Preparation method of non-phosphorus pretreatment filming agent for circular cooling water treatment
A technology of circulating cooling water and pre-filming agent, applied in the direction of metal material coating process, etc., can solve the problems of small addition pollution and insignificant effect, and achieve the effect of reducing content, good pre-filming effect and small pollution.
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Example Embodiment
[0013] Example 1
[0014] (1) Prepare a mixed solution of calcium chloride and sodium polyacrylate, wherein the mass ratio of calcium chloride and sodium polyacrylate is 26:8;
[0015] (2) Prepare a mixed solution of zinc sulfate heptahydrate and sodium gluconate, where the mass ratio of zinc sulfate heptahydrate and sodium gluconate is 37:29;
[0016] (3) Mix the solution obtained in step (1) with the solution obtained in step (2) in a volume ratio of 1:1. The mixed solution contains four components: calcium chloride, sodium polyacrylate, zinc sulfate heptahydrate and sodium gluconate The total mass concentration is controlled at 1100mg / L, the pre-filming time is 48 hours at room temperature, and the pre-filming is completed.
[0017] Detected by the red dot method, the time for the hanging film to turn red is 32s.
Example Embodiment
[0018] Example 2
[0019] (1) Prepare a mixed solution of calcium chloride and sodium polyacrylate, where the mass ratio of calcium chloride and sodium polyacrylate is 26:8;
[0020] (2) Prepare a mixed solution of zinc sulfate heptahydrate and sodium gluconate, wherein the mass ratio of zinc sulfate heptahydrate and sodium gluconate is 47:19;
[0021] (3) Mix the solution obtained in step (1) with the solution obtained in step (2) in a volume ratio of 1:1, and the mixed solution contains four components: calcium chloride, sodium polyacrylate, zinc sulfate heptahydrate and sodium gluconate The total mass concentration is controlled at 1050mg / L, the pre-filming time is 48 hours at room temperature, and the pre-filming is completed.
[0022] Detected by the red dot method, the time for the hanging film to turn red is 29s.
Example Embodiment
[0023] Example 3
[0024] (1) Prepare a mixed solution of calcium chloride and sodium polyacrylate, where the mass ratio of calcium chloride and sodium polyacrylate is 33:10;
[0025] (2) Prepare a mixed solution of zinc sulfate heptahydrate and sodium gluconate, wherein the mass ratio of zinc sulfate heptahydrate and sodium gluconate is 40:17;
[0026] (3) Mix the solution obtained in step (1) with the solution obtained in step (2) in a volume ratio of 1:1. The mixed solution contains four components: calcium chloride, sodium polyacrylate, zinc sulfate heptahydrate and sodium gluconate The total mass concentration is controlled at 900mg / L, and the pre-filming time is 48 hours at room temperature, and the pre-filming is completed.
[0027] Detected by the red dot method, the time for the hanging film to turn red is 26s.
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