Wool fabric dyeing process of rhizoma dioscoreae cirrhosae extracting solution
A technology of extracting liquid and diospyross, applied in the field of wool fabric dyeing process, can solve the problems of poor color fastness to rubbing, light tone, hindering the diffusion of pigments, etc., and achieve the effect of improving color fastness to rubbing.
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Embodiment 1
[0019] The wool fabric dyeing process of the Ranunculus yam extract of embodiment 1 comprises the following steps:
[0020] S1: Take yam as raw material, wash, dry and crush to get yam powder, add 1000ml of deionized water and lower ketone mixed solution for every 50g of yam powder, heat the mixed system to reflux at 100°C 2h, filter, and the extracted dye stock solution is directly used for dyeing wool fabrics;
[0021] S2: Add 5g of sodium hydroxymethyl cellulose to 1000ml of dyeing liquor, adjust the pH of the dyeing liquor to 4 with an acidic pH value regulator, enter the dyeing at room temperature according to the bath ratio of 1:30, slowly raise the temperature of the dyeing liquor to 90°C, and keep it warm React for 50 minutes, cool down to 60°C, keep it warm for 1 hour, then cool down to room temperature, and the dyeing is over;
[0022] S3: The wool fabric is washed, soaped, washed, and dried at room temperature in sequence.
[0023] The heating rate in S2 is 2°C / mi...
Embodiment 2
[0026] The difference between embodiment 2 and embodiment 1 is:
[0027] S1: Add 1000ml of deionized water and a mixed solution of lower ketones for every 70g of yam powder, heat the mixed system to reflux at 100°C for 1 hour, filter, and use the extracted dye stock solution directly for dyeing wool fabrics;
[0028] S2: Add 10g sodium hydroxymethyl cellulose to 1000ml dyeing solution, adjust the pH value of the dyeing solution to 3 with an acidic pH regulator, and dye at room temperature according to the liquor ratio of 1:40, slowly raise the temperature of the dyeing solution to 80°C, and keep it warm React for 90 minutes, cool down to 55°C, keep it warm for 2 hours, then cool down to room temperature, and the dyeing is over;
[0029] The dye solution in S2 also contains a mordant; the mordant is tin chloride.
[0030] The content of mordant in the dyeing liquor is 2g / L.
[0031] The heating rate in S2 is 1.4°C / min, and the cooling rate when the temperature of the dye liqu...
Embodiment 3
[0034] The difference between embodiment 3 and embodiment 2 is:
[0035] S1: Add 1000ml of deionized water and a mixed solution of lower ketones for every 60g of yam powder, heat the mixed system to 100°C and reflux for 1.5h, filter, and the extracted dye stock solution is directly used for dyeing wool fabrics;
[0036] S2: Add 7g of sodium hydroxymethyl cellulose to 1000ml dyeing solution, adjust the pH value of the dyeing solution to 3.5 with an acidic pH value regulator, enter the dyeing at room temperature according to the bath ratio of 1:35, slowly raise the temperature of the dyeing solution to 85°C, and keep it warm React for 70 minutes, cool down to 57°C, keep it warm for 1.5 hours, then cool down to room temperature, and the dyeing is over;
[0037] The mordant is copper sulfate. The content of mordant in the dyeing liquor is 4g / L.
[0038] The heating rate in S2 was 1.7°C / min, and the cooling rate when the dye liquor temperature dropped to 57°C was 2.5°C / min.
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