PVD (Physical Vapor Deposition) super-black coating

A black coating and coating technology, applied in coating, metal material coating process, ion implantation plating, etc., can solve the problems of low sputtering deposition energy, rough film layer, high evaporation rate of deposited ions, and achieve surface The effect of high finish, high film compactness and high film adhesion

Inactive Publication Date: 2012-08-08
SHANGHAI ZENIX VACUUM COATING TECH
View PDF5 Cites 3 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Plasma arc (commonly known as electric arc, multi-arc) deposition refers to the generation of arc discharge on the surface of the target (the material to be deposited) under certain vacuum conditions, thereby causing changes in the physical state of the target, and simultaneously ejecting target atoms, Ions, molten particles; advantages: high evaporation rate of deposited ions, high sputtering energy; disadvantages: relatively rough film; in the preparation of metal carbide coatings, due to the poisoning of the target surface, the arc is unstable and even arc extinguished
[0006] Sputtering deposition refers to the generation of glow discharge on the target surface under certain vacuum conditions, and at the same time high-energy ions or neutral atoms are generated to collide with the target, and some materials are sputtered from the target surface through the transfer of kinetic energy; advantages : The deposited particles are mainly atoms, and the deposited coating is smoother; Disadvantage: The bonding fastness is worse than that of arc
The resistance value of the target surface will also become larger and larger (even insulation), resulting in unstable glow (or termination of glow power generation), making sputtering deposition impossible; therefore, under the existing technical conditions, in order to prevent target poisoning When the glow is unstable, the ratio of the metal compound can only be reduced rigidly, and the blackness of the produced black film layer is always light, and it is difficult to reach the depth of the favorite piano black developed by major 3C companies; in addition, traditional sputtering deposition The energy is low, and the overall film layer 40 formed is relatively loose, resulting in poor bonding force between the entire film layer 40 and the substrate 10; although simply increasing the deposition temperature can improve the material, shape, thickness, etc. of the substrate 10 of the coating film. There are more limitations, which is not conducive to large-scale industrial application

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • PVD (Physical Vapor Deposition) super-black coating
  • PVD (Physical Vapor Deposition) super-black coating
  • PVD (Physical Vapor Deposition) super-black coating

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] please see image 3 As shown, a multifunctional PVD coating machine in the embodiment of the present invention includes a vacuum chamber 60, a conductive workpiece turret 110 arranged in the vacuum chamber, a plasma arc evaporation source 70 and an arc power supply 80, and also includes a pulse bias power supply 100 , intermediate frequency sputtering source 130 and 140, intermediate frequency power supply 160, gas ion source 150, ion source power supply 90, described pulse bias power supply 100 and plasma arc evaporation source 70, intermediate frequency sputtering source 130 and 140, gas ion source 150 pass The four sets of switches are individually controlled, and the pulse bias power supply 100, the plasma arc evaporation source 70, the intermediate frequency sputtering sources 130 and 140, and the gas ion source 150 can all work independently or in coordination.

[0027] The conductive workpiece turret 110 is insulated from the vacuum chamber 60, and the vacuum cha...

Embodiment 2

[0032] The substrate 1 is prepared, and the material of the substrate is conductive metal material. The film layer 2 is deposited using the multifunctional PVD coating machine described in the embodiment. The specific method is: using the plasma multi-arc deposition device 70 , using a low-voltage, high-current power source 80 to generate arc power on the surface of the target, generating a target plasma, and depositing the plasma on the substrate 1 . And by using the pulse bias power supply 100, a negative bias voltage of 300-600V is applied on the surface of the substrate 1, and the thickness of the metal film layer 2 is controlled at 0.05-0.15um.

[0033] Deposit the film layer 3, turn on the plasma multi-arc deposition device 70, use a low-voltage, high-current power supply 80 to generate arc power on the surface of the metal film layer 2, generate plasma, and deposit the plasma on the base metal film layer 2 while using an intermediate frequency The sputtering sources 13...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a PVD (Physical Vapor Deposition) super-black coating. A 0.05-0.15 micron thick metal film layer, a 0.05-0.15 micron thick magnetron sputtering compound layer, a 0.10-0.20 micron thick jointing base coating, a 0.20-1.00 micron thick metal compound transition layer and a 0.20-0.50 micron thick compound surface layer are arranged on a metal substrate in turn. The PVD super-black coating has the advantages that the color blackness of the PVD super-black coating is deep, L value can reach 26, the binding force of the film layer is high, the surface smoothness is high, the compactness of the film layer is high, and the PVD super-black coating is suitable for mass production.

Description

technical field [0001] The invention relates to the field of PVD vacuum ion coating, in particular to an ultra-black coating formed by the improvement of a sputtering and plasma arc coating machine. Background technique [0002] PVD is the abbreviation of Physical Vapor Deposition in English, which means "Physical Vapor Deposition" in Chinese, which refers to the film preparation technology that deposits materials on the workpiece to be plated by physical methods under vacuum conditions. The method of PVD is to transfer the desired bulk deposited physical material to the surface of the substrate through direct mass transfer. [0003] PVD (Physical Vapor Deposition) technology is mainly divided into three categories, vacuum evaporation coating, vacuum sputtering coating and vacuum ion coating. Compared with the three classifications of PVD technology, the corresponding vacuum coating equipment also includes vacuum evaporation coating machine, vacuum sputtering coating machin...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/06C23C14/22
Inventor 张笑朱宏辉
Owner SHANGHAI ZENIX VACUUM COATING TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products