Pt/Rh nano composite material and preparation method and application thereof
A nanocomposite material and nanotechnology, applied in the field of nanomaterials, can solve the problems of unsuitable Pt-based nanomaterials, etc., and achieve the effects of excellent activity, simple preparation method, and enhanced activity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0058] The present embodiment prepares Pt / Rh nanocomposite material according to the following method:
[0059] Dissolve chloroplatinic acid and rhodium acetylacetonate in benzyl alcohol, add polyvinylpyrrolidone and formaldehyde, stir well, wherein the concentration of chloroplatinic acid is 0.7mmol / L, the concentration of rhodium acetylacetonate is 3.2mmol / L, and the concentration of polyvinylpyrrolidone is 16.0g / L, formaldehyde concentration is 7000mmol / L. The reaction was heated at 180°C for 8h. After the reaction is finished, cool down to room temperature, wash the reactant with acetone and ethanol, centrifuge to remove the supernatant, and obtain the Pt / Rh nanocomposite material.
[0060] The Pt / Rh nanocomposite material provided by this embodiment is composed of Rh nanosheets and Pt nanoclusters loaded on the Rh nanosheets, the molar ratio of Pt nanoclusters to Rh nanosheets is 0.219:1, and the ratio of Rh nanosheets is The shape is trapezoidal, the average length of ...
Embodiment 2
[0071] The present embodiment prepares Pt / Rh nanocomposite material according to the following method:
[0072] Dissolve potassium chloroplatinate and rhodium chloride in ethylene glycol, add polyethylene glycol and formaldehyde, stir well, wherein the concentration of potassium chloroplatinate is 1.0mmol / L, the concentration of rhodium chloride is 3.0mmol / L, polyethylene glycol The diol concentration is 12.0g / L, and the formaldehyde concentration is 5000mmol / L. The reaction was heated at 180°C for 8h. After the reaction is finished, cool down to room temperature, wash the reactant with acetone and ethanol, centrifuge to remove the supernatant, and obtain the Pt / Rh nanocomposite material.
[0073] The Pt / Rh nanocomposite material provided in this embodiment is composed of Rh nanosheets and Pt nanoclusters loaded on the Rh nanosheets, the molar ratio of Pt nanoclusters to Rh nanosheets is 0.327:1, and the ratio of Rh nanosheets is The shape is trapezoidal, the average length ...
Embodiment 3
[0076] The present embodiment prepares Pt / Rh nanocomposite material according to the following method:
[0077] Dissolve platinum acetylacetonate and rhodium acetylacetonate in benzyl alcohol, add polyvinylpyrrolidone and salicylaldehyde, stir evenly, wherein the concentration of platinum acetylacetonate is 1.5mmol / L, the concentration of rhodium acetylacetonate is 3.3mmol / L, polyvinylpyrrolidone The concentration is 25.0g / L, and the concentration of salicylaldehyde is 4mmol / L. The reaction was heated at 180°C for 8h. After the reaction is finished, cool down to room temperature, wash the reactant with acetone and ethanol, centrifuge to remove the supernatant, and obtain the Pt / Rh nanocomposite material.
[0078] The Pt / Rh nanocomposite material provided in this embodiment is composed of Rh nanosheets and Pt nanoclusters loaded on the Rh nanosheets, the molar ratio of Pt nanoclusters to Rh nanosheets is 0.449:1, and the Rh nanosheets The shape is trapezoidal, the average len...
PUM
Property | Measurement | Unit |
---|---|---|
length | aaaaa | aaaaa |
length | aaaaa | aaaaa |
thickness | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com