7results about How to "Reduce reactivity" patented technology

This application relates to the field of hydrosilylation, and in particular to a highly efficient catalyst for hydrosilylation reactions and its preparation method. This application provides a method for preparing a microcapsule-form catalyst, which first modifies methyl-terminated hydroxyl silicone oil with silazane, and then forms a microcapsule coating system with paraffin, thereby improving the release performance of the microcapsule coating system, so that the catalyst has low reactivity in the early stage of release, thereby improving the uniformity of the reaction process inside the silicone rubber, and thus improving the transparency and overall strength of the silicone rubber.

This invention discloses a method for microwave-catalyzed dehydrogenation of naphtha to produce aromatics, specifically comprising the following steps: Step 1, oxidizing and etching the surfaces of four different diameter carbon fibers to obtain four modified carbon fibers; Step 2, preparing four platinum-carbon fibers of different diameters based on the four modified carbon fibers obtained in Step 1; Step 3, preparing a gradient-pore structured platinum-carbon fiber paper based on the four different diameter platinum-carbon fibers obtained in Step 2; Step 4, using the gradient-pore structured platinum-carbon fiber paper obtained in Step 3 to catalyze the dehydrogenation of naphtha to obtain aromatics. This invention uses microwave-assisted catalysis to lower the reaction temperature, achieving localized catalytic heating to reduce side reactions, and also achieves high dehydrogenation efficiency.

This invention discloses a heterocyclic polyarylamide-polyhydroxyarylamide precipitated fiber, its preparation method, and a heterocyclic polyarylamide-polybenzodioxazole paper, belonging to the technical field of high-performance organic fiber and paper preparation. The preparation method of the precipitated fiber includes the following steps: A. Preparation of the polymerization solution: 3,3'-dihydroxybenzyl diamine (DHB) and 2-(4-aminophenyl)-5-aminobenzimidazole (DAPBI) are dissolved in an organic solvent containing a solubilizing salt, and then terephthaloyl chloride is added to react and obtain a polymer solution with a solid content of 1-10%; B. Precipitation: After degassing, filtering, metering, and spinning, the polymer solution is mixed with a coagulation bath and precipitated to obtain the heterocyclic polyarylamide-polyhydroxyarylamide precipitated fiber. A heterocyclic polyarylamide-polybenzodioxazole paper prepared from this precipitated fiber is also provided. This invention introduces a heterocyclic polyaromatic amide structure through copolymerization, which not only improves the strength and composite properties of the cyclized PBO paper, but also maintains a decomposition temperature comparable to that of pure PBO fiber, exceeding 600℃, demonstrating excellent thermal stability. Furthermore, this method is simple and easy to implement, making it suitable for industrial production applications.

This invention belongs to the field of heterocyclic pharmaceutical intermediate synthesis technology, specifically disclosing a method for synthesizing N-alkoxycarbonyl-4-amino-4-alkylpiperidine. Using N-alkoxycarbonylpiperidine-4-carboxylate as the starting material, the target product is obtained through a four-step reaction involving alkylation, hydrolysis, amidation, and Hoffmann rearrangement. This invention, through the adaptation and control of the substrate, synthetic route, and synthetic conditions, can solve the problems existing in the substrate-based synthetic route, thereby improving product yield and quality. The method described in this invention achieves a total yield of ≥60% of the target product, with key impurities all <0.1%. The process is safe and controllable, suitable for both laboratory-scale and industrial-scale production.

This invention provides an enhanced chlorine-resistant reverse osmosis membrane, comprising a base layer, a polyamide layer, and a polymeric protective layer. The polyamide layer is disposed on the base layer, and the polymeric protective layer is disposed on the polyamide layer. The polyamide layer is formed by interfacial polymerization of a diamine aqueous phase and a polyacrylamide oil phase. The solute in the diamine aqueous phase includes common amines and specific diamines, and the specific diamine includes at least one selected from 2-methyl-p-phenylenediamine, 4-methyl-1,3-phenylenediamine, 2,6-diaminotoluene, and 2,4,6-trimethyl-1,3-phenylenediamine. The polymeric protective layer is connected to the surface of the polyamide layer through polyaldehyde molecules. This invention, through the combination of the base layer, the polyamide layer, and the polymeric protective layer, enables the enhanced chlorine-resistant reverse osmosis membrane to achieve both a high desalination rate and excellent chlorine resistance.

This application discloses a cathode material, its preparation method, and an all-solid-state battery. It includes a substrate and a first coating layer and a second coating layer sequentially coated on the surface of the substrate. The substrate is a phosphorus-doped spinel-type lithium nickel manganese oxide. The first coating layer includes an oxygen-doped halide electrolyte. The second coating layer includes an Sb / O co-doped argentite-germanium sulfide. The cathode material provided by this application has the advantage of synergistically improved structural stability, interfacial stability, and air stability.

The invention provides a novel process route for preparing perfluorohexane (C6F14), and the preparation method comprises the following steps: diluting fluorine gas with inert gas to obtain first mixed gas, and mixing hexafluoropropylene dimer (C6F12) with perfluorinated liquid to obtain first mixed liquid; the first mixed gas and the first mixed solution are treated through a microchannel reactor and then transferred into a reaction kettle, a product in the reaction kettle is collected, the product is separated, and the crude perfluorohexane product is obtained. The problems that in the prior art, the C6F14 preparation process is complex, and the conversion rate is low are solved. On the other hand, the invention discloses a purification method for obtaining a high-purity C6F14 finished product. The conversion rate and the purity of the perfluorohexane obtained by the scheme of the invention are obviously improved.