Rare earth permanent magnet and preparation method thereof

A rare earth permanent magnet and magnet technology, which is applied in the fields of magnetic objects, inductance/transformer/magnet manufacturing, magnetic materials, etc., can solve the problem that the diffusion amount of heavy rare earth elements is difficult to control, and achieve the effect of simple process and easy industrialization.

Active Publication Date: 2018-10-09
NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method only diffuses a small amount of heavy rare earth elements, and it is difficult to diffuse more heavy rare earth elements into the interior of the magnet
In other words, this method is limited by the thickness of the magnet. When the thickness of the magnet is larger, the proportion of heavy rare earth elements diffused into the magnet decreases, and the diffusion amount of heavy rare earth elements is not easy to control

Method used

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  • Rare earth permanent magnet and preparation method thereof
  • Rare earth permanent magnet and preparation method thereof
  • Rare earth permanent magnet and preparation method thereof

Examples

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preparation example Construction

[0029] The invention provides a preparation method of a rare earth permanent magnet. This preparation method comprises the following steps:

[0030] S1, provide a first magnetic powder and a second magnetic powder respectively, wherein the first magnetic powder is alloy magnetic powder B, the second magnetic powder is alloy magnetic powder R or mixed magnetic powder A, and the mixed magnetic powder A is obtained by mixing alloy magnetic powder B and alloy powder, so The coercive force of the magnet prepared by the second magnetic powder is higher than that of the magnet prepared by the first magnetic powder;

[0031] S2, placing the first magnetic powder in the middle part of a mould, placing the second magnetic powder in the upper part and the lower part of the mould, and performing thermocompression molding to obtain a thermocompressed magnet;

[0032] S3, performing thermal deformation molding on the hot-pressed magnet to obtain a rare earth permanent magnet, the rare eart...

Embodiment 1

[0053] According to neodymium copper alloy (Nd 70 Cu 30 , at%) in the proportion of neodymium and copper elements in precise batching, and made ingots in a vacuum induction melting furnace, using a rapid quenching furnace to make it into a rapid quenching thin strip, and then mechanically crushed to make a particle size of about 200μm neodymium copper alloy powder.

[0054] The neodymium-copper alloy powder and the composition are Nd 29.8 PR 0.4 Ga 0.5 Fe bal. co 4 B 0.93 The NdFeB master alloy magnetic powder is evenly mixed to obtain the mixed magnetic powder, wherein the neodymium-copper alloy powder accounts for 4% of the total mass of the mixed magnetic powder.

[0055] Put the mixed magnetic powder and NdFeB master alloy magnetic powder into the first mold for hot pressing, wherein the mixed magnetic powder is placed in the upper and lower parts of the first mold, and the NdFeB master alloy magnetic powder is placed in the middle part of the first mold. The mass ...

Embodiment 2

[0059] This preparation method is basically the same as that of Example 1, except that the mass ratio of the mixed magnetic powder to the NdFeB master alloy magnetic powder is 1:3 during hot pressing, the highest temperature of hot pressing is 670°C, and the highest temperature of hot deformation It is 830°C.

[0060] The magnetic properties of the obtained rare earth permanent magnet were tested at room temperature, and the test results are shown in Table 1.

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Abstract

The invention relates to a preparation method of a rare earth permanent magnet. The preparation method comprises the following steps of (1) providing first magnetic powder and second magnetic powder separately, wherein the first magnetic powder is alloy magnetic powder B; the second magnetic powder is alloy magnetic powder R or mixed magnetic powder A; the mixed magnetic powder A is obtained by mixing of the alloy magnetic powder B and alloy powder; the coercivity of a magnet prepared from the second magnetic powder is higher than that of a magnet prepared from the first magnetic powder; (2) putting the first magnetic powder in the middle part of a die, putting the second magnetic powder into the upper part and the lower part of the die, and performing hot press molding to obtain a hot pressed magnet; and (3) performing thermal deformation molding on the hot pressed magnet to obtain the rare earth permanent magnet, wherein the rare earth permanent magnet comprises a middle layer formedby the first magnetic powder and an upper layer and a lower layer formed by the second magnetic powder; and in addition, a transition layer is formed between the middle layer and the upper layer, andbetween the middle layer and the lower layer separately. The invention also relates to a rare earth permanent magnet body.

Description

technical field [0001] The invention belongs to the technical field of rare earth permanent magnet materials, and relates to a rare earth permanent magnet and a preparation method thereof. Background technique [0002] In recent years, rare earth permanent magnets have been used in various industries, especially in clean energy such as wind power generation, energy-saving appliances, and electric vehicles. The output and consumption of rare earth permanent magnets are increasing year by year. With the expansion of the application range, rare earth permanent magnets are required to have high performance and high temperature resistance, and at the same time, rare earth permanent magnets are required to be used in relatively high temperature environments. [0003] The most common way to improve the high temperature resistance of rare earth permanent magnets is to increase the coercive force of the magnets. There are many ways to increase the coercive force of the magnet. For e...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01F1/057H01F41/02C22C38/06C22C38/10C22C38/16
CPCC22C38/002C22C38/005C22C38/06C22C38/10C22C38/16H01F1/0576H01F41/0266H01F41/0293
Inventor 剧锦云陈仁杰靳朝相唐旭尹文宗李东闫阿儒
Owner NINGBO INST OF MATERIALS TECH & ENG CHINESE ACADEMY OF SCI
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