Ultrathin bipolar plate for vanadium battery, and preparation method of ultrathin bipolar plate
A bipolar plate, vanadium battery technology, applied in fuel cells, regenerative fuel cells, circuits, etc., can solve the problems of low cross-sectional conductivity and thick thickness, and achieve the effects of thin thickness, improved energy density, and fewer operating units
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Embodiment 1
[0084] (1) Preparation of ultra-thin bipolar plates
[0085] 1) Select graphite flakes with an average particle size of 0.1 μm, add them to deionized water, and vigorously stir at 500 rpm. After 6 hours, a uniformly distributed conductive functional material spraying solution with a solid content of 35% is obtained.
[0086] 2) The polyethylene film with a thickness of 40 μm was washed repeatedly in excess absolute ethanol, and dried at 60° C. for later use.
[0087] 3) Further adopting a pressure of 1.5MPa, spray the conductive functional material spray liquid prepared in the above step 1) on both sides of the film respectively, the spray thickness is 300 μm, and the mass ratio of conductive functional material to film resin is 2:1.
[0088] 4) Put the film resin attached with the conductive functional material prepared in the above step 3) into a mold, hot press at 160° C. and 55 MPa for 20 minutes, and cool naturally to obtain the ultra-thin bipolar plate of the present inv...
Embodiment 2
[0096] (1) Preparation of ultra-thin bipolar plates
[0097] 1) Select graphene with an average thickness of 45nm and a plane size of 0.5×2 μm, add it to absolute ethanol, and vigorously stir at 300 rpm. After 12 hours, a uniformly distributed spray solution with a solid content of 50% is obtained.
[0098] 2) The polypropylene film with a thickness of 15 μm was washed repeatedly in excess deionized water, and dried at 80° C. for later use.
[0099] 3) Further adopting a pressure of 3.2MPa, spray the conductive functional material spraying liquid prepared in the above step 1) on both sides of the film respectively, the spraying thickness is 100 μm, and the mass ratio of conductive functional material to film resin is 1:1.
[0100] 4) Put the film resin attached with the conductive functional material prepared in the above step 3) into a mold, hot press at 200°C and 120MPa for 10min, and cool naturally to obtain the ultra-thin bipolar plate of the present invention.
[0101] (...
Embodiment 3
[0108] (1) Preparation of ultra-thin bipolar plates
[0109] 1) Select carbon fibers with an average diameter of 0.1 μm and a length of 5 μm, add them to acetone, and vigorously stir at 500 rpm to obtain a uniformly distributed spray solution with a solid content of 5% after 6 hours.
[0110] 2) The polystyrene film with a thickness of 115 μm was washed repeatedly in excess absolute ethanol, and dried at 70° C. for later use.
[0111] 3) Further adopting a pressure of 4 MPa, spray the conductive functional material spray liquid prepared in the above step 1) on both sides of the film respectively, the spray thickness is 1500 μm, and the mass ratio of conductive functional material to film resin is 5:1.
[0112] 4) Put the film resin attached with the conductive functional material prepared in the above step 3) into a mold, hot press at 180° C. and 40 MPa for 20 minutes, and cool naturally to obtain the ultra-thin bipolar plate of the present invention.
[0113] (2) Performance...
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