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Safe type civil propellant and preparation method thereof

A propellant and safe technology, which is applied in the field of safe civil propellant and its preparation, can solve the problems of complex manufacturing method and large dust, and achieve good fracturing effect, good safety performance and low content of corrosive gas components Effect

Inactive Publication Date: 2018-11-06
HUBEI INST OF AEROSPACE CHEMOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The manufacturing methods of most existing civil propellants are relatively complicated, and the binders in most formulations need to be dissolved with solvents, and then undergo the process of pharmaceutical preparation, granulation, drying, and tabletting; some are prepared by dry mixing Powdered civil propellant with large dust

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A kind of safe civilian propellant, its formulation composition (by mass percentage) is as follows: coating agent: HTPB, 2%, DOA, 2%; Oxidant: KP, 58%; Fuel: GN: 32%, ADC, 5% %; Combustion catalyst: CuO, 1%, d 50 = 2 μm.

[0034] Its preparation method is as follows:

[0035] (1) Weigh according to the formula ratio, then add HTPB, DOA, GN, and ADC to a vertical mixer for mixing, the mixing temperature is 50°C, and the mixing time is 15 minutes;

[0036] (2) Add 1 / 2 of the oxidant KP and 1 / 2CuO into the vertical mixer, mix for 10 minutes, and then obtain the powder;

[0037] (3) Add the medicinal powder of (2) together with the remaining KP and CuO into a three-dimensional motion mixer and mix for 10 minutes. After the mixing is completed, the propellant is obtained by discharging.

[0038] The gas production rate of the obtained propellant is 2.87mol / 100g, and the detonation heat is 4512J / g; the content of CO is 0mol / 100g, the content of NO is 0.02mol / 100g, and the...

Embodiment 2

[0040] A safe civil propellant, its formulation composition (calculated by mass percentage) is as follows: coating agent: HTPB, 2.5%, TA, 2.5%; Oxidant: KP, 49%, AN, 5%; Fuel: DHG, 40% %; Combustion catalyst: CuO, 1%, d 50 = 2 μm.

[0041] Its preparation method is as follows:

[0042] (1) Weighing according to the formula ratio;

[0043] (2) Then add HTPB, TA, and DHG to the first-stage feed port of the screw mixer, AN from the second-stage feed port, and KP and CuO from the third-stage feed port for mixing; mix for 20 minutes to obtain a propellant.

[0044] The gas yield of the obtained propellant is 3.06mol / 100g; the detonation heat is 4486J / g; the content of CO is 0mol / 100g, the content of NO is 0.019mol / 100g, and the content of NO 2 The content is 0mol / 100g. According to GJB6195-2008 "Composite Solid Propellant Hazard Classification Method", the hazard level of this civil propellant belongs to 1.3.

Embodiment 3

[0046] A safe civil propellant, its formula composition (calculated by mass percentage) is as follows: coating agent: HTPB, 2%, DOS, 2%; Oxidant: KP, 45%, AP, 2%, AN, 13%; Fuel: GN: 26%, Melamine: 9%; Combustion catalyst: Fe 2 o 3 , 1%, d50 = 2.2 μm.

[0047] Its preparation method is as follows:

[0048] (1) Weigh according to the formula ratio, then add HTPB, DOS, GN, and melamine into the vertical mixer for mixing, the mixing temperature is 50°C, and the mixing time is 10 minutes;

[0049] (2) Add the auxiliary oxidants AN and AP into the mixer and mix for 10 minutes;

[0050] (3) 1 / 4 of the main oxidant KP, 1 / 2Fe 2 o 3 Add it into the mixer and mix for 12 minutes; then get the powder;

[0051] (4) mix the powder of (3) with the remaining KP, Fe 2 o 3 Add them together into a three-dimensional motion mixer and mix for 10 minutes. After the mixing is completed, the propellant is obtained by discharging.

[0052] The gas yield of the obtained propellant is 2.94mol / 1...

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Abstract

A safe type civil propellant is prepared from, by mass, 2%-8% of coating agent, 40%-60% of main oxidizing agent, 0%-25% of auxiliary oxidant, 25%-40% of fuel and 1%-2% of combustion catalyst, whereinthe coating agent contains liquid rubber and grease. The friction sensitivity and impact sensitivity of the propellant are 0, and the electrostatic spark sensitivity is greater than 120 mJ, excluding1.1-level explosive materials, the danger level is 1.3 level, and because that no metal powder is contained in a formula, and reaction products do not likely ignite oil, gas and coal bed methane and are safe and reliable. The explosion heat of the civil propellant is greater than 4400 J / g, and the gas production is greater than 2.8 mol / 100g, can be ignited by electric ignition heads, electric igniters and other civil pyrotechnic equipment, the gases generated by the reaction are mainly nitrogen, carbon dioxide and water steam, the content of CO and nitrogen oxide is very low, and the safe typecivil propellant can be used for oil and shale gas mining and coal mine fracturing.

Description

technical field [0001] The present invention generally relates to the technical field of composite propellants, in particular to a safe civil propellant and a preparation method thereof. Background technique [0002] Fracturing technology refers to pressurizing gas, liquid, gas-liquid mixed foam and other working fluids through explosive explosion, propellant deflagration, mechanical pressurization, etc., and acting on oil, shale gas and other resource reservoirs to make the reservoir Create cracks to increase and unblock the seepage channels of liquid and gaseous resources, communicate with different reservoirs, facilitate the later mechanical mining of solid mineral resources, and finally achieve the purpose of increasing production. [0003] Commonly used fracturing methods mainly include hydraulic fracturing (WPF), explosive fracturing (EF) and high energy gas fracturing (HEGF). Hydraulic pressure can generally produce a single crack, and the maximum length of the crack...

Claims

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Application Information

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IPC IPC(8): C06B29/16C06B31/32C06D5/06
CPCC06B29/16C06B31/32C06D5/06
Inventor 熊伟强李忠友庞爱民鲁锐华李彦荣朱雯娟王鹏赵新岩高扬
Owner HUBEI INST OF AEROSPACE CHEMOTECH
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