Filtration and clarification process for baijiu

A liquor and technology technology, applied in the field of liquor processing, can solve the problems of alcohol smell, not suitable for clarification of Debao liquor, solid content exceeding the standard, etc.

Active Publication Date: 2019-02-01
广西德保新贝侬酒厂有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Debao County, Guangxi is located in the Shishan area. Its underground mineral content is rich, and its water is mostly hard water. The content of calcium ions, magnesium ions, and iron ions in the water is relatively high. The solid content exceeds the

Method used

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  • Filtration and clarification process for baijiu

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Embodiment 1

[0019] A kind of filtration and clarification process of liquor of the present embodiment comprises the following steps:

[0020] (1) Coarse filtration: add 0.5g / L diatomaceous earth to the liquor, stir for 20min, let stand at 5°C for 5 days, centrifuge at 2000r / min for 15min, remove the precipitate, take the supernatant, and obtain the coarsely filtered liquor ;

[0021] (2) Fine filtration: add 0.05g / L chitosan solution to the above-mentioned coarse filter wine, mix and stir evenly, after ultrasonic treatment at 200W for 20min, add 1g / L active adsorbent, stir for 30min, at 5°C Let it stand for 3 days, centrifuge at 2000r / min for 15min, remove the precipitate, and filter the upper liquor with a microporous membrane with a pore size of 0.1μm.

[0022] The preparation method of the chitosan solution is as follows: add chitosan into a citric acid solution with a mass concentration of 1% and heat until dissolved, the mass ratio of chitosan to the citric acid solution is 1:100, a...

Embodiment 2

[0025] A kind of filtration and clarification process of liquor of the present embodiment comprises the following steps:

[0026] (1) Coarse filtration: add 1.8g / L diatomaceous earth to the liquor, stir for 50min, let stand at 10°C for 7 days, centrifuge at 2500r / min for 25min, remove the precipitate, take the supernatant, and obtain the coarsely filtered liquor ;

[0027] (2) Fine filtration: add 0.15g / L chitosan solution to the above-mentioned coarse filter wine and mix well, after ultrasonic treatment at 300W for 30min, add 3g / L active adsorbent, stir for 50min, and then filter the mixture at 8°C Let it stand for 5 days, centrifuge at 2500r / min for 25min, remove the precipitate, and filter the upper liquor with a microporous membrane with a pore size of 0.3μm.

[0028] The preparation method of the chitosan solution is as follows: add chitosan into a citric acid solution with a mass concentration of 2% and heat until dissolved, the mass ratio of chitosan to the citric acid...

Embodiment 3

[0031] A kind of filtration and clarification process of liquor of the present embodiment comprises the following steps:

[0032] (1) Coarse filtration: add 1.5g / L diatomaceous earth to liquor, stir for 30min, let it stand at 8°C for 6 days, centrifuge at 2200r / min for 20min, remove the precipitate, take the supernatant, and obtain coarse filtration liquor ;

[0033] (2) Fine filtration: add 0.10g / L chitosan solution to the above-mentioned coarse filter wine, mix and stir evenly, after ultrasonic treatment at 250W for 25min, add 2g / L active adsorbent, stir for 40min, and place at 7°C Let it stand for 4 days, centrifuge at 2300r / min for 18min, remove the precipitate, and filter the upper liquor with a microporous membrane with a pore size of 0.2μm.

[0034] The preparation method of the chitosan solution is as follows: add chitosan into a citric acid solution with a mass concentration of 1.5% and heat until dissolved, the mass ratio of chitosan to citric acid solution is 1.5:1...

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Abstract

Relating to the technical field of liquor processing, the invention discloses a filtration and clarification process for baijiu. The process includes: firstly adding diatomite into baijiu, conductingstirring, standing, centrifuging and precipitate removing to obtain coarse filtered liquor, then adding a chitosan solution into the coarse filtered liquor, mixing the substances evenly, conducting ultrasonic treatment, then adding an active adsorbent, and carrying out stirring, standing, centrifuging and filtering. The preparation method of the active adsorbent includes: grinding attapulgite andsodium silicate, then performing high temperature calcination, mixing the treated mixture with shrimp shell powder, then performing grinding and granulation, and finally adding the granules into a sodium hydroxide solution for soaking treatment. The process provided by the invention can remove calcium ions, magnesium ions and iron ions from liquor targetedly, effectively prevents excessive solid content and fishy smell of the product, and improves the product quality.

Description

【Technical field】 [0001] The invention relates to the technical field of liquor processing, in particular to a filtration and clarification process for liquor. 【Background technique】 [0002] Filtration and clarification is one of the important links in the production and processing of liquor. In addition to alcohol and water, newly brewed liquor also contains insoluble substances, proteins, tannins, pigments, colloids and other components, which are prone to browning, loss of light, turbidity and precipitation during storage. Filtration and clarification will shorten the shelf life and reduce the quality. At present, diatomite, bentonite, chitosan or gelatin are generally used in liquor production to settle and remove impurities, or to filter and clarify by natural clarification, which have good results. [0003] Debao County, Guangxi is located in the Shishan area. Its underground mineral content is rich, and its water is mostly hard water. The content of calcium ions, m...

Claims

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Application Information

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IPC IPC(8): C12H1/048C12H1/052C12H1/07C12H1/06
CPCC12H1/0408C12H1/0416C12H1/06C12H1/063
Inventor 杨维特
Owner 广西德保新贝侬酒厂有限公司
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