A kind of catalyst composition and application
A composition and catalyst technology, applied in the direction of hydrocarbons, hydrocarbons, physical/chemical process catalysts, etc., can solve problems affecting catalysts, product quality, aromatics residues, etc., and achieve high oligomerization activity and strong applicability , running smoothly
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Embodiment 1
[0048] Under the protection of nitrogen, slowly add 7 mmol of water dropwise to 10 mmol of triisobutylaluminum (1M toluene solution) in an ice bath, stir and react for 0.5 hours, then raise the temperature and reflux for 1 hour, then lower it to room temperature for later use; take 10 mmol of methyl aluminum oxide Alkane (1M toluene solution) was added to the above solution, then heated to reflux for 1 hour, and then lowered to room temperature; 2 mmol of water was slowly added to the above mixed solution in an ice bath, and after stirring for 0.5 hours, heated to reflux for 1 hour, and then Cool down to room temperature, remove the toluene solvent under reduced pressure, then add methylcyclohexane solvent, the total volume of the mixed solution is 20mL, and obtain cocatalyst A (1M, methylcyclohexane solution).
[0049] Product analysis: take the quantitative cocatalyst A, slowly add excess water to decompose it, the aluminum content of the liquid phase component is 3.4wt% by I...
Embodiment 2
[0051] Under the protection of nitrogen, slowly add 5 mmol of water dropwise to 10 mmol of triisobutylaluminum (1M toluene solution) in an ice bath, stir and react for 0.5 hours, then raise the temperature and reflux for 1 hour, then lower it to room temperature for later use; take 10 mmol of methyl aluminum oxide Alkane (1M toluene solution) was added to the above solution, then heated to reflux for 1 hour, and then lowered to room temperature; 2 mmol of water was slowly added to the above mixed solution in an ice bath, and after stirring for 0.5 hours, heated to reflux for 1 hour, and then Cool down to room temperature, remove the toluene solvent under reduced pressure, then add methylcyclohexane solvent, the total volume of the mixed solution is 20mL, and obtain cocatalyst B (1M, methylcyclohexane solution).
[0052] Product analysis: get quantitative (with embodiment 1) cocatalyst B, slowly add excessive water and make it decompose, liquid phase component is 3.4wt% with ICP...
Embodiment 3
[0054] Under the protection of nitrogen, slowly add 10 mmol of water dropwise to 10 mmol of triisobutylaluminum (1M toluene solution) in an ice bath, stir and react for 0.5 hours, then raise the temperature and reflux for 1 hour, and then lower it to room temperature for later use; take 10 mmol of methyl aluminum oxide Alkane (1M toluene solution) was added to the above solution, then heated to reflux for 1 hour, and then lowered to room temperature; 2 mmol of water was slowly added to the above mixed solution in an ice bath, and after stirring for 0.5 hours, heated to reflux for 1 hour, and then Cool down to room temperature, remove the toluene solvent under reduced pressure, then add methylcyclohexane solvent, the total volume of the mixed solution is 20mL, and obtain cocatalyst C (1M, methylcyclohexane solution).
[0055] Product analysis: get quantitative (with embodiment 1) cocatalyst C, slowly add excessive water and make it decompose, liquid phase component is 3.4wt% wit...
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