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System and method for preparing deuterium-depleted water and deuterium-rich water by separating natural water

A technology of deuterium-depleted water and natural water, applied in the field of water treatment, can solve the problems of complicated control of parameters such as temperature and flow rate, lack of practical application value, low separation efficiency, etc., and achieves low-cost packing, simple structure and flexible operation. Effect

Active Publication Date: 2019-03-12
MATERIAL INST OF CHINA ACADEMY OF ENG PHYSICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the industrial application of the water / hydrogen dual-temperature exchange method has the following problems: on the one hand, the cooling tower must use expensive platinum-based hydrophobic catalysts as fillers, and the system construction cost is high; on the other hand, the exchange reaction of water / hydrogen isotopes Including two continuous processes of liquid-phase catalytic exchange and vapor-phase catalytic exchange, the control of parameters such as temperature and flow is more complicated
However, at present, the water separation research using the above-mentioned inorganic fillers only adopts the small-scale fixed bed carrier gas purging mode. After the bed penetrates, there is a large amount of water remaining in the molecular sieve filler, which requires complex regeneration treatment before it can be reused, and the separation efficiency is low. , has no practical application value

Method used

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  • System and method for preparing deuterium-depleted water and deuterium-rich water by separating natural water

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0036] The purpose of this embodiment is to provide a system for separating natural water to prepare deuterium-depleted water and deuterium-rich water, which not only helps to solve the problem of high cost of preparing deuterium-depleted water by the current distillation method and dual temperature exchange method, but also can be obtained at the same time Deuterium-rich water is used as a raw material for heavy water production.

[0037] A system for separating natural water to prepare deuterium-poor water and deuterium-rich water, such as figure 1 As shown, the system includes a sealed electric heating box, separation components arranged in the electric heating box, and a raw material water storage tank 3, a deuterium-rich water storage tank 4, a deuterium-depleted water storage tank 5 and a vacuum pump arranged outside the electric heating box. The electric heating box is a phenolic foam board box, and a dry-burning electric heating rod is arranged at the bottom of the electr...

example 1

[0052] Example 1: Single-cycle mode, preparation of deuterium-poor water with a deuterium concentration of 80ppm

[0053] The core component of the system for separating natural water to prepare deuterium-poor water and deuterium-rich water of the present invention is 8 separation columns (No. 1-8), and the separation columns are numbered (No. 1 → No. 2 →... → No. 8 → No. 1) The pipeline is connected end to end in turn to form a closed loop; the system also includes a raw water storage tank, a deuterium-rich water storage tank, a deuterium-depleted water storage tank, a metering pump, a vaporizer, a vacuum pump, and the pipes and valves connecting the above devices.

[0054] The separation column, metering pump, vaporizer, and the corresponding connecting pipes and valves are all placed in a sealed electric heating box. The box of the electric heating box is made of phenolic foam board; the bottom of the electric heating box is equipped with a dry-burning electric heating rod, and t...

example 2

[0066] Example 2: Double circulation mode, preparation of deuterium-poor water with a deuterium concentration of 30ppm

[0067] Follow the steps S1 to S4 of Example 1 to complete the first cycle separation;

[0068] Follow the steps S3 to S4 in Example 1 to complete the second cycle separation;

[0069] Then connect the deuterium-rich water storage tank pipeline, heat the No. 1 separation column, discharge the deuterium-rich water from the top of the column, the deuterium-rich water collection volume is about 160g, the deuterium concentration is about 410ppm; connect the deuterium-depleted water storage tank pipeline, and heat No. 7 separation column, drain deuterium-depleted water from the bottom of the column, the collected amount of deuterium-depleted water is about 340g, and the deuterium concentration is about 30ppm.

[0070] Sampling and analysis of the deuterium content of the water vapor in the No. 2 to No. 6 separation columns showed that the No. 4 separation column, which ha...

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Abstract

The invention discloses a system for preparing deuterium-depleted water and deuterium-rich water by separating natural water. A core of the system is provided with a closed loop, a plurality of separation columns are sequentially connected in an end-to-end manner to form the closed loop, the system further comprises a raw material water storage tank, a deuterium-rich water storage tank, a deuterium-depleted water storage tank, a metering pump, a carburetor, pipelines and valves, and the pipelines and the valves are connected with the devices. According to the system, separation is implementedby the aid of moving bed simulation principles, raw material water vapor circularly moves in the closed loop formed by the separation columns through sequentially heating and cooling of the separationcolumns and control of a one-way valve, a constantly increased deuterium concentration gradient is acquired along with increase of cycle number, the deuterium-rich water is extracted from the top ofthe separation column at the near end of a heating loop, and the deuterium-depleted water is extracted from the bottom of the separation column at the far end of the heating loop after certain times of heating and cooling circulation of the separation columns are implemented. The system is simple in structure, convenient to control, smaller in device size and lower in construction cost, fillers are low in cost, and the natural water can be directly separated by the aid of a semi-continuous mode to prepare the deuterium-depleted water and the deuterium-rich water.

Description

Technical field [0001] The invention relates to the technical field of water treatment, in particular to a system and method for separating natural water to prepare deuterium-poor water and deuterium-rich water. Background technique [0002] Deuterium-depleted water refers to water with a deuterium content of less than 150ppm. Tests by Hungarian scientist Gabor Somlyai and Kanagawa University Guan Bobo of Japan have proved that deuterium-depleted water has a variety of biological effects beneficial to the human body: activate human cells and enhance human immunity , Anti-cancer health care functions, etc. Deuterium-depleted water is currently an important auxiliary product combined with cancer treatment in the world. Some qualified countries in the world are committed to the research and development of deuterium-depleted water. For example, Japan, the United States, Romania, etc. have put products on the market in the field of cancer treatment. Has been leading the application. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B5/00C01B5/02C02F1/02B01D59/02
CPCB01D59/02C01B5/00C01B5/02C02F1/02
Inventor 姚勇文明邓立李佩龙陈军陈俊光陈闽陈克琳黄国强
Owner MATERIAL INST OF CHINA ACADEMY OF ENG PHYSICS
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