Digital pre-coating film and preparation method thereof
A pre-coating and digital technology, applied in the field of digital pre-coating, can solve the problems of affecting the composite effect and insufficient composite fastness of ordinary laminations, and achieve the effect of increasing composite fastness, reducing cracking or even separation, and increasing wetting performance.
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[0022] A preparation method of a digital pre-coating film, comprising the following steps:
[0023] Step 1, unwinding the substrate film layer and performing corona treatment on the inner surface of the substrate film layer;
[0024] Step 2, uniformly coating the polyethyleneimine solution on the inner surface of the substrate film layer, and drying, the concentration of the polyethyleneimine solution is 2.5-5.0%;
[0025] Step 3, under the oxidation of ozone, the mixture of ethylene-vinyl acetate polymer and tackifier is melt-extruded, and compounded on the surface of the primer layer by casting method, the ethylene-vinyl acetate polymer The melt index is 15-16g / 10min at 190°C and 2.16kg;
[0026] Step 4. Trimming and measuring the thickness of the prepared pre-coating film, and then performing high-frequency and high-voltage corona treatment on the hot-melt adhesive layer, and finally winding and cutting.
Embodiment 1
[0028] 1) Unwind the 15 μm biaxially oriented polypropylene film substrate and perform corona treatment on its inner surface;
[0029] 2) Uniformly coat a layer of primer solution with a polyethyleneimine content of 2.5% on the corona treated surface, and dry it in an oven at 70±10°C;
[0030] 3) At the same time of ozone oxidation, a mixture of 90% mass fraction of hot melt adhesive ethylene-vinyl acetate polymer and 10% mass fraction of terpene resin (the content of vinyl acetate is 28wt%, ethylene-vinyl acetate polymer The melt index is 15g / 10min under the conditions of 190°C and 2.16kg), melted and extruded at 220±5°C, and compounded on the surface of the primer layer by casting method to form a hot melt adhesive layer;
[0031] 4) Cooling on a cooling roll at 22±2°C, and finally trimming and measuring the thickness to obtain a pre-coating film with a total thickness of about 35 μm;
[0032] 5) Carry out high-frequency and high-voltage corona treatment on both sides of th...
Embodiment 2
[0034] 1) Unwind the 15 μm biaxially oriented polypropylene film substrate and perform corona treatment on its inner surface;
[0035] 2) Uniformly coat a layer of primer solution with a polyethyleneimine content of 5.0% on the corona-treated surface, and dry it in an oven at 70±10°C;
[0036] 3) while ozone oxidation, the mixture of the hot-melt adhesive ethylene-vinyl acetate polymer of 95% mass fraction and the petroleum resin of 5% mass fraction (the content of vinyl acetate is 28wt%, the content of ethylene-vinyl acetate polymer The melt index is 16g / 10min under the conditions of 190°C and 2.16kg), melted and extruded at 220±5°C, and compounded on the surface of the primer layer by casting method to form a hot melt adhesive layer;
[0037] 4) Cooling on a cooling roll at 22±2°C, and finally trimming and measuring the thickness to obtain a pre-coating film with a total thickness of about 35 μm;
[0038] 5) Carry out high-frequency and high-voltage corona treatment on both...
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