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A kind of preparation method of lattice structure nickel-based sponge material

A lattice structure and sponge technology, applied in the field of foam metal materials, can solve the problems of poor uniformity of polyurethane foam, complex immersion and pyrolysis process, and no good compatibility, so as to improve uniformity and ensure performance. , the effect of prolonging the service life

Active Publication Date: 2020-06-26
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Although the preparation method has been gradually improved with the deepening of research work, the uniformity of the internal pores of the foamed metal cannot be guaranteed at present, such as the consistency of the internal pore size of the foamed metal, the consistency of the pore wall size, and the uniformity of the joints. The degree of uniform combination at the place, these three points cannot be guaranteed in the above-mentioned preparation method
The organic foam impregnation process is an important method for preparing metal foam at present, but the polyurethane foam used in it has many shortcomings: such as poor uniformity of the internal tendons of the polyurethane foam, and lack of good compatibility with the water-based slurry. Soaking stagnation and pyrolysis process are complicated, etc.

Method used

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  • A kind of preparation method of lattice structure nickel-based sponge material

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The preparation method of the present embodiment comprises the following steps:

[0026] Step 1. Use CAD drawing software to draw the internal lattice structure diagram of the nickel-based sponge material, and design the overall graphic with the size of the nickel-based sponge material 100mm×20mm (diameter×height) as the boundary, and then input the data of the overall graphic into 3D printing Equipment, using PLA plastic as raw material for 3D printing to prepare a lattice-structured plastic precursor with a uniform pore structure and a porosity of 75%; the internal pores of the nickel-based sponge material are in a snowflake-like structure. The root frame is 1mm;

[0027] Step 2, using 1.5mol / L NaOH solution to roughen the lattice structure plastic precursor obtained in step 1;

[0028] Step 3, In718 nickel-based alloy powder and additives are prepared into slurry; the additives include binder PVA, dispersant CMC, rheology modifier CMC and defoamer n-octanol, binder ...

Embodiment 2

[0034] The preparation method of the present embodiment comprises the following steps:

[0035]Step 1, use CAD drawing software to draw the internal lattice structure diagram of the nickel-based sponge material, and design the overall figure with the size of the nickel-based sponge material 10mm × 10mm × 20mm (length × width × height) as the boundary, and then the overall figure The data is input into the 3D printing equipment, and ABS plastic is used as a raw material for 3D printing to prepare a lattice-structured plastic precursor with a uniform pore structure and a porosity of 95%. The single skeleton in this structure is 1mm;

[0036] Step 2, using 3.5mol / L NaOH solution to roughen the lattice structure plastic precursor obtained in step 1;

[0037] Step 3, In690 nickel-based alloy powder and additives are prepared into slurry; the additives include binder PVA, dispersant CMC, rheology modifier CMC and defoamer n-octanol, binder in the slurry The mass percentage of PVA ...

Embodiment 3

[0042] The preparation method of the present embodiment comprises the following steps:

[0043] Step 1. Use CAD drawing software to draw the internal lattice structure diagram of the nickel-based sponge material, and design the overall graphic with the size of the nickel-based sponge material 100mm×20mm (diameter×height) as the boundary, and then input the data of the overall graphic into 3D printing equipment, using ABS plastic as raw material for 3D printing, and preparing a lattice-structured plastic precursor with a uniform pore structure and a porosity of 85%; the internal pores of the nickel-based sponge material have a face-centered cubic structure. The single frame is 1.2mm;

[0044] Step 2, using 2.78mol / L NaOH solution to roughen the lattice structure plastic precursor obtained in step 1;

[0045] Step 3, In718 nickel-based alloy powder and additives are prepared into slurry; the additives include binder PVA, dispersant CMC, rheology modifier CMC and defoamer n-octa...

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Abstract

The invention discloses a preparation method of a lattice structure nickel-based sponge material. The method comprises the steps that firstly, a lattice structure plastic precursor is prepared througha 3D printing method; secondly, roughening treatment is conducted on the lattice structure plastic precursor; thirdly, nickel-based alloy powder and an additive are made into slurry; fourthly, the roughened lattice structure plastic precursor is placed in the slurry and immersed, and then a nickel-based sponge material blank is obtained centrifugally; and fifthly, the nickel-based sponge materialblank is sintered, and the nickel-based sponge material is obtained. The lattice structure plastic precursor with a uniform structure is prepared through the 3D printing method and used as a framework of the nickel-based sponge material blank, the distribution uniformity of the slurry with the nickel-based alloy powder as a main component on the framework is improved, the nickel-based sponge material with pore structures is obtained, the uniformity of pores and pore ribs of the nickel-based sponge material is improved, good development of joints of the nickel-based sponge material is promoted, the performance of the nickel-based sponge material is ensured, and the service life of the nickel-based sponge material is prolonged.

Description

technical field [0001] The invention belongs to the technical field of metal foam materials, and in particular relates to a preparation method of a nickel-based sponge material with a lattice structure. Background technique [0002] There are many pores inside the metal foam, and the size, uniformity, connectivity, and closure of the pores all affect its performance. In recent years, metal foam has been widely used as sound-absorbing, shielding, shock-absorbing and impact-resistant materials. As the application environment puts forward higher and higher performance indicators for materials, higher requirements are also put forward for the preparation method of metal foam. At present, there are many methods for preparing metal foam: such as casting method, metal deposition method, powder metallurgy method, spray deposition method and so on. Although the preparation method has been gradually improved with the deepening of research work, the uniformity of the internal pores of...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/08C22C19/03B22F3/11B22F3/22B29C64/10B33Y10/00
CPCB22F3/1121B22F3/114B22F3/22B29C64/10B33Y10/00C22C19/03
Inventor 敖庆波王建忠马军李广忠汪强兵汤慧萍
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH