Super black material and preparation method and application thereof
A technology of ultra-black materials and light-absorbing materials, applied in the field of ultra-black materials and their preparation, can solve the problems of inability to carry out large-scale production and high cost, and achieve the effects of low price of finished products, easy operation, and easy control of process conditions
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[0038] Example 1
[0039] The present invention provides a preparation method of super black material, including the following steps:
[0040] (1) Put the quartz plate in alcohol, clean it with ultrasonic for 5 minutes, and dry it for later use;
[0041] (2) Use a medicine spoon to add copper acetylacetonate (Cu(acac) 2 , Aldrich Chemical Co, 97%;) placed in a quartz boat for use;
[0042] (3) Place the copper acetylacetonate in the quartz boat in the evaporation zone of the tube furnace, raise the temperature to 150°C, hold the temperature for 120 min, and place the quartz glass plate (40mm×200mm×2mm) on which the sample is collected in the tube furnace. In the deposition zone, the temperature is raised to 700℃, the holding time is 120min, and then the tube furnace is closed;
[0043] (4) Close all valves, open the vacuum pump to pump air, after confirming that the system is airtight, set the experimental parameters, turn on the heating button, and pass in the carrier gas Ar (flow: 20...
Example Embodiment
[0045] Example 2
[0046] The present invention provides a preparation method of super black material, including the following steps:
[0047] (1) Put the quartz plate in alcohol, clean it with ultrasonic for 5 minutes, and dry it for later use;
[0048] (2) Use a medicine spoon to add copper acetylacetonate (Cu(acac) 2 , Aldrich Chemical Co, 97%;) placed in a quartz boat for use;
[0049] (3) Place the copper acetylacetonate in the quartz boat in the evaporation zone of the tube furnace and heat it to 150°C. Place the quartz glass plate (40mm×200mm×2mm) on which the sample is collected in the deposition zone of the tube furnace, and heat it to 700℃, the holding time is 120min, then the tube furnace is closed;
[0050] (4) Close all valves, open the vacuum pump for air extraction, after confirming that the system is airtight, set the experimental parameters, turn on the heating button, and pass in the carrier gas Ar (flow: 50ml / min, purity: 99.99%), and maintain a pressure of 50Pa;
[0...
Example Embodiment
[0052] Example 3
[0053] The present invention provides a preparation method of super black material, including the following steps:
[0054] (1) Put the quartz plate in alcohol, clean it with ultrasonic for 5 minutes, and dry it for later use;
[0055] (2) Use a medicine spoon to add copper acetylacetonate (Cu(acac) 2 , Aldrich Chemical Co, 97%;) placed in a quartz boat for use;
[0056] (3) Place the copper acetylacetonate in the quartz boat in the evaporation zone of the tube furnace and heat it to 180°C. Place the quartz glass plate (40mm×200mm×2mm) on which the sample is collected in the deposition zone of the tube furnace, and heat it to 700℃, the holding time is 120min, then the tube furnace is closed;
[0057] (4) Close all valves, open the vacuum pump to pump air, after confirming that the system is airtight, set the experimental parameters, turn on the heating button, and pass in the carrier gas Ar (flow: 500ml / min, purity: 99.99%), and maintain a pressure of 50Pa;
[0058] (...
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