Ferrite stainless steel grain refiner, preparation method and application thereof
A grain refiner, stainless steel technology, applied in the field of grain refinement of metal materials, can solve the problems of unsatisfactory use requirements, easy cracking, complicated preparation process, etc., to solve the problem of cracking in forging and rolling process, refine The effect of ferritic stainless steel grains and simple preparation process
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[0043] Example 1
[0044] A method for refining the as-cast structure of ferritic stainless steel is as follows:
[0045] (1) Ingredients
[0046] Fe powder and large-grain TiN powder are used as raw materials, and the mass fraction of TiN powder is 0.01%. The particle size of the large-grain TiN powder used is between 4 and 5 μm.
[0047] (2) Preparation of Fe-TiN block
[0048] The prepared raw materials are ground and mixed in a planetary ball mill, and the mixing time is 2.5h. It should be noted that the ratio of raw materials to the volume of the mill tank does not exceed 2 / 3.
[0049] The particle size of the TiN powder after ball milling is less than 2μm. The ball milled powder is hot pressed into a block in a mold, the hot pressing pressure is 27MPa, the hot pressing temperature is 1352°C, and the holding time is 6min. After cooling, it is taken out to obtain the Fe-TiN block.
[0050] (3), smelting
[0051] The ferritic stainless steel is smelted in a low-carbon steel crucible us...
Example Embodiment
[0052] Example 2
[0053] A method for refining the as-cast structure of ferritic stainless steel is as follows:
[0054] (1) Ingredients
[0055] Fe powder and large-particle TiN powder are used as raw materials, and the mass fraction of TiN powder is 0.02%.
[0056] (2) Preparation of Fe-TiN block
[0057] The prepared raw materials are ground and mixed in a planetary ball mill, and the mixing time is 3h. The particle size of the ball-milled TiN powder is less than 2μm. The ball-milled powder is hot-pressed into a block in a mold. The hot-pressing pressure is 25MPa, the hot-pressing temperature is 1374°C, and the holding time is 8min. After cooling, take it out to obtain Fe-TiN block.
[0058] (3), smelting
[0059] The ferritic stainless steel is smelted in a low-carbon steel crucible using a resistance furnace; after the ferritic stainless steel is melted, pressed into the Fe-TiN block prepared above, where the Fe-TiN block is based on TiN as the total mass of the ferritic stainless ...
Example Embodiment
[0060] Example 3
[0061] A method for refining the as-cast structure of ferritic stainless steel is as follows:
[0062] (1) Ingredients
[0063] Fe powder and large-grain TiN powder are used as raw materials, and the mass fraction of TiN powder is 0.03%.
[0064] (2) Preparation of Fe-TiN block
[0065] The prepared raw materials are ground and mixed in a planetary ball mill, and the mixing time is 3.5h. The particle size of the TiN powder after ball milling is less than 2μm. The ball milled powder is hot pressed into a block in a mold, the hot pressing pressure is 28MPa, the hot pressing temperature is 1365°C, and the holding time is 8min. After cooling, it is taken out to obtain Fe-TiN block.
[0066] (3), smelting
[0067] The ferritic stainless steel is smelted in a low-carbon steel crucible using a resistance furnace; after the ferritic stainless steel is melted, pressed into the Fe-TiN block prepared above, where the Fe-TiN block is based on TiN as the total mass of the ferritic ...
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