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Salt-storage sustained-release snow-melt deicer and preparation method thereof

A slow-release, deicing agent technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of long release time and limited release of deicing agents, achieve large amount of ice melting, simple preparation process, and easy raw materials The effect

Active Publication Date: 2018-12-07
CHONGQING JIAOTONG UNIVERSITY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In view of the above-mentioned deficiencies in the prior art, the object of the present invention is to provide a salt-storage slow-release snow-melting and de-icing agent that is not limited by temperature-controlled molecules, has a long release time, and improves the amount of ice-melting and its preparation method, which solves the problem of The problem that the release of existing deicing agents is limited by temperature-controlled molecules

Method used

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  • Salt-storage sustained-release snow-melt deicer and preparation method thereof
  • Salt-storage sustained-release snow-melt deicer and preparation method thereof

Examples

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Comparison scheme
Effect test

Embodiment 1

[0026] A salt-storage slow-release snowmelting and deicing agent, comprising the following ingredients: 128g of slow-release inorganic salts, 33g of isopropanol and 40g of polymer monomers in the encapsulating polymer; Calcium chloride saturated solution 120g, 8g diatomaceous earth, 0.8g nano silicon dioxide, 3.8g OP-10 and 180mL absolute ethanol; the encapsulation polymer includes 1g acrylic acid, 18g methyl acrylate, 14g butyl acrylate, 7g styrene , 1gKH570, 0.8gAIBN, 2g isopropanol, 2g triethylamine and 5g water.

[0027] The preparation method of the salt-storage slow-release snow melting and deicing agent comprises the following steps:

[0028] (1) prepare 120g antifreezing calcium chloride saturated solution;

[0029] (2) Dissolve 8g of diatomite, 0.8g of nano-silica, and 3.8g of OP-10 in a flask previously filled with 180mL of absolute ethanol, and place the flask in a 60°C water bath with a polytetrafluoroethylene stirring rod Stir evenly to obtain a diatomite suspen...

Embodiment 2

[0034]A salt-storage slow-release snow-melting and deicing agent, comprising the following ingredients: 175g of slow-release inorganic salts, 65g of propylene glycol methyl ether and 50g of polymer monomers in the encapsulating polymer; Sodium chloride saturated solution 136g, 10g diatomaceous earth, 1.2g nano silicon dioxide, 4.3gOP-10 and 220mL absolute ethanol; The said wrapping polymer comprises 1.5g acrylic acid, 22g methyl acrylate, 18g butyl acrylate, 8.5g Styrene, 2g KH570, 1.3g AIBN, 65g propylene glycol methyl ether, 3g triethylamine and 10g water.

[0035] The preparation method of the salt-storage slow-release snow melting and deicing agent comprises the following steps:

[0036] (1) prepare 136g antifreezing sodium chloride saturated solution;

[0037] (2) Dissolve 10g of diatomite, 1.2g of nano-silica, and 4.3g of OP-10 in a flask previously filled with 220mL of absolute ethanol, and place the flask in a 60°C water bath with a Teflon stirring rod Stir evenly to...

Embodiment 3

[0042] A salt-storage slow-release snowmelting and deicing agent, comprising the following ingredients: 158.2g of slow-release inorganic salts, 45.2g of isopropanol and 45.2g of polymer monomers in the encapsulating polymer; the slow-release inorganic salts include anti- 110g of frozen magnesium chloride saturated solution, 9g of diatomaceous earth, 1g of nano-silica, 4g of OP-13 and 200mL of absolute ethanol; , 1.5g KH570, 0.9g AIBN, 2.5g isopropanol, 2.5g triethylamine and 7.5g water.

[0043] The preparation method of the salt-storage slow-release snow melting and deicing agent comprises the following steps:

[0044] (1) prepare 110g antifreeze magnesium chloride saturated solution;

[0045] (2) Dissolve 9g of diatomite, 1g of nano-silica, and 4g of OP-13 in a flask previously filled with 200mL of absolute ethanol, and place the flask in a 60°C water bath and stir evenly with a Teflon stirring rod , to obtain a diatomite suspension modified by nano-silica;

[0046] (3) t...

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Abstract

The invention provides a salt-storage sustained-release snow-melt deicer and a preparation method thereof. The method comprises the following steps: firstly, respectively preparing an anticoagulationchloride saturated solution and a nano-silicon dioxide modified diatomite suspension; then, adding the anticoagulation chloride saturated solution into the nano-silicon dioxide modified diatomite suspension, stirring, filtering in vacuum, drying and grinding to obtain sustained-release inorganic salt; preparing a polymer monomer solution, sequentially adding the sustained-release inorganic salt, isopropyl alcohol or propylene glycol monomethyl ether solution into a flask, putting the flask in an oil bath, and uniformly stirring, adding the polymer monomer solution and a mixed solution of KH570and gAIBN, keeping on stirring, reducing the temperature, adding triethylamine into the flask, stirring, and adding water to obtain the salt-storage sustained-release snow-melt deicer. According to the salt-storage sustained-release snow-melt deicer, snow-melt substances are not limited by temperature-control molecules, and have long release time and relatively high ice melting capacity.

Description

technical field [0001] The invention belongs to the technical field of road materials, in particular to a salt-storage slow-release snow-melting and deicing agent and a preparation method thereof. Background technique [0002] my country's road network is huge, most of which are located in snow-prone areas. The snow and ice on the road surface in winter greatly reduces the adhesion coefficient of the road surface, which seriously affects the smooth flow of the road and causes traffic safety accidents. The traditional methods of snow melting and deicing include manual mechanical removal method and spraying deicing agent method. However, the artificial mechanical removal method is expensive to remove snow and ice, and the deicing rate is low; the method of spreading deicing agent will cause serious pollution to the environment and corrode the road. . Therefore, the adoption of active, long-term, safe and environmentally friendly snow and ice removal technology will become an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K3/18
CPCC09K3/185
Inventor 郭鹏冯云霞李正强孟建玮魏琳王一村陈秀谨王成符世辉孙易男尹红飞肖振涛杨俊芳高云
Owner CHONGQING JIAOTONG UNIVERSITY
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