Preparation method of poplar catkin/biomass fiber composite thermal insulation material

A composite thermal insulation material and biomass fiber technology, which is applied in the field of building thermal insulation materials, can solve the problems of reduced flexibility of poplar fiber, reduced thermal insulation performance of composite materials, inability to form, etc., and achieves broad application prospects, improved thermal insulation performance, and reduced production. cost effect

Active Publication Date: 2019-06-28
CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Liu Juan and others attached poplar fiber to the surface of polypropylene filament, and prepared poplar/polypropylene nonwoven insulation material by spunbonding method (Liu Juan, Xu Zhenglin, Zeng Beini, etc., Morphology Analysis of Poplar Fiber and the preparation and characterization of thermal insulation materials, Wuhan Textile University Journal, 2016, 29, 3: 3-7), the thermal insulation performance of the prepared composite fabric has been significantly improved, and the problem that poplar fiber is short and cannot be formed can be used as The wadding material is used in the thermal insulation field, but due to manual laying, the poplar wadding fiber uniformity is poor in this method, and the mechanical properties of the composite material vary greatly.
[0007] The Chinese invention patent with the publication number CN107488910 A discloses a composite insulation material prepared from poplar fiber, polypropylene fiber and cotton fiber at a ratio of 9:6:4. The blended fiber greatly strengthens the gap between the poplar fiber The cohesion force of the material improves the thermal insulation performance and air permeability of the material, but this method leads to a decrease in the flexibility of the poplar fiber and a significant increase in the

Method used

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Examples

Experimental program
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Effect test

Embodiment 1

[0041] The embodiment of the present invention provides a preparation method of poplar catkin / bamboo parenchyma cell-derived microfibrillated cellulose composite thermal insulation material.

[0042] 1. Raw materials: poplar fiber, bamboo parenchyma cells.

[0043] 2. The specific process steps are as follows:

[0044] S1. Sieve the bamboo after crushing, collect the material passing through the standard 30-60 mesh screen, add deionized water 20 times the volume of the material, stir and let it stand, and collect the floating matter in the upper layer to be parenchyma cells;

[0045]S2, take 10g of parenchyma cells and join in phenylethanol solution (volume ratio 2:1) and extract for 6 hours, and collect the precipitated part, and parenchyma cells are added in 1wt% acidified sodium chlorite solution (pH value 2-4) react at 75°C for 6 hours, wherein the acidified sodium chlorite with the same concentration is changed every 1 hour, and then the parenchyma cells are treated with...

Embodiment 2

[0052] The embodiment of the present invention provides a preparation method of poplar floc / bamboo fiber source microfibrillated cellulose composite thermal insulation material.

[0053] 1. Raw materials: poplar fiber, bamboo fiber.

[0054] 2. The specific process steps are as follows:

[0055] S1. Sieve the bamboo after crushing, collect the material passing through the standard 30-60 mesh screen, add deionized water 20 times the volume of the material, stir and let it stand, and collect the lower sediment as fiber;

[0056] S2, take 10g of parenchyma cells and join in phenylethanol solution (volume ratio 2:1) and extract for 6 hours, and collect the precipitated part, and parenchyma cells are added in 1wt% acidified sodium chlorite solution (pH value 2-4) Reaction at 75°C for 8 hours, wherein the acidified sodium chlorite with the same concentration was changed every 1 hour, and then the treated thin-walled Cells were treated at 90°C for 2 hours each, and finally added to...

Embodiment 3

[0063] The embodiment of the present invention provides a preparation method of poplar catkin / bamboo parenchyma cell-derived microfibrillated cellulose composite thermal insulation material.

[0064] 1. Raw materials: poplar fiber, bamboo parenchyma cells.

[0065] 2. The specific process steps are as follows:

[0066] S1. Sieve the bamboo after crushing, collect the material passing through the standard 30-60 mesh screen, add deionized water 20 times the volume of the material, stir and let it stand, and collect the floating matter in the upper layer to be parenchyma cells;

[0067] S2, take 10g of parenchyma cells and join in phenylethanol solution (volume ratio 2:1) and extract for 6 hours, and collect the precipitated part, and parenchyma cells are added in 1wt% acidified sodium chlorite solution (pH value 2-4) Reaction at 75°C for 6 hours, wherein the acidified sodium chlorite with the same concentration was changed every 1 hour, and then the treated thin-walled Cells w...

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Abstract

The invention discloses a preparation method of a poplar catkin/biomass fiber composite thermal insulation material. The preparation method comprises the steps of degreasing the poplar catkin so as toobtain degreased poplar catkin, simultaneously preprocessing biomass fibers so as to obtain fuzz fiber sol, controlling the raw material mass ratios of poplar catkin to fuzz fibers at 10:1-4, addingthe degreased poplar catkin into the diluted fuzz fiber sol, uniformly stirring to obtain degreased poplar catkin/fuzz fiber mixed liquid, discharging the residual diluent, and sequentially carrying out pre-freezing and vacuum freezing drying. According to the provided preparation method, different composite thermal insulation materials with different pore structures and different thickness are prepared by changing the contents and pre-freezing temperatures of the poplar catkin and the biomass fibers; the adopted poplar catkin is wide in source and low in cost, and the fuzz fibers obtained through the preprocessing of the biomass fibers can be of a three-dimensional net structure, so that the thermal insulation property of the composite thermal insulation material is improved; and the method is simple in process, low in preparation energy consumption, low in cost and wide in practical application prospects.

Description

technical field [0001] The invention belongs to the technical field of building thermal insulation materials, and in particular relates to a preparation method of a poplar catkin / biomass fiber composite thermal insulation material. Background technique [0002] Insulation materials are an important means to reduce building energy consumption and greenhouse gas emissions. With the increasingly serious problem of global warming, the application of insulation materials is becoming more and more important. Traditional insulation materials include polystyrene, polyurethane, cork, mineral wool, melamine, etc.; super insulation materials include vacuum panels, airgel, vacuum glass, etc. [0003] Traditional thermal insulation materials are widely used due to their low cost and simple preparation process, but the thickness of traditional thermal insulation materials is relatively thick, which increases the complexity of the building structure, and is not environmentally friendly, an...

Claims

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Application Information

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IPC IPC(8): C08L99/00C08L1/02
Inventor 黄汉霄喻云水张晓凤王汉坤黎静
Owner CENTRAL SOUTH UNIVERSITY OF FORESTRY AND TECHNOLOGY
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