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Super black material and preparation method and application thereof

A technology of ultra-black materials and light-absorbing materials, applied in the field of ultra-black materials and their preparation, can solve the problems of inability to carry out large-scale production and high cost, and achieve the effects of low price of finished products, easy operation, and easy control of process conditions

Active Publication Date: 2019-02-19
CENT SOUTH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Most of these methods have the disadvantages of high cost and inability to carry out large-scale production.

Method used

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  • Super black material and preparation method and application thereof
  • Super black material and preparation method and application thereof
  • Super black material and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] The invention provides a kind of preparation method of super black material, comprises the following steps:

[0040] (1) Place the quartz plate in alcohol, clean it with ultrasonic waves for 5 minutes, and dry it for later use;

[0041] (2) Copper acetylacetonate (Cu(acac) 2 , Aldrich Chemical Co, 97%;) placed in the quartz boat, stand-by;

[0042] (3) Place the copper acetylacetonate in the quartz boat in the evaporation zone in the tube furnace, raise the temperature to 150°C, and hold the temperature for 120min. The quartz glass plate (40mm×200mm×2mm) for collecting the samples is placed in the tube furnace. In the deposition area, the temperature is raised to 700°C, the holding time is 120min, and then the tube furnace is closed;

[0043] (4) Close all valves, turn on the vacuum pump to pump air, and after confirming that the system is airtight, set the experimental parameters, turn on the heating button, and feed the carrier gas Ar (flow rate: 200ml / min, purity: ...

Embodiment 2

[0046] The invention provides a kind of preparation method of super black material, comprises the following steps:

[0047] (1) Place the quartz plate in alcohol, clean it with ultrasonic waves for 5 minutes, and dry it for later use;

[0048] (2) Copper acetylacetonate (Cu(acac) 2 , Aldrich Chemical Co, 97%;) placed in the quartz boat, stand-by;

[0049] (3) Copper acetylacetonate in the quartz boat is placed in the evaporation zone in the tube furnace, and the temperature is raised to 150°C. The quartz glass plate (40mm×200mm×2mm) for collecting the samples is placed in the deposition zone of the tube furnace, and the temperature is raised to 150°C. 700°C, the holding time is 120min, and then the tube furnace is closed;

[0050](4) Close all valves, turn on the vacuum pump to pump air, and after confirming that the system is airtight, set the experimental parameters, turn on the heating button, and feed the carrier gas Ar (flow rate: 50ml / min, purity: 99.99%), and keep the...

Embodiment 3

[0053] The invention provides a kind of preparation method of super black material, comprises the following steps:

[0054] (1) Place the quartz plate in alcohol, clean it with ultrasonic waves for 5 minutes, and dry it for later use;

[0055] (2) Copper acetylacetonate (Cu(acac) 2 , Aldrich Chemical Co, 97%;) placed in the quartz boat, stand-by;

[0056] (3) Copper acetylacetonate in the quartz boat is placed in the evaporation zone in the tube furnace, and the temperature is raised to 180°C. The quartz glass plate (40mm×200mm×2mm) for collecting the samples is placed in the deposition zone of the tube furnace, and the temperature is raised to 180°C. 700°C, the holding time is 120min, and then the tube furnace is closed;

[0057] (4) Close all valves, turn on the vacuum pump to pump air, and after confirming that the system is airtight, set the experimental parameters, turn on the heating button, and feed the carrier gas Ar (flow rate: 500ml / min, purity: 99.99%), and mainta...

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Abstract

The invention discloses a super black material and a preparation method and application thereof, and belongs to the technical field of nanometer material preparation. The super black material is composed of a base copper nanometer cluster and a graphitized carbon layer supported on the surface thereof, and the super black material forms the core-shell structure and is composed of, by weight: 51.9%to 84.3% of the copper nanometer cluster and 15.7% to 48.1% of carbon. By using the copper 4-pentanedionate hydrate as an elementary material, the super black material and preparation method and application thereof coats the surface of the copper nanometer cluster with the graphitized carbon layer to form a unique core-shell structure. The obtained super black material is characterized by excellent light absorption, and has significant optical loss effect caused by surface effect and quantum effect. The absorption range of the copper nanometer cluster or the super-black carbon material is soextensive that the copper nanometer cluster or the super-black carbon material has good light absorption performance at the wavelength of 200-900 nm; and the preparation method of the super black material is easy to operate, low in cost of finished products and process cost and conducive to industrial production, and the process conditions are easy to control.

Description

technical field [0001] The invention belongs to the technical field of nanomaterial preparation, and in particular relates to an ultra-black material and its preparation method and application. Background technique [0002] Ultra-black material is a material with a reflectivity of less than 1% and an absorption rate of more than 99% for incident light within a certain range. In many optical devices, sensors, and solar energy converters, there is an urgent need for ultra-black materials in such devices because unnecessary reflection of incident light by the interface will have many adverse effects on performance. At the same time, due to the excellent stealth performance of the ultra-black material itself, it is also of great use in the military. [0003] In view of this, ultra-black materials have been extensively studied and applied in recent years. At present, the most outstanding performance is Vantablack developed by Surrey Nanosystems, which is mainly composed of vert...

Claims

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Application Information

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IPC IPC(8): B22F1/02B22F9/30C08K9/12C08K3/08C08K3/04C08L63/00
CPCC08K3/04C08K3/08C08K9/12C08L63/00B22F9/30C08K2003/085C08K2201/011B22F1/16
Inventor 邓联文徐运超罗衡黄生祥王晓廖聪维
Owner CENT SOUTH UNIV
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