The present invention comprises: a method for preparing nanocrystals; ITO nanocrystals and a core-shell-structured FITO as products using same; and a method for preparing and depositing FITO nanocrystals that can be deposited in a single layer. According to the present invention, the method for preparing ITO nanocrystals comprises a step of highly-efficiently preparing ITO nanocrystals by using a mixture comprising
indium acetate and a
tin compound, and a method for preparing a core-shell-structured FITO coats FITO core particles with
indium, thereby producing stable FITO nanocrystals having high durability even in extreme environments. In addition, the method for depositing FITO comprises injecting FITO on a polar solution so as to implement uniform
monolayer deposition through phase separation and self-
assembly, thereby enabling precise fine patterning. Therefore, the present invention efficiently produces a high-performance nanomaterial, thereby providing a technical
advantage suitable for various industrial applications such as smart windows, highly durable materials and precision electronic and optical devices.