The application belongs to the technical field of
processing of super-black functional surfaces, and discloses a preparation method of a super-black surface with a large angle and low
reflectivity, which comprises the following steps: S1, cleaning and
drying treatment is performed on the surface of a sample; S2, a
femtosecond laser is used to perform
direct writing processing on the sample, and a
regular array of parabolic microscale structures is processed on the surface of the sample; S3, nano-particle
extinction black paint is uniformly sprayed on the surface of the sample, and the nano-particle
extinction black paint is distributed on the surface and the gap of the parabolic microscale structures; and S4, the sample is heated and dried, so that a required super-black surface product is obtained. Through the application, the
femtosecond laser processing and the spraying process are ingeniously combined, a multi-scale hierarchical structure is formed, and the extreme light
absorption effect from visible light to near-
infrared in a wide spectral band and in all directions is realized. The prepared super-black surface still has excellent anti-reflection performance (specular
reflectivity is lower than 0.05%) under the condition of a large incident angle (> 60°) and a wide spectrum (200nm-2500nm).