Method for preparing and detecting ardisia mamillata extract
A detection method and a technology for Rhizoma Rhizoma Radix are applied in the field of preparation and detection of Rhizoma Radix Rhizoma extract, which can solve problems such as loss of effective components, and achieve the effects of simple steps, convenient operation and high content of saponins.
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Embodiment 1
[0031] (1) Take the fresh whole herb of Hutonghong, wash it, cut it into 2-4cm sections, add water of the same quality, place it in a homogenizer at 12000rpm for 3 minutes, and make a slurry;
[0032] (2) Add 20 times the volume of petroleum ether with a boiling range of 30-60°C to the slurry, extract at 50°C, separate the petroleum ether extraction components, concentrate the remaining slurry at 50°C and -0.085MPa to less than the weight of the original tiger tongue red, and obtain the infusion paste; the petroleum ether extract is condensed and recovered, which can be further used to separate the volatile oil;
[0033] (3) Add ethanol solution with a volume fraction of 70% to the extract, the solid-liquid ratio is 30mL / g, and the pressure is maintained at 200MPa for 8min;
[0034] (4) The extract obtained in step (3) is concentrated, put on a macroporous adsorption resin column, eluted with water, 30% ethanol, and 80% ethanol successively, collects the 80% ethanol eluate, co...
Embodiment 2
[0036] (1) Take the fresh whole herb of Hutonghong, wash it, cut it into 2-4cm sections, add water of the same quality, place it in a homogenizer at 6000rpm for 5 minutes, and make a slurry;
[0037] (2) Add 15 times the volume of petroleum ether with a boiling range of 30-60°C to the slurry, extract at 50°C, separate the petroleum ether extraction components, concentrate the remaining slurry at 40°C and -0.095MPa to less than the weight of the original tiger tongue red, and obtain the infusion paste; the petroleum ether extract is condensed and recovered, which can be further used to separate the volatile oil;
[0038] (3) Add an ethanol solution with a volume fraction of 60% to the extract, the solid-liquid ratio is 25mL / g, and the pressure is maintained at 100MPa for 10min;
[0039] (4) The extract obtained in step (3) is concentrated, put on a macroporous adsorption resin column, eluted with water, 30% ethanol, and 80% ethanol successively, collects the 80% ethanol eluate,...
Embodiment 3
[0041] (1) Take the fresh whole herb of Hutonghong, wash it, cut it into 2-4cm small pieces, add water of equal quality and place it in a homogenizer at 8000rpm for 4 minutes to make a slurry;
[0042] (2) Add 20 times the volume of petroleum ether with a boiling range of 30-60°C to the slurry, extract at 50°C, separate the petroleum ether extraction components, concentrate the remaining slurry at 45°C and -0.090MPa to less than the weight of the original tiger tongue red, and obtain the infusion paste; the petroleum ether extract is condensed and recovered, which can be further used to separate the volatile oil;
[0043] (3) Add an ethanol solution with a volume fraction of 65% to the extract, the solid-liquid ratio is 30mL / g, and the pressure is maintained at 150MPa for 9min;
[0044] (4) The extract obtained in step (3) is concentrated, put on a macroporous adsorption resin column, eluted with water, 30% ethanol, and 80% ethanol successively, collects the 80% ethanol eluate...
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