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Preparation method of copper hydroxide nanobelt oriented film

An oriented film and copper hydroxide technology, applied in the field of nanomaterials, can solve problems such as limiting versatility, and achieve the effects of good orientation, low cost and simple operation

Inactive Publication Date: 2019-07-12
FUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although high-quality oriented films can be obtained by these methods, they require high-energy processes and unique substrates, which limit the versatility of material selection

Method used

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  • Preparation method of copper hydroxide nanobelt oriented film
  • Preparation method of copper hydroxide nanobelt oriented film
  • Preparation method of copper hydroxide nanobelt oriented film

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] (1) Dissolve 0.005mol of cuprous nitrate trihydrate in deionized aqueous solution, add 5mL of polyethylene glycol, and after uniform dissolution, add 2g of sodium hydroxide particles into the mixed solution.

[0026] (2) The reaction was stirred at room temperature for 4h to form a blue suspension.

[0027] (3) Wash with distilled water and absolute ethanol several times in a centrifuge to remove impurities;

[0028] (4) Dissolving the substance obtained above in a high-purity ethanol solution to obtain the copper hydroxide precursor solution.

[0029] (5) Take 1 mL of the solution of (4) with a concentration of 5 mol / mL, and inject it into the aqueous solution at a rate of 200 μL / min with a syringe to form an oriented film, transfer the film to the substrate, and place it in a vacuum oven at 40 °C after the transfer drying to obtain the copper hydroxide nanoribbon oriented film.

[0030] The schematic diagram of the copper hydroxide nanobelt oriented film prepared in...

Embodiment 2

[0032] (1) Dissolve 0.005mol of cuprous nitrate trihydrate in deionized aqueous solution, add 5mL of polyethylene glycol, and after uniform dissolution, add 2g of sodium hydroxide particles into the mixed solution.

[0033] (2) The reaction was stirred at room temperature for 4h to form a blue suspension.

[0034] (3) Wash with distilled water and absolute ethanol several times in a centrifuge to remove impurities;

[0035] (4) Dissolving the substance obtained above in a high-purity ethanol solution to obtain the copper hydroxide precursor solution.

[0036] (5) Take 1 mL of the solution of (4) with a concentration of 5 mol / mL, and inject it into the aqueous solution with a syringe at a speed of 600 μL / min to form an oriented film, transfer the film to the substrate, and place it in a vacuum oven at 40 °C after the transfer Drying, copper hydroxide nanoribbon oriented film.

[0037] In this example, the solution of (4) was injected into the liquid phase at a speed of 600 μL...

Embodiment 3

[0039] (1) Dissolve 0.005mol of cuprous nitrate trihydrate in deionized aqueous solution, add 5mL of polyethylene glycol, and after it is uniformly dissolved, add 2g of sodium hydroxide particles into the mixed solution.

[0040] (2) The reaction was stirred at room temperature for 4h to form a blue suspension.

[0041] (3) Wash with distilled water and absolute ethanol several times in a centrifuge to remove impurities;

[0042] (4) Dissolving the substance obtained above in a high-purity ethanol solution to obtain the copper hydroxide precursor solution.

[0043](5) Take 1 mL of the solution of (4) with a concentration of 5 mol / mL, and inject it into the aqueous solution with a syringe at a speed of 1000 μL / min to form an oriented film, transfer the film to the substrate, and place it in a vacuum oven at 40 °C after the transfer Drying, copper hydroxide nanoribbon oriented film.

[0044] In this example, the solution of (4) is injected into the liquid phase at a speed of 1...

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Abstract

The invention discloses a preparation method of a copper hydroxide nanobelt oriented film. The method comprises the following steps: uniformly mixing 0.002-0.008 mol of cuprous nitrate trihydrate and5-15 mL of polyethylene glycol, performing dissolution, adding 1-5 g of sodium hydroxide particles, and performing a reaction for 2-10 h under stirring to form a blue suspension; performing washing for a plurality times by using distilled water and absolute ethanol to remove impurities, and performing dissolution in a high-purity ethanol solution to obtain a copper hydroxide precipitate; and injecting precursor solutions with different concentrations of 1-10 mol / mL into an aqueous solution at a speed of 100-1000 [mu]L / min to form an oriented film, transferring the oriented film onto a substrate, and performing drying in a vacuum drying oven at 40-60 DEG C. According to the preparation method provided by the invention, the copper hydroxide nanobelt oriented film prepared by the method has auniform surface, uniform arrangement of nanobelts and a higher orientation degree, and opens up novel possibilities for preparation methods of organic, inorganic and organic-inorganic hybrid orientedfilms.

Description

technical field [0001] The invention belongs to the technical field of nanometer materials, and in particular relates to a method for preparing a copper hydroxide nanobelt oriented film. Background technique [0002] In recent years, oriented thin film materials composed of organic, inorganic and organic-inorganic hybrid materials have been extensively studied. Due to their good physical and chemical properties, they can be used in many aspects such as separation of substances, electronics, optics and device equipment. Generally, organically oriented films can be obtained by methods such as mechanical shearing, solution pulling, and melt stretching, but there are certain defects. Mechanical shearing is not easy to prepare films with uniform surface and consistent orientation, and the instability of solution pulling makes The degree of orientation of the film is low, and it is difficult to prepare an organic oriented film with a high melting point and strong rigidity by melt ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01G3/02B82Y30/00B82Y40/00
CPCB82Y30/00B82Y40/00C01G3/02C01P2004/17
Inventor 萨百晟边智芸陈建辉温翠莲谭小林
Owner FUZHOU UNIV
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