The invention relates to a kettle residue
recovery process of
methyl carbamate, and belongs to the technical field of
chemical engineering, the kettle residue
recovery process of
methyl carbamate comprises the following steps: adding the kettle residue of
methyl carbamate into water, stirring for dissolving, adding
chloroform, extracting, standing for layering, taking an
oil phase dissolved with methyl
carbamate at the lower layer, cooling to
room temperature, filtering, washing, and
drying to obtain the methyl
carbamate.
Drying to constant weight to obtain recycled methyl
carbamate; and adjusting the pH value of an upper water phase composed of impurities such as
urea, biuret and triuret to 7.5-8 by using a pH
regulator, introducing into a sealed reaction tank filled with a modified mesoporous
molecular sieve, adsorbing at normal temperature and normal pressure, filtering, and treating the filtrate at 60-80 DEG C to obtain the recycled and treated
urea. The whole preparation process is simple and controllable, and the methyl carbamate and the
urea in the kettle residues of the methyl carbamate are recycled.