Preparation method and application of three-dimensional spherical scorodite crystal
A scorodite and spherical technology, which is applied in the field of preparation of three-dimensional spherical scorodite crystals, can solve the problem that the arsenic removal effect needs to be further improved, and achieve the effects of good application potential, efficient removal, and reduction of wastewater treatment costs.
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[0034] Example 1
[0035] This embodiment provides a method for preparing three-dimensional spherical scorodite crystals, including: weighing ferric nitrate and sodium arsenate solids, and using deionized water and concentrated nitric acid to prepare a mixed solution, the iron concentration and arsenic concentration are both 0.15 mol / L, the concentration of concentrated nitric acid is 0.12mol / L, and the pH of the mixed solution is 1.43. The mixed solution is placed in a 50mL autoclave and placed in an oven at 200°C for 12 hours to react. The reacted solution is natural After cooling to room temperature, it was separated by suction filtration, and the filter residue was washed with deionized water and dried at 60° C. to obtain a solid sample.
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[0036] Example 2
[0037] This embodiment provides a method for preparing three-dimensional spherical scorodite crystals. The difference from Embodiment 1 is that the concentration of nitric acid added is 0.15 mol / L, and the pH of the mixed solution is 1.33.
Example Embodiment
[0038] Example 3
[0039] This embodiment provides a method for preparing three-dimensional spherical scorodite crystals. The difference from Embodiment 1 is that the concentration of nitric acid added is 0.18 mol / L, and the pH of the mixed solution is 1.20.
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