylate-coated CdTe quantum dot is selected, therefore, fluorescence is stable, and the microsphere can be adjusted in size and can be used for field of fluorescent display and the like.
Owner:HEILONGJIANG UNIV

Modified no-rainbow organic silicon release film taking biaxially oriented poly benzoic acid gylcol ester film and preparation method thereof

The invention discloses a modified no-rainbow organic silicon release film taking biaxially oriented poly benzoic acid gylcol ester film and a preparation method thereof, relating to an organic silicon release film and a preparation method thereof. By using modified no-rainbow organic silicon release film, the problems of low organic silicon release film surface tension and poor organic solvent resistant performance can be solved. The release film is prepared from a base material and coating liquid, wherein the coating liquid is prepared from acrylic acid, butyl acrylate, methyl methacrylate, styrene, vinyl dimethyl siloxane prepolymer, epoxy resin E-44, benzoyl peroxide and toluene. The method comprises the following steps: adding parts of acrylic acid, butyl acrylate, methyl methacrylate, styrene and toluene and whole vinyl dimethyl siloxane prepolymer into a reactor; carrying out a reaction in two steps to obtain emulsion; preparing into coating liquid; coating onto the biaxially oriented poly benzoic acid gylcol ester film; and drying to obtain the modified no-rainbow organic silicon release film. The surface tension of the release film is 29-31mN / m, stripping resistance is 19-24g / cm, and the modified no-rainbow organic silicon release film can be used for the field of optical products.
Owner:HARBIN INST OF TECH

Method for preparing polycrystalline doping molybdenum zinc oxide transparent conductive film

The invention belongs to the transparent conductive film technical field, in particular to a preparation method of a polycrystalline molybdenum doped zinc oxide transparent conductive film. The steps of the method are that: a zinc inlay molybdenum target is taken as a target and ordinary glass is taken as substrate, the substrate temperature is 100-300 DEG C, through a reactive dc magnetron sputtering method, an Ar ion beam bombards and sputters the target, the sputtering current is 150-300mA, the sputtering voltage is 100-400 V, the work pressure of a reaction chamber is 0.45-2.5 Pa, the percentage of the parcial pressure P (O 2 ) = Po 2 / (Po 2 +P Ar ) of the reactive gas O 2 is 4.0 to 10.0%, the sputtering time is 40-100 minutes, thus forming the molybdenum-doped zinc oxide transparent conductive film with a polycrystalline structure. The film thickness is 100-250 nm. The film prepared by the invention is characterized by low resistivity, high visible light range of optical transparency and high carrier mobility. The invention has industrial production prospect and has good technological stability. The invention is a novel method in the preparation of ZMO transparent conductive oxide films and the guarantee of excellent quality of parts produced by films.
Owner:FUDAN UNIV
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