Antistatic finishing agent for wool fabric and preparation method thereof

An antistatic finishing agent and fabric technology, applied in the field of antistatic finishing agent and its preparation, can solve the problems of poor durability, poor washing resistance, and the surface is easily damaged by friction, so as to improve antistatic performance, improve poor water resistance, reduce The effect of static electricity

Inactive Publication Date: 2018-12-07
SUZHOU INSILK CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the use of antistatic finishing agents also has disadvantages such as poor washing resistance, poor durability, and the surface is susceptible to friction defects, and further research and improvement are needed.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A preparation method for an antistatic finishing agent for wool fabrics, comprising the following steps:

[0027] (1) Add polybutylene adipate diol, pentaerythritol polyether tetraol, ethylenediamine polyether tetraol and norbornane diisocyanate into the reaction kettle, heat to maintain the temperature at 110 ° C, at 40 rpm Stir at a speed of 1 min, add acetone and N,N-dihydroxyethyl monomaleic anhydride, and hydroxyethyl acrylate and diethylpentanediol, and lower the temperature to 40 ° C, continue stirring for 90 min, and then add water to Stir at a speed of 200 revs / min, evaporate acetone to obtain a polyurethane emulsion with a solid content of 55%;

[0028] (2) Add methacrylic acid, glycidyl methacrylate, polyethylene glycol acrylate, methylol acrylamide, sodium lauryl sulfate, lauryl glucoside and water into the reaction kettle and heat to 60°C , after stirring evenly, a pre-emulsion is prepared;

[0029] (3) Raise the temperature of the polyurethane emulsion t...

Embodiment 2

[0038] A preparation method for an antistatic finishing agent for wool fabrics, comprising the following steps:

[0039](1) Add polybutylene adipate diol, pentaerythritol polyether tetraol, ethylenediamine polyether tetraol and norbornane diisocyanate into the reaction kettle, heat to maintain the temperature at 120 ° C, at 60 rpm Stir at a speed of 1 min, add acetone and N,N-dihydroxyethyl monomaleic anhydride, and hydroxyethyl acrylate and diethylpentanediol, and lower the temperature to 55 ° C, continue stirring for 120 min, and then add water to Stir at a speed of 300 revs / min, evaporate acetone to obtain a polyurethane emulsion with a solid content of 55%;

[0040] (2) Add methacrylic acid, glycidyl methacrylate, polyethylene glycol acrylate, methylol acrylamide, sodium lauryl sulfate, lauryl glucoside and water into the reaction kettle and heat to 80°C , after stirring evenly, a pre-emulsion is prepared;

[0041] (3) Raise the temperature of the polyurethane emulsion t...

Embodiment 3

[0050] A preparation method for an antistatic finishing agent for wool fabrics, comprising the following steps:

[0051] (1) Add polybutylene adipate diol, pentaerythritol polyether tetraol, ethylenediamine polyether tetraol and norbornane diisocyanate into the reaction kettle, heat to maintain the temperature at 110 ° C, at 60 rpm Stir at a speed of 1 min, add acetone and N,N-dihydroxyethyl monomaleic anhydride, and hydroxyethyl acrylate and diethylpentanediol, and lower the temperature to 40 ° C, continue stirring for 120 min, then add water to Stir at a speed of 200 revs / min, evaporate acetone to obtain a polyurethane emulsion with a solid content of 55%;

[0052] (2) Add methacrylic acid, glycidyl methacrylate, polyethylene glycol acrylate, methylol acrylamide, sodium lauryl sulfate, lauryl glucoside and water into the reaction kettle and heat to 80°C , after stirring evenly, a pre-emulsion is prepared;

[0053] (3) Raise the temperature of the polyurethane emulsion to 8...

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PUM

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Abstract

The invention discloses an antistatic finishing agent for a wool fabric and a preparation method thereof, the preparation method comprises the following steps: taking a polyurethane emulsion, heatingup to 80 to 90 DEG C, dropwise adding a pre-emulsion and an initiator into the polyurethane emulsion, continuing reflux and heat preservation reaction for 2-3h after the completion of the dropwise addition of the pre-emulsion and the initiator, adding citric acid to adjust the pH to 3-4, adding polyethylene glycol-200, stirring for reaction for 1-2h, adjusting to neutral, adding water to dilute, sieving, adding dodecyl diphenyl ether disulfonate ammonia, stirring and mixing uniformly, then cooling to room temperature, and removing air bubbles to obtain the antistatic finishing agent for the wool fabric. The wool fabric after being finished by the antistatic finishing agent has good antistatic property, is easy to process, reduces static electricity generation during use, has good water washing and abrasion resistance, and has a long service life.

Description

technical field [0001] The invention relates to the field of textile auxiliaries, in particular to an antistatic finishing agent for wool fabrics and a preparation method thereof. Background technique [0002] Wool fiber has the advantages of good elasticity, good warmth retention, and strong hygroscopicity. It has been widely used in various textile raw materials, and plays an increasingly important role in textile processing. Wool fabric has the characteristics of full texture, good drapability, smooth hand feeling, light and comfortable wearing, etc., and is favored by consumers. With the improvement of people's living standards, consumers have higher and higher requirements for the comprehensive performance of traditional wool fabrics, requiring them to not only have a soft and slender feel, but also have a crisp shape. Inside the wool fiber is the hair shaft, which is composed of a variety of amino acids through peptide bond chains as the main chain of protein polymers...

Claims

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Application Information

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IPC IPC(8): D06M15/572D06M15/568C08G18/32C08G18/42C08G18/48C08G18/50C08G18/67C08G18/75C08G18/66C08G18/62C08G18/38C08F220/06C08F220/32C08F220/28C08F220/58C08F2/26C08F2/30D06M101/12
CPCC08F2/26C08F2/30C08F220/06C08G18/3206C08G18/3857C08G18/4063C08G18/4238C08G18/482C08G18/4829C08G18/5021C08G18/6216C08G18/672C08G18/758D06M15/568D06M15/572D06M2101/12C08G18/6607C08G18/0823C08F220/325C08F220/286C08F220/58
Inventor 周继东
Owner SUZHOU INSILK CO LTD
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