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Semisynthetic gasoline engine oil and preparation method thereof

A gasoline engine oil, semi-synthetic technology, applied in the field of lubricating oil, can solve the problems of difficult dispersion of nanoparticles, affecting the quality of gasoline engine oil, and failing to achieve expected results, so as to improve quality and service life, improve anti-oxidation performance, reduce bubble effect

Inactive Publication Date: 2018-09-04
金诺斯(北京)石油化工制品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Nanoparticles are often added to gasoline engine oil as a friction modifier. Nanoparticles will fill and repair the worn metal surface on the surface of the friction pair, and form a lubricating film, which can effectively reduce the wear loss of the engine. In addition, due to the accumulation of gas in the pores of the nanoparticles, when the nanoparticles and gasoline engine oil are mixed, the gas accumulated in the pores overflows, forming a large number of fine bubbles, which affects the quality of gasoline engine oil

Method used

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  • Semisynthetic gasoline engine oil and preparation method thereof
  • Semisynthetic gasoline engine oil and preparation method thereof
  • Semisynthetic gasoline engine oil and preparation method thereof

Examples

Experimental program
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Embodiment 1

[0029] Preparation of molybdenum dialkyldithiocarbamate: add 30Kg carbon disulfide and 30Kg molybdenum trioxide successively in the reactor, stir vigorously, and add 65Kg di-n-undecylamine drop by drop, control the temperature at 45°C, After the addition of n-undecylamine was completed, the vigorous stirring was continued for 9 hours, and then cooled, washed with water, extracted, dried, and distilled under reduced pressure to obtain molybdenum dialkyldithiocarbamate.

[0030] Preparation of composite functional additives: Add 35Kg molybdenum dialkyl dithiocarbamate, 10Kg sodium dibenzyl dithiocarbamate, and 18Kg polyisobutenyl succinimide in sequence in the mixing kettle, heat up to 50°C, and stir for 20 minutes , followed by adding 6.1Kg nanometer molybdenum disulfide, 0.92Kg calcium phytate, 22Kg trimethylhydroxypentyl isobutyrate and 3.5Kg butylated hydroxyethylbenzene, continue to stir for 30 minutes, stand still for 5 minutes, filter and cool , to obtain composite functi...

Embodiment 2

[0036] The difference between embodiment 2 and embodiment 1 is that the method for preparing molybdenum dialkyldithiocarbamate is different;

[0037] Preparation of molybdenum dialkyldithiocarbamate: Add 30Kg carbon disulfide and 30Kg molybdenum trioxide in sequence in the reactor, stir vigorously, and add 31.5Kg di-tert-amylamine drop by drop, control the temperature at 45°C, After the pentylamine was added dropwise, the vigorous stirring was continued for 8.5 hours, and then cooled, washed with water, extracted, dried, and distilled under reduced pressure to obtain molybdenum dialkyldithiocarbamate.

Embodiment 3

[0039] The difference between embodiment 3 and embodiment 1 is that the method for preparing molybdenum dialkyldithiocarbamate is different;

[0040] Preparation of molybdenum dialkyldithiocarbamate: Add 30Kg carbon disulfide and 30Kg molybdenum trioxide in sequence in the reactor, stir vigorously, and add 53.4Kg di-n-nonylamine drop by drop, control the temperature at 45°C, and After the nonylamine was added dropwise, the vigorous stirring was continued for 8 hours, and then cooled, washed with water, extracted, dried, and distilled under reduced pressure to obtain molybdenum dialkyldithiocarbamate.

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Abstract

The invention relates to semisynthetic gasoline engine oil and a preparation method thereof, and belongs to the technical field of lubricating oil. The semisynthetic gasoline engine oil comprises thefollowing raw materials: mineral base oil HVI150, mineral base oil HVI500, poly alpha-olefin synthetic base oil, a viscosity index improver, a composite function additive, a pour point reducer and a defoaming agent, wherein the composite function additive comprises molybdenum dialkyldithiocarbamate, nanometer molybdenum disulfide, dibenzyldithiocarbamic acid sodium salt, polyisobutylene succinimide, calcium phytic acid, trimethyl hydroxypentyl isobutyrate and butylated hydroxyethyl benzene; the semisynthetic gasoline engine oil is prepared and obtained according to the method comprising the steps of mixing, stirring, program warming, and program cooling in sequence. According to the semisynthetic gasoline engine oil, the dispersibility of nanometer molybdenum dioxide is improved, bubbles inside the nanometer molybdenum dioxide are reduced, and the semisynthetic gasoline engine oil has good functions of lubrication, abrasion resistance, oxidation resistance, defoaming, energy conservation and emission reduction.

Description

technical field [0001] The invention relates to the technical field of lubricating oil, in particular to a semi-synthetic gasoline engine oil and a preparation method thereof. Background technique [0002] In the current development of the automobile industry, there are many metal surfaces in the engine that rub against each other. Especially for new cars leaving the factory or after engine overhaul of old cars, the fit gaps of various parts are uneven or too tight, and running-in adjustment is required. As a kind of lubricating oil, gasoline engine oil plays an increasingly important role in reducing friction in the engine. Nanoparticles are often added to gasoline engine oil as a friction modifier. Nanoparticles will fill and repair the worn metal surface on the surface of the friction pair, and form a lubricating film, which can effectively reduce the wear loss of the engine. In addition, due to the accumulation of gas in the pores of the nanoparticles, when the nanopar...

Claims

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Application Information

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IPC IPC(8): C10M169/04C10M177/00C10N30/04C10N30/06C10N30/10C10N30/18C10N40/25
CPCC10M169/044C10M177/00C10M2201/062C10M2201/066C10M2201/105C10M2203/1006C10M2205/0206C10M2205/022C10M2205/024C10M2205/026C10M2205/04C10M2205/06C10M2207/021C10M2207/046C10M2207/281C10M2209/062C10M2209/084C10M2209/086C10M2215/28C10M2219/068C10M2223/042C10M2227/00C10N2030/04C10N2030/06C10N2030/10C10N2030/18C10N2030/54C10N2030/64C10N2040/255C10N2010/12C10N2010/02
Inventor 王英奎王文博王广宇
Owner 金诺斯(北京)石油化工制品有限公司