A kind of hot-melt pressure-sensitive adhesive for toilet gasket and preparation method thereof
A hot-melt pressure-sensitive adhesive and gasket technology, used in adhesives, adhesive types, mineral oil-hydrocarbon copolymer adhesives, etc., can solve problems affecting the use experience, and achieve excellent user experience and excellent cohesive strength. , the effect of excellent coating performance
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[0057] A second aspect of the present invention provides a method for preparing a hot-melt pressure-sensitive adhesive for a toilet gasket, the steps comprising:
[0058] (1) drop described naphthenic oil, antioxidant into stainless steel reactor;
[0059] (2) After the temperature rises to 140°C, add SBR rubber, and control the temperature of the reactor at 150°C;
[0060] (3) After the SBR rubber is completely dissolved, put in hydrogenated C5 / C9 copolymerized petroleum resin, modified aromatic C9 petroleum resin, styrene-acrylate, control the temperature of the stainless steel reactor within 200°C and stir for 30-60min, then vacuumize To -0.085MPa, the material is cooled and packaged.
Embodiment 1
[0064] Example 1 provides a hot-melt pressure-sensitive adhesive for toilet gaskets, including the following components: 8 parts of hydrogenated C5 / C9 copolymerized petroleum resin, 20 parts of modified aromatic C9 petroleum resin, 3 parts of styrene-acrylate, SBR 22 parts of rubber, 10 parts of naphthenic oil, 0.5 parts of antioxidant.
[0065] The hydrogenated C5 / C9 copolymerized petroleum resin is commercially available from Kolon, Korea, with the brand name SU-400.
[0066] The modified aromatic C9 petroleum resin is a product commercially available from Eastman Chemical, USA under the brand name of PiccoAR85.
[0067] The styrene-acrylic acid salt is styrene-acrylic acid sodium salt, and the preparation steps include:
[0068] (1): Add a certain amount of initiator azobisisobutylcyanide (AIBN), monomer styrene and acrylic acid in a four-necked flask, use benzene as a solvent, pass nitrogen to remove oxygen for 30 minutes, and then heat in a water bath at a temperature of...
Embodiment 2
[0080] Example 2 provides a hot-melt pressure-sensitive adhesive for toilet gaskets, including the following components: 15 parts of hydrogenated C5 / C9 copolymerized petroleum resin, 25 parts of modified aromatic C9 petroleum resin, 5 parts of styrene-acrylate, SBR 30 parts of rubber, 20 parts of naphthenic oil, 1 part of antioxidant.
[0081] The hydrogenated C5 / C9 copolymerized petroleum resin is commercially available from Kolon, Korea, with the brand name SU-400.
[0082] The modified aromatic C9 petroleum resin is a product commercially available from Eastman Chemical, USA under the brand name of PiccoAR85.
[0083] The styrene-acrylic acid salt is styrene-acrylic acid sodium salt, and the preparation steps include:
[0084] (1): Add a certain amount of initiator azobisisobutylcyanide (AIBN), monomer styrene and acrylic acid in a four-necked flask, use benzene as a solvent, pass nitrogen to remove oxygen for 30 minutes, and then heat in a water bath at a temperature of ...
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