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High-abrasion-resistance lubricating oil containing carbon nitride-graphene additive and preparation method thereof

A technology of graphene and carbon nitride, which is applied in the field of lubricating oil, can solve problems such as unsatisfactory performance of lubricating oil and affect dispersion stability, and achieve the effects of small friction coefficient, improved dispersion, and improved stability

Inactive Publication Date: 2018-12-14
CHENDU NEW KELI CHEM SCI CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] Aiming at the fact that graphene, which is currently widely used, is prone to agglomeration in lubricating oil and water, which affects its dispersion stability in lubricating oil and water and other solvents, making the performance of lubricating oil unsatisfactory, the present invention proposes a nitrogen-containing High wear-resistant lubricating oil with carbonized-graphene additive and preparation method thereof, thereby effectively improving the dispersibility of graphene in lubricating oil and improving the performance of lubricating oil

Method used

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  • High-abrasion-resistance lubricating oil containing carbon nitride-graphene additive and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] The preparation process is:

[0034] (1) Disperse two-dimensional carbon nitride nanosheets in excess copper chloride and graphene colloidal solution, soak the surface of carbon nitride in the colloidal solution, then filter, filter out excess colloidal substances, dry, and In a hydrogen environment, treat at 450°C for 10 minutes to reduce copper chloride to copper, and fix graphene on the surface of two-dimensional carbon nitride; High temperature makes the copper on the surface of carbon nitride slightly melt, further leveling and fixing graphene, and making a wear-resistant composite additive for carbon nitride supported graphene; the colloidal solution is copper chloride, graphene, polyvinyl alcohol , Water is formulated with a mass ratio of 1:5:0.1:20. The inert gas is helium;

[0035](2) Add the composite additive prepared in step (1) to the lubricating base oil, mix well, then add viscosity index improver, dispersant, detergent, anti-oxidant, anti-corrosion and...

Embodiment 2

[0040] The preparation process is:

[0041] (1) Disperse two-dimensional carbon nitride nanosheets in excess copper chloride and graphene colloidal solution, soak the surface of carbon nitride in the colloidal solution, then filter, filter out excess colloidal substances, dry, and In a hydrogen environment, treat at 450°C for 15 minutes to reduce copper chloride to copper, and fix graphene on the surface of two-dimensional carbon nitride; High temperature makes the copper on the surface of carbon nitride slightly melt, further leveling and fixing graphene, and making a wear-resistant composite additive for carbon nitride supported graphene; the colloidal solution is copper chloride, graphene, polyvinyl alcohol , Water is formulated with a mass ratio of 1:5:0.1:20. The inert gas is helium;

[0042] (2) Add the composite additive prepared in step (1) to the lubricating base oil, mix well, then add viscosity index improver, dispersant, detergent, anti-oxidant, anti-corrosion an...

Embodiment 3

[0047] The preparation process is:

[0048] (1) Disperse two-dimensional carbon nitride nanosheets in excess copper chloride and graphene colloidal solution, soak the surface of carbon nitride in the colloidal solution, then filter, filter out excess colloidal substances, dry, and In a hydrogen environment, treat at 450°C for 15 minutes to reduce copper chloride to copper, and fix graphene on the surface of two-dimensional carbon nitride; High temperature makes the copper on the surface of carbon nitride slightly melt, further leveling and fixing graphene, and making a wear-resistant composite additive for carbon nitride supported graphene; the colloidal solution is copper chloride, graphene, polyvinyl alcohol , Water is formulated with a mass ratio of 1:5:0.1:20. The inert gas is helium;

[0049] (2) Add the composite additive prepared in step (1) to the lubricating base oil, mix well, then add viscosity index improver, dispersant, detergent, anti-oxidant, anti-corrosion an...

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Abstract

The invention provides a high-abrasion-resistance lubricating oil containing carbon nitride-graphene additive and a preparation method thereof. A two-dimensional carbon-nitride nano-sheet is dispersedin excess copper chloride and graphene colloid solution, copper chloride is reduced to copper in hydrogen gas environment, and graphene is fixed on the surface of the two-dimensional carbon-nitride;the product is subjected to further treatment in a reactor under inert gas protection 5-10 seconds, copper on the surface of carbon-nitride is micro-melted by instantaneous high temperature, and the abrasion-resistance composite additive of the carbon-nitride loaded with graphene is prepared; the high-abrasion-resistance lubricating oil containing two-dimensional carbon nitride-graphene additive is synthesized by mixing the abrasion-resistance composite additive with base oil and various auxiliaries. The two-dimensional carbon nitride-graphene additive is prepared, the conventional additive carbon nitride is used as carrier, so as to significantly improve the dispersion of graphene in base oil, improve the stability of lubricating oil, and effectively improve the friction and wear behaviorof friction surface in application, and furthermore be conducive to prolonging the service life of mechanical parts.

Description

technical field [0001] The invention relates to the field of lubricating oil, in particular to the preparation of high wear-resistant lubricating oil, in particular to a high wear-resistant lubricating oil containing carbon nitride-graphene additive and a preparation method thereof. Background technique [0002] Lubricating oil is a liquid or semi-solid lubricant used in various types of automobiles and mechanical equipment to reduce friction and protect machinery and processed parts. It mainly plays the roles of lubrication, auxiliary cooling, rust prevention, cleaning, sealing and buffering. Lubricating oil generally consists of two parts: base oil and additives. Base oil is the main component of lubricating oil, which determines the basic properties of lubricating oil. Additives can make up for and improve the performance of base oil, endow some new properties, and are an important part of lubricating oil. [0003] Lubricating oil additives are a key part of lubricating ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M125/20C10M169/04C10N30/06
CPCC10M125/20C10M169/048C10M2201/041C10M2201/05C10M2201/061C10M2201/085C10M2201/087C10M2203/1006C10M2205/022C10M2205/024C10M2205/026C10M2205/04C10M2205/06C10M2207/126C10M2209/04C10M2209/08C10M2209/104C10M2209/105C10M2209/108C10M2217/022C10M2223/045C10N2030/06C10N2010/02C10N2010/04C10N2060/02
Inventor 陈庆昝航
Owner CHENDU NEW KELI CHEM SCI CO LTD
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