Preparation method for positive electrode material of lithium sulfur battery
A cathode material, lithium-sulfur battery technology, applied in battery electrodes, lithium storage batteries, non-aqueous electrolyte storage batteries, etc., can solve the problems of small output and complex preparation methods, and achieve improved conductivity, not easy to agglomerate, and excellent cycle stability. Effect
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[0034] Step 1: Preparation of ZIF-67@GO / CNTS composite:
[0035] 1455mg of Co(NO 3 ) 2 ·6H 2 O was added to the methanol solution of 125ml and stirred for 10min; the 2-methylimidazole of 1640mg was added to the methanol solution of 125ml and stirred for 10min, and the solution mixed with 2-methylimidazole was slowly poured into the still stirring Co ( NO 3 ) 2 ·6H 2O solution, stirred for 30min and then stood still. After 24 h the solution was centrifuged and dried. Graphene and carbon nanotubes were formulated into a mixed solution with a mass ratio of 1:1. The prepared ZIF-67 was added to the mixed solution with graphene and carbon nanotubes, and the ZIF-67@GO / CNTS composite was prepared by spray drying.
[0036] Step 2: Carbonization of ZIF-67@GO / CNTS composite:
[0037] The ZIF-67@GO / CNTS composite material prepared in the first step was placed in a porcelain boat, and then the porcelain boat was placed in a tube furnace, and the sample was heated at 350°C for 2h ...
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