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A method for preparing high-basicity chromium-containing all-vanadium-titanium pellets by adding calcium carbonate

A calcium carbonate and high alkalinity technology, which is applied in the field of iron and steel metallurgy and ironmaking, can solve the problems of easy-to-explode ball formation, high reduction and pulverization rate, low ball formation efficiency, etc. Scrolling, high-speed effects

Active Publication Date: 2020-01-24
NORTHEASTERN UNIV LIAONING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] Based on the above reasons, the present invention proposes a method for adding calcium carbonate to prepare high-basic chromium-containing all-vanadium-titanium pellets, to overcome the traditional production method of acid pellets that is prone to occur in the process of producing alkaline pellets A series of technical problems, such as large amount of water absorption in the process of mineral powder and pelletizing, low pelletizing efficiency, easy bonding between cue balls, uneven composition, low pelleting rate caused by easy bursting after drying, and low pelleting rate after roasting. The compressive strength is lower than the blast furnace requirement and the reduction pulverization rate is high.

Method used

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  • A method for preparing high-basicity chromium-containing all-vanadium-titanium pellets by adding calcium carbonate
  • A method for preparing high-basicity chromium-containing all-vanadium-titanium pellets by adding calcium carbonate
  • A method for preparing high-basicity chromium-containing all-vanadium-titanium pellets by adding calcium carbonate

Examples

Experimental program
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Embodiment 1

[0072] This embodiment provides a method for preparing a high-alkalinity low-chromium full-vanadium-titanium pellet ore with low-chromium-type full-vanadium-titanium magnetite in the Hongge area as raw material ore, adding calcium carbonate and sodium bentonite. Described method comprises following implementation steps:

[0073] (1), raw material preparation: get the low-chromium type vanadium-titanium magnetite of 5Kg Hongge area as raw material ore, prepare analysis pure calcium carbonate powder 444.4g, sodium bentonite 50g as additive, and it is 1.9-2 to get alkalinity.

[0074] The X-ray diffraction pattern of the low-chromium vanadium-titanium magnetite in the Hongge area, such as figure 2 As shown, it contains the following composition and mass percentage: TiO 2 : 10wt%-12wt%, Cr 2 o 3 : 0.3wt%-0.6wt%, V 2 o 5 : 0.9wt%-1.4wt%, MgO: 2.5wt%-4wt%, CaO: 0.5wt%-1.0wt%, SiO 2 : 1wt%-3wt%; wherein, TFe is 53%-57wt%.

[0075] Taking 5Kg of raw material ore as a benchmark...

Embodiment 2

[0087] This embodiment provides a method for preparing a high-alkalinity low-chromium full-vanadium-titanium pellet ore with low-chromium-type full-vanadium-titanium magnetite in the Hongge area as raw material ore, adding calcium carbonate and sodium bentonite. Described method comprises following implementation steps:

[0088] (1), raw material preparation: take 4Kg low-chromium type vanadium-titanium magnetite in Hongge area as raw material ore, prepare and analyze pure calcium carbonate powder 360g, sodium-based bentonite 40g as additives, and prepare a mixture with an alkalinity of 1.9-2 .

[0089] The X-ray diffraction pattern of the low-chromium vanadium-titanium magnetite in the Hongge area, such as figure 2 As shown, it contains the following composition and mass percentage: TiO 2 : 10wt%-12wt%, Cr 2 o 3 : 0.3wt%-0.6wt%, V 2 o 5 : 0.9wt%-1.4wt%, MgO: 2.5wt%-4wt%, CaO: 0.5wt%-1.0wt%, SiO 2 : 1wt%-3wt%; wherein, TFe is 53%-57wt%.

[0090] Taking 4Kg of raw mate...

Embodiment 3

[0102] This embodiment provides a method for preparing a high-alkalinity low-chromium full-vanadium-titanium pellet ore with low-chromium-type full-vanadium-titanium magnetite in the Hongge area as raw material ore, adding calcium carbonate and sodium bentonite. Described method comprises following implementation steps:

[0103] (1), raw material preparation: take 5Kg Hongge area low chromium type vanadium titanium magnetite as raw material ore, prepare analysis pure calcium carbonate powder 464.6g, sodium base bentonite 50g as additives, mix the mixture that alkalinity is 1.8-1.9 material.

[0104] The X-ray diffraction pattern of the low-chromium vanadium-titanium magnetite in the Hongge area, such as figure 2 As shown, it contains the following composition and mass percentage: TiO 2 : 10wt%-12wt%, Cr 2 o 3 : 0.3wt%-0.6wt%, V 2 o 5 : 0.9wt%-1.4wt%, MgO: 2.5wt%-4wt%, CaO: 0.5wt%-1.0wt%, SiO 2 : 1wt%-3wt%; wherein, TFe is 53%-57wt%.

[0105] Taking 5Kg raw material or...

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Abstract

The invention relates to a method for preparing high alkalinity chromium-containing all-vanadium titanium pellets by adding calcium carbonate, which includes the steps: S1: Ingredients: adding calcium carbonate and sodium bentonite ingredients to the red grid chromium-containing vanadium titanium magnetite; S2: Divide the mixture into two parts. Add 3-4% of the mass of water to the first part and 6-8% of the mass of the material to the second part. Wet mix them separately and let them stand for stewing; S3 : Material separation and pelletizing: Make balls on the disc pelletizing machine at a speed of 30‑45r / min. The water spray volume is controlled at 1‑2ml / 10g of mineral material. The interval between adding water and materials is 30s‑100s; during the cue ball forming period, use the third One part of the mineral material is pelletized, and the second part of the mineral material is used for long-term pelletizing in the cue ball; S4: drying; S5: pre-roasting of calcium carbonate decomposition and pre-oxidation: first decompose calcium carbonate at 900℃-950℃ Pre-baking, and then introduce insufficient air into the furnace for pre-oxidation and pre-baking; S6: High-temperature oxidation consolidation roasting: Inject increasing amounts of air into the furnace at 1250℃-1300℃ for high-temperature oxidation consolidation roasting and sintering. After completion, it is cooled to obtain high alkalinity chromium-containing all-vanadium titanium pellets.

Description

technical field [0001] The invention belongs to the field of iron and steel metallurgy and ironmaking production, in particular to a method for preparing high-alkalinity chromium-containing all-vanadium-titanium pellets. Background technique [0002] Vanadium-titanium magnetite is a special magnetic iron ore in which iron, vanadium and titanium are symbiotic. Due to the symbiosis of iron and titanium, vanadium exists in titanium-magnetite in the same quality and shape, so it is called vanadium-titanium magnetite. . This kind of ore is distributed all over the world. Due to the differences in geological structure and ore-forming conditions, the characteristics of vanadium-titanium magnetite in various places are different. According to different types of vanadium-titanium magnetite, its smelting method and internal reaction properties of the smelting process There are also obvious differences. [0003] There are four major ore deposits in the vanadium-titanium-magnetite met...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22B1/243C22B1/16
CPCC22B1/16C22B1/2406C22B1/243
Inventor 薛向欣宋翰林高子先程功金黄壮杨合
Owner NORTHEASTERN UNIV LIAONING
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