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39results about How to "Slow water absorption" patented technology

Method for preparing microcapsulated superfine red phosphorus

The invention discloses a method for preparing micro-capsulized superfine red phosphorus, boiling the superfine red phosphorus with vitriol, sodium cyanide solution and sodium hydroxide solution, separately, filtering, eliminating impurities, and drying, and storing by sealing; blending and dissolve metal compound, depositing with ammonia, centrifuging and adding water to dilute, raising temperature, dropping in aluminum nitrate, vitriol or HCl and making metal hydroxide sol; mixing propylene acylamide monomers and N, Ní»-methylene dipropylene acylamide with ammonium persulphate, raising temperature and reacting to form high molecular network gel; adding the high molecular network gel into the metal hydroxide sol, raising the temperature and reacting to form high molecular network gel of metal hydroxide, mixing the high molecular network gel of metal hydroxide with the processed superfine red phosphorus, blending and placing still so that the sol takes the red phosphorus as the center to make surface absorption to form gel and coating a layer of colloid membrane on the red phosphorus surface, so as to obtain the micro-capsulized superfine red phosphorus. The advantages of the invention: it improves the stability, invariability and surface activity of the red phosphorus, improving processing property.
Owner:NANJING UNIV OF SCI & TECH

Preparation method of concrete internal curing agent

ActiveCN105439490AImprove early autogenous shrinkage reduction effectSolve the problem of early crackingChemical structureAfter treatment
The invention provides a preparation method of a concrete internal curing agent. The preparation method comprises the following steps: mixing acrylamide, a hydrophobic monomer, ethanol, a crosslinking agent and an initiating agent uniformly, heating until the temperature is 50-70 DEG C, then carrying out reaction for 4-10 hours, and carrying out conventional after treatment on a generated gel to obtain a shell material with a hydrophobic structure; mixing deionized water, acrylic acid and sodium hydroxide uniformly, controlling the neutralization temperature to be lower than 30 DEG C, then sequentially adding a crosslinking agent and an initiating agent, and mixing uniformly to obtain a core solution; and soaking the shell material with the hydrophobic structure in the core solution for 30-60 minutes, putting the shell material after filtration into a drying oven for reaction for 1-3 hours at 60-80 DEG C, and finally carrying out conventional after treatment to obtain the concrete internal curing agent. According to the preparation method, the preparation process is simple and convenient, the chemical structure is easy to control, an outer layer hydrophobic structure of the prepared internal curing agent enables the water absorbing rate to be relatively slow and can significantly reduce the influence of the water absorbing rate on the workability of concrete, and an inner layer hydrophilic structure can improve the early autogenous shrinkage reduction effect to solve the difficult problem of concrete early cracking.
Owner:JIANGSU SOBUTE NEW MATERIALS

Preparation method of fruit and vegetable crisps

The invention discloses a preparation method of fruit and vegetable crisps. The preparation method comprises the following steps of performing film painting treatment on fruit and vegetable blanks after being subjected to vacuum freezing and drying with a film painting solution which is prepared in advance, and performing drying after film painting, so as to obtain the fruit and vegetable crisps.Compared with the prior art, the preparation method has the beneficial effects that the method for performing film painting treatment on the fruit and vegetable blanks after being subjected to vacuumfreezing and drying is used, so that the effect of slowing the moisture absorption rate of the fruit and vegetable crisps can be realized; a film painting layer is used for packing the fruit and vegetable crisps, and the fruit and vegetable crisps are separated from air, so that moisture regain time is slow, the texture of the fruit and vegetable crisps is not liable to soften, and the texture ismaintained; and thereof, the shelf life of the frozen-fried fruit and vegetable crisps is prolonged. The fruit and vegetable crisps disclosed by the invention are subjected to film painting treatment,and film painting on the surface has the protective effect, so that the moisture absorption is not liable to cause, and the business application value of the frozen-dried fruits and vegetables is greatly increased.
Owner:SERICULTURE & AGRI FOOD RES INST GUANGDONG ACAD OF AGRI SCI

Black shale soluble salt extracting method

The invention discloses a black shale soluble salt extracting method which comprises the following steps: (1) preparing black shale into a centimeter-level block sample in any shape; (2) utilizing a vacuum drying box to dry the sample and weighing; (3) adding distilled water and an organic reducing agent acetone oxime into a container to make a water solution be in strong reducing environment (anEh value is lower than -200mV); (4) completely immersing the shale block sample into the water solution in the step (3) and utilizing an oxidizing and reducing potentiometer and a conductivity meter to respectively monitor the Eh value and conductivity of the water solution in real time; (5) controlling the adding amount of the acetone oxime in an extracting experiment process to make the water solution keep the strong reducing environment (the Eh value is smaller than -200mV); (6) obtaining an extracting solution containing the black shale soluble salt when a conductivity value of the water solution does not increase any more. By means of the black shale soluble salt extracting method disclosed by the invention, mineral oxidization and dissolution in a soluble salt extracting process areeffectively avoided, and the soluble salt is prevented from being lost in a sample preparing process; thus, accurate black shale soluble salt ion composition data can be obtained.
Owner:SOUTHWEST PETROLEUM UNIV

Chlorine dioxide slow-release particle sterilization disinfectant and preparation method thereof

The invention discloses a chlorine dioxide slow-release particle sterilization disinfectant and a preparation method thereof. The chlorine dioxide slow-release particle sterilization disinfectant is prepared from the following components in percentage by mass: 40% of self-made citric acid; 20% of sodium chlorite; 17.5% of a drying agent sodium chloride; 5% of sodium bicarbonate; 5% of a sustained-release agent sodium cyclamate; 2% of an activator; 0.1% of essence; 0.05% of a fluorine-containing surfactant; 10.35% of a filler sodium sulfate; the preparation method comprises the following steps:firstly, preparing citric acid, secondly, weighing the components, and uniformly mixing the weighed citric acid, activating agent, fluorine-containing active agent, filler sodium sulfate and drying agent sodium chloride to prepare a composite material for loading the acidifying agent on the adsorbent; and adding the weighed sustained-release agent sodium cyclamate into the prepared composite material to prepare a sustained-release agent carrier, finally, uniformly mixing the weighed sodium chlorite and sodium bicarbonate, adding the mixture into the sustained-release agent carrier, and uniformly mixing to obtain the product. The disinfectant has the advantages of uniform , low-speed and effective release of chlorine dioxide gas.
Owner:任建军

Concrete curing agent containing modified pina fibers as well as manufacturing method and application of concrete curing agent

The invention discloses a concrete curing agent containing modified pina fibers as well as a manufacturing method and application of the concrete curing agent. The concrete curing agent is prepared from the following components in percentage by mass: 25 percent to 32 percent of the modified pina fibers, 48 percent to 55 percent of styrene-acrylic emulsion, 2.3 percent to 2.7 percent of dibutyl diformate, 0.45 percent to 0.78 percent of a fluorocarbon modified polyacrylate leveling agent, 0.12 percent to 0.18 percent of an organic silicon de-foaming agent, 0.18 percent to 0.22 percent of tributyl phosphate and the balance of water, wherein the modified pina fibers are prepared from pina fibers, silica sol, concentrated hydrochloric acid, nano calcium oxide and vinyl trimethoxy silane. The concrete curing agent with high water retention rate and anti-cracking and shrinkage reducing effect is obtained through the following steps: taking the modified pina fibers and water which is one half of the mass of a formula amount at the ratios, and uniformly mixing to obtain a first mixed solution; weighing the other components at the ratios, and uniformly mixing to obtain a second mixed solution; combining the first mixed solution and the second mixed solution, and sufficiently and uniformly stirring to obtain the product.
Owner:安徽阳光水泥有限公司

Method of preparing high-alkalinity chromium-containing all-vanadium titaniferous pellets by adding calcium carbonate

ActiveCN109576490ASimple water absorption speedSlow water absorptionAlkalinitySodium Bentonite
The invention relates to a method of preparing high-alkalinity chromium-containing all-vanadium titaniferous pellets by adding calcium carbonate. The method comprises the following steps that S1, batching is performed, calcium carbonate and sodium-based bentonite ingredients are added into red-lattice chromium-containing vanadium titano-magnetite; S2, the mixture is divided into two parts, the first part of the mixture material is added with 3-4% of water by mass, the second part of the mixture material is added with the 6-8% of the water by mass, and wet mixing and leaving the materials to stand to ferment are performed correspondingly; and S3, material dividing and pelletizing are performed, pelletizing is performed on a disk pelletizer with revolving speed of 30-45 r / min, the water spraying amount is controlled to be 1-2 ml / 10 g of mineral aggregates, and the water adding and material feeding are performed per 30-100 seconds at intervals; the first part of mineral aggregates are used for pelletizing in the forming period of a master ball, and the second part of ore material aggregates are used for pelletizing in the growth period of the mother ball; S4, drying is performed; S5,the calcium carbonate is decomposed, pre-oxidated and pre-roasted, the calcium carbonate is decomposed and pre-roasted firstly at the temperature of 900-950 DEG C, and then insufficient amount of airis introduced into a furnace for pre-oxidation and pre-roasting; and S6, high-temperature oxidation consolidation roasting is performed, the incremental air is introduced into the furnace at the temperature of 1250-1300 DEG C to perform the high-temperature oxidation consolidation roasting, after sintering is completed, cooling is performed to prepare the high-alkalinity chromium-containing all-vanadium titaniferous pellets.
Owner:NORTHEASTERN UNIV LIAONING

A method for preparing high-basic chromium-vanadium-titanium pellets by using calcium oxide

ActiveCN109852791BGood for bonding into ballsHigh compressive strengthSodium BentoniteDry mixing
The invention relates to a method for preparing high-alkalinity chromium-containing vanadium-titanium pellets by adopting calcium oxide. The method comprises the following steps of mixing the raw materials including vanadium titano-magnetite, additive calcium oxide powder and sodium bentonite, so that the alkalinity of the raw materials is 1.8 to 2.1, drying and drying respectively, and carrying out dry mixing and mixing; averagely distributing the mixed ore materials into two parts, adding water accounting for 3% to 4% of the total mass of the raw materials in the first part, adding water with the total mass of 6% to 8% of the total mass of the raw materials in the second part, uniformly mixing, and hermetically standing; when pelletizing is carried out, a first part of mineral powder isused in the forming period of the master ball, a second part of mineral powder is used in the growth period of the master ball, the water spraying amount before the growth of the master ball is controlled to be 1ml of 10g of ore powder to 2ml of 10g of ore powder of mineral powder, preventing adhesion between the master balls, and adding water for 40 seconds to 90 seconds at each time, so that thediameter of the prepared pellets ranges from 8mm to 12mm; and preparing raw ball braised material, drying, pre-xidizing and roasting, carrying out secondary high-temperature oxidation roasting to obtain high-alkalinity chromium-containing vanadium-titanium pellets.
Owner:NORTHEASTERN UNIV LIAONING

Artificial cell membrane coating microcarrier for cell culture and preparation method thereof

The invention provides an artificial cell membrane coating microcarrier for cell culture and a preparation method thereof. The microcarrier provided by the invention takes konjac glucomannan microspheres as a matrix, and an artificial cell membrane coating microsphere is made by a biomimetic new material. The preparation method of the microcarrier comprises the following steps: respectively washing the matrix microspheres with petroleum ether and absolute ethyl alcohol, and drying for later use; dissolving 2-methacryloyloxyethyl phosphate choline (MPC) and n-butyl methacrylate in ethanol, polymerizing into an artificial cell membrane material under the effect of an initiator azodiisobutyronitrile (AIBN), diluting to 2 percent concentration for later use; adding the washed konjac glucomannan microspheres to an artificial cell membrane ethanol solution and soaking, and drying by a rotary evaporator in a vacuum, thus obtaining a microcarrier product. The artificial cell membrane materialcovers the surface of the microcarrier evenly and is connected firmly, has the advantages of avirulence, good cell adhesion, degradability, capability of easily eluting cells without adhesion, and thelike, the cost of the prepared microcarrier is low, the production process is simple, and the period is shorter, thus being beneficial for industrial production.
Owner:苏州怡彼得生物技术有限公司

A method for preparing self-fluxing pellets of medium-low alkalinity chromium-containing all-vanadium-titanium

ActiveCN109852790BSimple water absorption speedSlow water absorptionMagnetiteTitanium
The invention relates to a method for preparing medium-low-alkalinity chromium-containing all-vanadium-titanium self-fluxing pellets. The method comprises the following steps of S1, ingredient, addingcalcium carbonate and sodium-based bentonite into red-lattice chromium-containing vanadium titano-magnetite, and preparing a medium-low-alkalinity mixture; S2, wet-mixing and braising, adding water which does not exceed 7% of the mass of the mixture, and uniformly mixing; and then standing is carried out, so that the humidity is uniformly distributed; S3, pelletizing is carried out, wherein 30r to 40r per minute is used on a disc pelletizer, the water spraying amount in the forming period of the mother ball is controlled to be every 10 g is provided with1ml to 2ml of mineral materials, and fully rolling and compacting the ore materials, increasing the water spraying amount in the growth period of the mother balls to obtain the diameter of 6mm to 13mm; S4, drying the green pellets; S5, placing the green pellets in a furnace to be heated to 900 DEG c to 950 DEG c , and in the heat preservation condition, introducing insufficient amount of air into the furnace for pre-oxidation roasting,wherein the roasting time is 10minutes to 20minutes; S6, and carrying out high-temperature oxidation consolidation roasting, introducing the increment air into a furnace of 1250 DEG c to 1300 DEG c to increase the oxidizing atmosphere, carrying out high-temperature oxidation consolidation roasting, and then cooling to room temperature to prepare the medium-low-alkalinity chromium-containing all-vanadium-titanium self-fluxing pellet.
Owner:NORTHEASTERN UNIV LIAONING
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