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Preparation of modified micron particles for wood welding and use and method of using the same

A micro-particle and modified technology, applied in the direction of wood impregnation, wood treatment, impregnated wood, etc., can solve the problems of poor water resistance and durability, insufficient mechanical properties, brittle interface, etc., to achieve improved durability, improved mechanical properties, Water resistance improvement effect

Active Publication Date: 2020-11-06
NANJING FORESTRY UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the interface of wood welding produced by these two methods is relatively brittle, which makes the overall mechanical properties of wood welding not good enough, and its water resistance and durability are poor.

Method used

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  • Preparation of modified micron particles for wood welding and use and method of using the same
  • Preparation of modified micron particles for wood welding and use and method of using the same
  • Preparation of modified micron particles for wood welding and use and method of using the same

Examples

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Effect test

specific Embodiment 1

[0029] A method for preparing modified micron particles for wood welding, comprising the following steps:

[0030] S01, put the ethanol solution, tetraethyl orthosilicate and ammonia solution into the stirring reactor for stirring reaction, after a period of time, vacuum filter out the silicon dioxide particles. Wherein, the volume concentration of ethanol solution is 95%, and the volume is 100cm 3 , the volume of tetraethyl orthosilicate is 34cm 3 , the mass fraction of ammonia solution is 25%, and the volume is 22cm 3 , the stirring rate of the stirred reactor was 1800 revolutions per minute, and the stirring reaction time was 60 min.

[0031] S02, use ethanol to ultrasonically wash the silicon dioxide particles obtained in S01, the number of times of ultrasonic washing is 3 times, then perform vacuum filtration, then use pure water to wash the silicon dioxide particles, and finally perform suction filtration.

[0032] S03 is dried after suction filtration, the drying tem...

specific Embodiment 2

[0045] This embodiment is the same as Embodiment 1, except that in S15 wood welding is combined with rotational friction welding. Sand the surface of the beech log tenon to be welded with 100-mesh sandpaper, then heat the sanded round tenon to 80°C by microwave, and immediately immerse it in the modification solution at 2°C while maintaining 80°C , the treatment time is 15 minutes, and then the round wooden tenons are taken out and dried at 50°C for 2 hours.

[0046]First, reserve a reserved hole with a diameter of 8mm on the masson pine wood member to be welded, with a depth of 30mm, and the welding direction is perpendicular to the direction of the wood fiber, and then weld the bamboo tenon into the reserved hole at a speed of 12mm / s, and the feeding time It is 2.5s, and the rotation speed is 1800r / min. When the bamboo tenon touches the bottom of the reserved hole, stop the rotation, keep the pressure for 45 seconds, and then cut off the round wooden tenon exposed on the su...

specific Embodiment 3

[0050] A method for preparing modified micron particles for wood welding, comprising the following steps:

[0051] S01, put the ethanol solution, tetraethyl orthosilicate and ammonia solution into the stirring reactor for stirring reaction, after a period of time, vacuum filter out the silicon dioxide particles. Wherein, the volume concentration of ethanol solution is 95%, and the volume is 90cm 3 , the volume of tetraethyl orthosilicate is 32cm 3 , the mass fraction of ammonia solution is 25%, and the volume is 20cm 3 , the stirring rate of the stirred reactor was 1600 rpm, and the stirring reaction time was 50 min.

[0052] S02, use ethanol to ultrasonically wash the silicon dioxide particles obtained in S01, the number of times of ultrasonic washing is 2 times, then perform vacuum filtration, then use pure water to wash the silicon dioxide particles, and finally perform suction filtration.

[0053] S03 is dried after suction filtration, the drying temperature is 100° C.,...

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Abstract

The invention discloses a method for preparing modified micron particles for wood welding, comprising the following steps: S01, putting ethanol solution, tetraethyl orthosilicate and ammonia solution into a stirring reactor for stirring reaction; S02, using ethanol to Silica particles are ultrasonically washed, followed by vacuum filtration; S03, dried after suction filtration, to obtain microdiameter silica particles; S04, configure a mixed solvent of water and methanol, and then dissolve N-β (ammonia ethyl Base)-γ-aminopropylmethyldimethoxysilane; S05, soak the silica particles in the microparticle modification solution for a period of time, vacuum filter, and finally dry to obtain modified microparticles. The invention also discloses a method for using the modified micron particles for wood welding and bonding. The preparation and use method of modified micron particles for wood welding and bonding of the present invention can greatly improve the toughness of wood welding from the aspect of microstructure design through the control of the interface structure, and at the same time enhance the water resistance and durability of wood welding.

Description

technical field [0001] The invention relates to a method for preparing and using modified micron particles for wood welding and bonding, and belongs to the field of wood gluing. Background technique [0002] Wood welding technology is a kind of wood glue-free gluing technology developed in recent years. Due to its advantages of environmental protection, simple process and high efficiency, it has attracted more and more people's attention. Wood welding is a new type of wood gluing method realized by using the natural components of wood itself under the action of temperature and mechanical force generated by friction. Therefore, wood welding generally refers to wood friction welding, and linear vibration friction welding and rotational friction welding are the two most widely used methods in wood welding. However, the interface of wood welding produced by these two methods is relatively brittle, which makes the overall performance of wood welding not good enough in mechanical...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B27K3/08B27K5/00B27K5/04B27K3/00
CPCB27K3/005B27K3/08B27K5/0055B27K5/0065B27K5/0085B27K5/04
Inventor 张海洋梅长彤詹先旭何倩洪璐鞠泽辉
Owner NANJING FORESTRY UNIV