A method for efficiently extracting vanadium from vanadium-containing ores
An ore and high-efficiency technology, applied in the field of rare metal extraction, can solve the problems of complex production process, increased production cost and high production cost, and achieve the effects of simple production process, low production cost and improved yield
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Embodiment 1
[0027] A method for efficiently extracting vanadium from vanadium-containing ores, specifically comprising the following steps:
[0028] (1) Pretreatment: First crush the vanadium-containing stone coal to a particle size of less than 1 cm, then add it to a ball mill, and then add 20% sulfuric acid solution to the ball mill according to the solid-to-liquid mass ratio of 1:1 for ball milling. Obtain an acidic mixed material with a particle size of less than 0.15mm;
[0029] (2) Leaching: Add potassium permanganate to the above-mentioned acidic mixture according to the mass ratio of 50:2, then react at 60°C for 5 hours, and obtain a vanadium-containing leaching solution through filtration and separation;
[0030] (3) Ion exchange: use a strong basic macroporous anion exchange resin to adsorb the vanadium-containing leaching solution, and then use a mixed solution composed of 8% NaOH and 4% NaCl to desorb, and prepare Obtain vanadium-containing eluent;
[0031] (4) Precipitation...
Embodiment 2
[0034] A method for efficiently extracting vanadium from vanadium-containing ores, specifically comprising the following steps:
[0035] (1) Pretreatment: First crush the vanadium-containing stone coal to a particle size of less than 1 cm, then add it to a ball mill, and then add 30% sulfuric acid solution to the ball mill according to the solid-to-liquid mass ratio of 1:1.2 for ball milling. Obtain an acidic mixed material with a particle size of less than 0.15mm;
[0036] (2) Leaching: Add potassium permanganate to the above-mentioned acidic mixture according to the mass ratio of 50:1, then react at 85°C for 2 hours, and prepare a vanadium-containing leaching solution through filtration and separation;
[0037] (3) Ion exchange: use a strong basic macroporous anion exchange resin to adsorb the vanadium-containing leaching solution, and then use a mixed solution composed of 9% NaOH and 4.5% NaCl by mass percentage to desorb, and prepare Vanadium-containing eluent;
[0038] ...
Embodiment 3
[0041] A method for efficiently extracting vanadium from vanadium-containing ores, specifically comprising the following steps:
[0042] (1) Pretreatment: first crush the vanadium-containing clay ore to a particle size of less than 1cm, then add it to a ball mill, and then add a sulfuric acid solution with a mass percentage of 28% to the ball mill according to the solid-to-liquid mass ratio of 1:1.3 for ball milling. Obtain an acidic mixed material with a particle size of less than 0.15mm;
[0043] (2) Leaching: add hydrogen peroxide to the above-mentioned acidic mixture according to the mass ratio of 50:2.4, then react at 68°C for 4 hours, and obtain a vanadium-containing leaching solution through filtration and separation;
[0044] (3) Ion exchange: use a strong basic macroporous anion exchange resin to adsorb the vanadium-containing leaching solution, and then use a mixed solution composed of 9% NaOH and 4.5% NaCl by mass percentage to desorb, and prepare Vanadium-containing...
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