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80results about How to "Reduced chance of reaction" patented technology

Equipment and method for removing light components through inert gas circulation gas stripping

The invention discloses equipment and method for removing light components through inert gas circulation gas stripping and relates to equipment and method which utilize gas stripping and steam condensation. The invention aims to provide equipment and method for removing light components through inert gas circulation gas stripping with the advantages of low cost and applicability to heat-sensitive materials. The equipment disclosed by the invention comprises a gas stripping tower, a light component collection tank, a heavy component collection tank, a demister, a first heater, a second heater, a first cooling device, a second cooling device, an ultralow temperature condenser, a circulating fan and a vacuum pump. The method disclosed by the invention comprises the following steps: heating inert gases; heating materials; carrying out gas stripping; cooling and collecting the light components and heavy components and recycling the inert gases. According to the equipment and method disclosed by the invention, local heating of the materials can be reduced, coking is avoided, and the reaction among the heat-sensitive materials is avoided; and moreover, the equipment can operate continuously and is suitable for large-scale industrial production. The equipment and method disclosed by the invention are applied to the separation field of organic matter monomers and intermediates, fine chemical engineering products, medicines, spices and the like.
Owner:TIANJIN AOZHAN XINGDA TECH

Method for preparing microcapsulated superfine red phosphorus

The invention discloses a method for preparing micro-capsulized superfine red phosphorus, boiling the superfine red phosphorus with vitriol, sodium cyanide solution and sodium hydroxide solution, separately, filtering, eliminating impurities, and drying, and storing by sealing; blending and dissolve metal compound, depositing with ammonia, centrifuging and adding water to dilute, raising temperature, dropping in aluminum nitrate, vitriol or HCl and making metal hydroxide sol; mixing propylene acylamide monomers and N, Ní»-methylene dipropylene acylamide with ammonium persulphate, raising temperature and reacting to form high molecular network gel; adding the high molecular network gel into the metal hydroxide sol, raising the temperature and reacting to form high molecular network gel of metal hydroxide, mixing the high molecular network gel of metal hydroxide with the processed superfine red phosphorus, blending and placing still so that the sol takes the red phosphorus as the center to make surface absorption to form gel and coating a layer of colloid membrane on the red phosphorus surface, so as to obtain the micro-capsulized superfine red phosphorus. The advantages of the invention: it improves the stability, invariability and surface activity of the red phosphorus, improving processing property.
Owner:NANJING UNIV OF SCI & TECH

Making method of fiber softening type areca seeds with prolonged quality guarantee period

The invention discloses a making method of fiber softening type areca seeds with prolonged quality guarantee period. The making method comprises the following steps of sorting raw materials, and performing cleaning; performing soaking treatment; performing corruption gas explosion treatment so that fibers are softened; performing vacuum seed germinating so as to improve the juice feeling when people chew areca seeds; roasting the seeds: performing vacuum drying; performing glue applying, and performing glue covering; performing seed cutting, and removing kernels; performing solidification withbrine, and performing airing; and performing packing and performing sterilization, so as to obtain the fiber softening type areca seeds with prolonged quality guarantee period. The invention aims toprovide the making method of the fiber softening type areca seeds with prolonged quality guarantee period. According to the making method, through steam explosion, on one hand, cellulose in the arecaseeds can be softened, the condition of enabling the areca seeds to be tasteful through fermentation liquid is facilitated, and on the other hand, the juice chewing feeling of the areca seeds can be improved in a focused manner; and besides, through vacuum seed germinating and seed roasting, the contact probability of the areca seeds and bacteria can be greatly reduced, and the quality guarantee period of products can be greatly prolonged to half a year or above.
Owner:湖南胖哥鑫鸿实业有限公司

Carbon raw material for carbon composite refractory material and preparation method thereof

The invention relates to a carbon raw material for a carbon composite refractory material and a preparation method thereof. The technical scheme comprises the following steps: firstly uniformly filling the bottom of a graphite crucible with a monatomic silicon powder, uniformly coating the monatomic silicon powder with graphite, carrying out thermal insulation at 1000-1400 DEG C in the atmosphere of argon or nitrogen for 1-4 hours, and taking out a substance which covers the monatomic silicon powder so as to prepare the carbon raw material for the carbon composite refractory material, wherein graphite is one of expandable graphite and graphene, and mass ratio of graphite to the monatomic silicon powder is (0.01-0.9):1. By adjusting the mass ratio of graphite to the monatomic silicon powder, in-situ preparation of different numbers and sizes of silicon carbide whiskers is realized on the edge of graphite. The prepared carbon raw material for the carbon composite refractory material has excellent resistance to oxidation, good dispersibility and excellent mechanical properties, is used in a carbon composite refractory material, and can be used to raise overall performance of a carbon composite refractory material and especially enhance mechanical properties and oxidation resistance of the carbon composite refractory material.
Owner:WUHAN UNIV OF SCI & TECH

Use method of self-generated gel for water plugging profile control and flooding

ActiveCN109779564AReduce calcium and magnesium ion contentImprove performanceFluid removalDrilling compositionCross-linkEconomic benefits
A use method of self-generated gel for water plugging profile control and displacement comprises the following steps: adding sodium alginate into a dispensing tank with wastewater under stirring to form the self-generated gel; adding a polymer in a water plugging profile control and flooding cross-linking system, and uniformly stirring; adding the rest components in the water plugging profile control and flooding cross-linking system 20-400 minutes before extrusion injection, then performing extrusion injection construction, enabling the self-generated gel and the water plugging profile control and flooding cross-linking system to form a mixed multiphase water plugging agent under stirring, and extruding the mixed multiphase water plugging agent into a well under the action of an injectionpump. Sodium alginate in the self-generated gel reacts with calcium and magnesium ions in wastewater to generate self-generated gel particles with very stable performance; therefore, the content of calcium and magnesium ions in the wastewater can be greatly reduced due to the generation of the self-generated gel particles, the concentration of the calcium and magnesium ions is greatly reduced dueto the generation of the self-generated gel particles, and the dissolving speed and viscosity of the polymer in a profile control and flooding system are improved. The investment cost of wastewater treatment can be greatly reduced, the yield increase range is increased, and economic benefits are obviously increased.
Owner:PETROCHINA CO LTD

Cleaning method of anode net of ionic membrane electrolysis bath

The invention discloses a cleaning method of an anode net of an ionic membrane electrolysis bath. Through the method, a compound scale layer on the surface of the anode net can be effectively removed, a surface coating of the anode net can be prevented from being damaged, and a voltage of the electrolysis bath can be lowered. The method includes the steps of carrying out pre-cleaning and leakage testing on a cleaning bath through pure water and placing the electrolysis bath into the cleaning bath after a cathode and an anode of the electrolysis bath are pressed by plastic membranes at an interval; preparing a primary cleaning agent through the pure water, heating the primary cleaning agent to 55-85 DEG C, then cleaning the anode net of the electrolysis bath for 1-4 hours, draining the primary cleaning agent and adding the pure water for flushing, wherein the primary cleaning agent is composed of 2-6% of hydrochloric acid and 0.2-0.3% of lan-826 corrosion inhibitors in concentration percentage; and preparing a secondary cleaning agent through the pure water, heating the secondary cleaning agent to 55-85 DEG C, then cleaning the anode net of the electrolysis bath for 4-6 hours, draining the secondary cleaning agent and adding the pure water for flushing, wherein the secondary cleaning agent is composed of 3-8% of citric acid, 0.2-0.35% of lan-826 corrosion inhibitors and 3-6% of sulfamic acid in concentration percentage.
Owner:PANZHIHUA STEEL ENTERPRISES XINYU CHEM

Method for preparing modified anode material of lithium ion battery

The preparation method for modified anode material in lithium ion cell comprises: (1) dispersing the metal salt or metal hydroxides into organic solvent, stirring at 80-90Deg, and adding LiCoO2 (LiNi(1-x)CoxO2, x=0.2 / 0.3) to form gel; (2) grinding the gel in tank for 4-8h; wherein, adding acetone, alcohol or mixed liquid by mass ratio as 10:1~20:1, and the mole measurement ratio of MyOz / LiCoO2(LiNi(1-x)CoxO2, x=0.2 / 0.3) as 0.01-0.05; (3) drying the grinded gel for 1-3h at 80-100Deg, and removing the organic solvent; (4) constant-temperature calcining the gel in muffle furnace for 6-12h at 400-600Deg, cooling naturally and obtaining the MyOzíñLiCoO2 (MyOzíñLiNixCo(1-x)O2, x=0.2 / 0.3). This invention improves the product cycle performance.
Owner:TIANJIN LISHEN BATTERY

Electronic device

An electronic device comprises: a fingerprint identification module; a protective cover plate comprising a protective layer and a protective layer, a decorative layer positioned on at least one surface of the protective layer; a first bonding layer located between the protective cover plate and the fingerprint identification module, so that the fingerprint identification module is attached to theprotective cover plate. The protective cover plate further comprises a second bonding layer, the second bonding layer is located between the decorative layer and the protective layer so as to achieveattachment of the decorative layer and the protective layer, and the elastic modulus of the second bonding layer is larger than that of the first bonding layer. And the connection strength between thedecorative layer and the second bonding layer is relatively high, so that the texture effect of the decorative layer can be kept, and the user experience is improved.
Owner:SHANGHAI OXI TECH

Preparation method of slate alkali reactivity restraining addition agent

The invention discloses a preparation method and a material using standards of a slate alkali reactivity restraining addition agent (FLSR-I). The addition agent is composed of mixing materials, ganister sands, nanometer SiO2, triethanolamine, a high-efficient plasticizing agent and an air entraining agent, the preparation method comprises accurately weighting dosage of the mixing materials, the ganister sands, the nanometer SiO2, the triethanolamine, the high-efficient plasticizing agent and the air entraining agent in proportion during preparation; sufficiently blending the mixing materials,the ganister sands, the nanometer SiO2, the high-efficient plasticizing agent and the air entraining agent, and manufacturing end products of the restraining addition agent by blending with the triethanolamine; and mixing in preparation of alkali reactive aggregate concrete in carious grades in proportion. The preparation method can effectively restrain reaction of slate alkali aggregate with expansion ratio between 0.2% to 0.5% and is obvious in restraining effect, simple and convenient in using method and free of needs of special construction control, thereby being capable of greatly lowering engineering using materials and transportation cost, and expanding material selecting range of the engineering using materials simultaneously.
Owner:CHINA RAILWAY NO 5 ENG GRP

Reactive emulsifier, water-borne epoxy resin emulsion, preparation and application

The invention belongs to the technical field of waterborne epoxy resin, and particularly relates to a reactive emulsifier, waterborne epoxy resin emulsion, preparation and application. Phenolic aldehyde amine generated by condensation reaction of cardanol, paraformaldehyde and micromolecular polyamine reacts with polyethylene glycol diglycidyl ether to obtain the reaction type emulsifier being ofan "amine-polyoxyethylene ether-amine" structure, which is terminated by the aldehyde group of the cardanol and has hydrophilic middle chain sections; then mixing the reactive emulsifier with water toform a nano-scale emulsion, and mixing the nano-scale emulsion with epoxy resin at a high speed to obtain the water-borne epoxy resin emulsion. The method is simple in technological process, safe tooperate, mild in reaction and low in production cost. The preparation method is simple and the prepared reactive emulsifier is good in emulsifying effect, so that the water-borne epoxy resin emulsionwith good stability is obtained under the condition that few hydrophilic components are introduced. The water-borne epoxy resin emulsion has excellent mechanical property, adhesion property, water resistance and corrosion resistance when used as a water-borne coating.
Owner:GUANGZHOU CHEM GROUTING CO LTD CAS

Single-component water-based outdoor top-coat varnish

ActiveCN103627280AReduced chance of reactionImprove chemical resistanceCoatingsSolventDefoaming Agents
The invention relates to a single-component water-based outdoor top-coat varnish. The single-component water-based outdoor top-coat varnish substantially consists of ingredients in percentage by weight: 75%-85% of water-based acrylic resin, 0.2%-0.4% of wetting agent, 0.3%-0.5% of defoaming agent, 6%-8% of cosolvent, 0.4%-0.6% of thickener, 0.1%-0.3% of preservative, 0.2%-0.4% of mould inhibitor, and 6%-15% of water. A layer of compact reticular thin film structure is formed on the surface in the film forming process by adopting water-based acrylic resin of self-crosslinked nanoscale polymer, the single-component water-based outdoor top-coat varnish has excellent hydrophobic performance, the contamination resistance and gloss retention of the product in outdoor use can be promoted, and the coating effect of the product in outdoor coating, protection and decoration materials can be improved.
Owner:GUANGDONG BADESE CHEM

Ceramic riser neck and sand mould structure capable of reducing defects of high-nickle nodular iron reaction layer

The invention discloses a ceramic riser neck and sand mould structure capable of reducing defects of a high-nickle nodular iron reaction layer. The ceramic riser neck and sand mould structure comprises a wet mould lower sand mould, a wet mould upper sand mould, a casting mould cavity formed in the interface of the wet mould lower sand mould and the wet mould upper sand mould and a cladding assembly arranged in the casting mould cavity and further comprises a casting assembly, wherein one end of the casting assembly is positioned at the interface of the wet mould lower sand mould and the wet mould upper sand mould and communicates with the casting mould cavity and a cladding mould cavity; the other end of the casting assembly stretches out of the wet mould upper sand mould; and the claddingassembly comprises a cladding shell mould, a cladding sand core and a heat insulating riser. According to the ceramic riser neck and sand mould structure, on the one hand, during pouring, wet mould sand moulds, a precoated sand cladding shell mould, a cladding sand core and a heat insulating riser sleeve react with iron liquid to generate plenty of turbulent flow oxidized gas, and the turbulent flow oxidized gas can be conveniently discharged out of a second exhausting rod to reduce the reaction probability of gas and Mg in the iron liquid; and on the other hand, a ceramic riser neck is arranged at the bottom of the heat insulating riser to prevent influence of the turbulent flow oxidized gas to nodularization of casting at the riser neck, so that generation of defects of the casting reaction layer at the high-nickle nodular iron riser neck is effectively reduced.
Owner:溧阳市联华机械制造有限公司

Vapor mixing device reducing NOx emission

The invention provides a vapor mixing device reducing NOx emission, aims at achieving the technical purpose of mixing atomized vapor with flames and reducing NOx emission of industrial fuel oil and fuel gas combustors and belongs to the technical field of emission reduction of the industrial fuel oil and fuel gas combustors. The vapor mixing device reducing NOx emission is characterized in that a plurality of spray guns are evenly arranged on the periphery of the outer side of a throat opening of a combustor; the spray guns and the axis of the throat opening of the combustor are arranged in the same direction in parallel; the ends, facing a hearth combustion chamber, of the spraying guns are provided with spray gun heads; and the tail ends of the spray guns are communicated with a high-pressure water / vapor pipeline. When the tail ends of the spray guns are connected with high-pressure water, the corresponding spray gun heads are mechanical atomization heads. When vapor exists in the pipeline, axial spraying through holes are formed in the middles of the corresponding spray gun heads. The mixing device is simple in structure, a combustor body does not need to be modified, running is stable, and the effect is obvious. As shown by a plurality of field test results, when gas is combusted, the NOx emission concentration can be reduced by 25%, and when oil is combusted, the NOx emission concentration can be reduced by 10-30%.
Owner:SHANGHAI WISEBOND TECH

Control method of boron content in refining process of acid slag produced in silicon killed steel production

The invention discloses a control method of boron content in the refining process of acid slag produced in silicon killed steel production. The control method includes the steps of firstly, molten steel is subjected bessemerizing and tapping, silicon iron and ferromanganese are added in the tapping process to perform deoxidization alloying, low-nitrogen carbon powder is added according to tappingcarbon content, a final slag modifier is added, and a tapping end point adopts slag-stopping tapping; secondly, after LF furnace slag temperature rise, 0.17-0.35kg of silicon iron is added into each ton of steel to perform slag top deoxidization; 2-4kg of lime is added into each ton of steel to produce high-alkalinity reducing slag, FeO and MnO in the slag is not more than 2.0%, and the alkalinityof the slag is not smaller than 2; thirdly, alloy is regulated according the components of refined molten steel, quartz sand is added to regulate the alkalinity to be not larger than 1.2, soft blow is performed for 15-20 minutes after slugging, and ferroboron is added to perform alloying; fourthly, argon stirring is performed for at least 5 minutes after the ferroboron is added, and delivering the molten steel out of a station. The control method has the advantages that boron alloying is performed in the refining late stage when O and N are stable, boron content fluctuation in the steel is controlled within 6ppm, boron yield is increased by 15%, and ferroboron adding quantity is reduced by 30%.
Owner:武汉钢铁有限公司

Coating method of lithium ion battery cathode material

The invention discloses a coating method of a lithium ion battery cathode material. According to the method, disk-nest grinding equipment is utilized to continuously input a lithium ion battery cathode material to be covered into a disk-nest grinder in a form of solid powder, solid powder is dispersed by an impeller and a disk which rotate at a high speed in a cavity of the disk-nest grinder, multiple nest type rotational flows are formed between the disk and a special lining plate, and air flow impact force between the disk and the special lining plate can fully disperse the solid powder; meanwhile, the rotation speed can be controlled to make a powder material keep morphology or be smashed; furthermore, a coating material can enter the disk-nest grinder in a form of solution or slurry ina mist spray mode and can evenly contact certain-temperature solid powder particles to be covered to finish coating. By means of the lithium ion battery cathode material coating method, a traditionalcoating technology for an existing lithium ion battery cathode material is greatly simplified, productivity is remarkably improved, a product coating effect is greatly improved, and cost is obviouslyreduced.
Owner:CENT SOUTH UNIV

Method for preparing Y2Ce2O7 transition layer thin film for superconduction coatings

The invention discloses a method for preparing Y2Ce2O7 transition layer thin film for superconduction coatings. The method includes the following steps: acetic acid yttrium, a first organic addition agent and methyl alcohol are mixed and blended to obtain a clear yttrium-contained solution; cerous nitrate, acetylacetone and propionic acid are mixed to obtain a clear cerium-contained solution; the obtained yttrium-contained solution and the obtained cerium-contained solution are mixed to obtain a first mixed solution, and methyl alcohol is added into the first mixed solution to obtain a precursor solution of the Y2Ce2O7 transition layer thin film; the Y2Ce2O7 transition layer thin film is coated on flexible nickel-tungsten alloy base bands through the adoption of the precursor solution of the Y2Ce2O7 transition layer thin film; after drying is conducted and 180 nm-250 nm ultraviolet irradiation is carried out, heat treatment is carried out in a first protective atmosphere, cooling is carried out in a second protective atmosphere, and the Y2Ce2O7 transition layer thin film is obtained from corresponding base sheets or the corresponding base bands. The method overcomes the defects that existing transition layer thin film is easy to crack, the surface is rough, and the texture degree is poor; YBCO superconduction thin film prepared on the basis of the transition layer is free of impurity phases, the good c-axis texture is achieved, and the application requirement of high temperature superconductor coating conductors is met.
Owner:JIANGSU HENGTONG PHOTOELECTRIC
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