Myrica leaf extract, preparation method and application in cosmetics thereof
A technology for extracts and cosmetics, applied in the field of bayberry leaf extract and its preparation method and application in cosmetics, can solve the problems of unclear main components and specific functions of bayberry leaves, achieve improved comprehensive utilization rate, and simple extraction process , the effect of low production cost
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Embodiment 1
[0033] Embodiment 1: the preparation of bayberry leaf extract
[0034] Take fresh red bayberry leaves, pick out rotten ones, wash them with deionized water, dry them in an oven at 45°C, and then crush them through a No. 3 sieve to obtain dry red bayberry leaves powder. Weigh 55g of dry powder of red bayberry leaves, place it in a 2000mL round bottom flask, add 1.5L of 40% ethanol solution, heat and reflux for extraction at 65°C for 75min, cool to room temperature, filter, collect the filtrate, and obtain red bayberry leaf extract liquid, the flavonoid content in the obtained bayberry leaf extract is 1.64mg / mL, and the polysaccharide content is 4.64mg / mL.
[0035] Concentrate the bayberry leaf extract in vacuum at 45°C until it has no alcohol smell, then dissolve and dilute it with deionized water to a flavonoid content of 14.21mg / mL, filter, and apply AB-8 macroporous adsorption resin at a flow rate of 2mL / min. When the effluent has a color, it indicates that the adsorption o...
Embodiment 2
[0036] Embodiment 2: the preparation of bayberry leaf extract
[0037] Take fresh red bayberry leaves, pick out rotten ones, wash them with deionized water, dry them in an oven at 45°C, and then crush them through a No. 3 sieve to obtain dry red bayberry leaves powder. Weigh 30g of dried red bayberry leaf powder, place it in a 2000mL round-bottomed flask, add 1.5L of 80% ethanol solution, heat and reflux for extraction at 80°C for 30min, cool to room temperature, filter, collect the filtrate, and obtain red bayberry leaf extract solution, the flavonoid content in the obtained bayberry leaf extract is 3.05mg / mL, and the polysaccharide content is 3.84mg / mL.
[0038]Concentrate the bayberry leaf extract in vacuum at 45°C until it has no alcohol smell, then dissolve and dilute it with deionized water to a flavonoid content of 15.35mg / mL, filter, and apply AB-8 macroporous adsorption resin at a flow rate of 2mL / min. When the effluent has a color, it indicates that the adsorption o...
Embodiment 3
[0039] Embodiment 3: the preparation of bayberry leaf extract
[0040] Take fresh red bayberry leaves, pick out rotten ones, wash them with deionized water, dry them in an oven at 45°C, and then crush them through a No. 3 sieve to obtain dry red bayberry leaves powder. Weigh 55g of dried bayberry leaf powder, put it in a 1000mL round-bottomed flask, add 550mL of 60% ethanol solution, heat and extract at 40°C for 120min, cool to room temperature, filter, collect the filtrate, and repeat the extraction of the filter residue 3 times , combined four filtrates to obtain a bayberry leaf extract, the flavonoid content in the gained bayberry leaf extract was 1.52 mg / mL, and the polysaccharide content was 4.84 mg / mL.
[0041] Concentrate the bayberry leaf extract in vacuum at 45°C until there is no alcohol smell, then dissolve and dilute it with deionized water to a flavonoid content of 13.05mg / mL, filter, and apply AB-8 macroporous adsorption resin at a flow rate of 2mL / min. When the...
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