Compound and organic photoelectric device, image sensor and electronic device including the same
A technology of compounds and chemical formulas, which can be used in electric solid devices, silicon organic compounds, germanium organic compounds, etc., and can solve the problems of small absorption area and deterioration of sensitivity.
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Embodiment 1
[0459] Synthesis Example 1: Compound (2-((5-(10H-phenoselenazin-10-yl)tellphen-2-yl)methylene)-1H-indene-1,3 represented by Chemical Formula 1-1 (2H)-Diketone) Synthesis
[0460] [chemical formula 1-1]
[0461]
[0462] [Reaction Scheme 1-1]
[0463]
[0464] (i) Synthesis of compound (1)
[0465] Synthesized with reference to methods disclosed in Efficient Synthesis of 2-Iodo and 2-Dicyanomethyl Derivatives of Thiophene, Selenophene, Tellurophene and Thieno[3,2-b]thiophene, Takahashi, K.; Tarutani, S.Heterocycles 1996,43,1927-1935 2-Iodotellphene.
[0466] (ii) Synthesis of compound (2)
[0467] 10.0g (32.7mmol) of 2-iodotellphene and 6.17g (25.2mmol) of 10H-phenoselenazine in 100ml of anhydrous toluene in 5 mol% of Pd (dba) 2 , 5 mol% P(tBu) 3 , and 2.66 g (27.7 mmol) of NaOtBu were heated and refluxed. The product therefrom was isolated and purified by silica gel column chromatography (toluene:hexane in a volume ratio of 1:4) to obtain 4.25 g of 10-(tellphen-2-...
Embodiment 2 to 7
[0650] Examples 2 to 7: Fabrication of Optoelectronic Devices
[0651] Photoelectric devices according to Examples 2 to 7 were manufactured according to the same method as in Example 1, except that the compounds according to Synthesis Examples 2 to 7 were used instead of the compounds according to Synthesis Example 1, respectively.
[0652] Reference Examples 1 to 5: Fabrication of Optoelectronic Devices
[0653] Photoelectric devices according to Reference Examples 1 to 5 were manufactured according to the same method as in Example 1, except that the compounds according to Synthesis Reference Examples 1 to 5 were used instead of the compounds according to Synthesis Example 1, respectively.
[0654] Evaluation 3: Light Absorption Characteristics of Optoelectronic Devices
[0655] The photoelectric devices according to Examples 1 to 7 and Reference Examples 1 to 5 were evaluated for light absorption characteristics in the ultraviolet-visible (UV-Vis) region using a Cary 5000...
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