Identification method of guava leaf processed products
A technique of guava leaf cannon and pomegranate leaf cannon, which is applied in the field of traditional Chinese medicine identification, can solve the problems of unrecorded detection methods of guava leaf cannon products, and achieve the effect of good spot separation effect, easy operation and high accuracy
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Embodiment 1
[0031] The preparation method of guava leaf processed product contrast medicinal material solution is as follows:
[0032] Weigh 2 g of guava leaf processed product reference medicinal material, crush it into powder, sieve the powder, pour it into a container with a stopper, add 50 mL of 95% ethanol solution, process it with ultrasonic for 0.5 h, filter, evaporate the filtrate to dryness, and dissolve the residue in water , extracted 2 times with petroleum ether, 10mL each time, combined the petroleum ether extracts, evaporated to dryness, and added 2mL of methanol as the reference medicinal solution of guava leaf processed products.
[0033] The preparation method of the test solution is as follows:
[0034] Weigh 2 g of the test product, crush it into powder, sieve the powder, pour it into a container with a stopper, and add 50 mL of 95% ethanol solution, after ultrasonic treatment for 0.5 h, filter, evaporate the filtrate to dryness, add water to dissolve the residue, and u...
Embodiment 2
[0038] The preparation method of guava leaf processed product contrast medicinal material solution is as follows:
[0039] Weigh 2 g of guava leaf processed product reference medicinal material, crush it into powder, sieve the powder, pour it into a container with a stopper, add 50 mL of 95% ethanol solution, process it with ultrasonic for 0.5 h, filter, evaporate the filtrate to dryness, and dissolve the residue in water , extracted 2 times with petroleum ether, 10mL each time, combined the petroleum ether extracts, evaporated to dryness, and added 2mL of methanol as the reference medicinal solution of guava leaf processed products.
[0040] The preparation method of the test solution is as follows:
[0041] Weigh 2 g of the test product, crush it into powder, sieve the powder, pour it into a container with a stopper, and add 50 mL of 95% ethanol solution, after ultrasonic treatment for 0.5 h, filter, evaporate the filtrate to dryness, add water to dissolve the residue, and u...
Embodiment 3
[0045] The preparation method of guava leaf processed product contrast medicinal material solution is as follows:
[0046] Weigh 2 g of guava leaf processed product reference medicinal material, crush it into powder, sieve the powder, pour it into a container with a stopper, add 50 mL of 95% ethanol solution, process it with ultrasonic for 0.5 h, filter, evaporate the filtrate to dryness, and dissolve the residue in water , extracted 2 times with petroleum ether, 10mL each time, combined the petroleum ether extracts, evaporated to dryness, and added 2mL of methanol as the reference medicinal solution of guava leaf processed products.
[0047] The preparation method of the test solution is as follows:
[0048] Weigh 2 g of the test product, crush it into powder, sieve the powder, pour it into a container with a stopper, and add 50 mL of 95% ethanol solution, after ultrasonic treatment for 0.5 h, filter, evaporate the filtrate to dryness, add water to dissolve the residue, and u...
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